Soumyadip Sett | University of Illinois at Urbana-Champaign (original) (raw)

Papers by Soumyadip Sett

Research paper thumbnail of Wettability-defined frosting dynamics between plane fins in quiescent air

International Journal of Heat and Mass Transfer

Research paper thumbnail of Dynamic Defrosting on Superhydrophobic and Biphilic Surfaces

Research paper thumbnail of Jumping droplets electronics cooling: Promise versus reality

Research paper thumbnail of Condensation of Satellite Droplets on Lubricant-Cloaked Droplets

ACS Applied Materials & Interfaces

Research paper thumbnail of “Dancing Droplets”: Partial Coalescence on Superhydrophobic Surfaces

Journal of Heat Transfer

Droplet coalescence has received significant attention due to its significant role in fluid mixin... more Droplet coalescence has received significant attention due to its significant role in fluid mixing, microfluidics, coalescence-induced droplet jumping, and heat and mass transfer applications. Coalescence of droplets has been extensively investigated from the perspectives of hydrodynamics and energy transfer. However, the study of coalescence characteristics of size-mismatched droplets on superhydrophobic surfaces remains a challenge due to visualization difficulty, limited droplet size control, and poor droplet manipulation. Here, in order to study coalescence dynamics of droplets with arbitrary initial sizes, a droplet dispensing and visualization system was developed. To control the size of droplets, monodispersed droplets with radii of ≈20 μm were dispensed using a frequency-controlled piezoelectric pulse injector onto a superhydrophobic surface, enabling the target droplets to accumulate in volume and grow in radii. The coalescence process of droplets having radii of ≈270 and ≈...

Research paper thumbnail of Fundamental limits of jumping droplet heat transfer

Research paper thumbnail of Dropwise condensation on solid hydrophilic surfaces

Science Advances

Droplet nucleation and condensation are ubiquitous phenomena in nature and industry. Over the pas... more Droplet nucleation and condensation are ubiquitous phenomena in nature and industry. Over the past century, research has shown dropwise condensation heat transfer on nonwetting surfaces to be an order of magnitude higher than filmwise condensation heat transfer on wetting substrates. However, the necessity for nonwetting to achieve dropwise condensation is unclear. This article reports stable dropwise condensation on a smooth, solid, hydrophilic surface (θa = 38°) having low contact angle hysteresis (<3°). We show that the distribution of nano- to micro- to macroscale droplet sizes (about 100 nm to 1 mm) for coalescing droplets agrees well with the classical distribution on hydrophobic surfaces and elucidate that the wettability-governed dropwise-to-filmwise transition is mediated by the departing droplet Bond number. Our findings demonstrate that achieving stable dropwise condensation is not governed by surface intrinsic wettability, as assumed for the past eight decades, but ra...

Research paper thumbnail of “Swimming Jellyfish“: Visualizing Jet-Like Internal Flow in Coalescing Droplets

Journal of Heat Transfer

Surface-tension-driven droplet coalescence has received significant attention due to its signific... more Surface-tension-driven droplet coalescence has received significant attention due to its significant role in microfluidics, coalescence-induced droplet jumping, fluid mixing, and microscale heat and mass transfer. However, the study of internal flow characteristics of merging droplets remains a challenge due to visualization difficulty, limited droplet size control, poor droplet manipulation, and insufficient droplet front tracking. Here, in order to study droplet coalescence dynamics, a droplet dispensing and visualization system was developed. To control the size of droplets, monodispersed droplets with diameters of ≈ 40 μm were dispensed onto a superhydrophobic surface, enabling the target droplets to accumulate in volume and grow in radii. To track the internal flow front, an ethanol (20 wt %)-water mixture was used as the working fluid. Due to the unequal evaporation rate of water and ethanol, a density gradient was introduced at the liquid-gas interface of the droplets, result...

Research paper thumbnail of Stable Dropwise Condensation of Ethanol and Hexane on Rationally-Designed Ultra-Scalable Nanostructured Lubricant-Infused Surfaces

Research paper thumbnail of Hierarchical Condensation

Research paper thumbnail of Supplemental Material for Dynamic Defrosting on Superhydrophobic and Biphilic Surfaces

Research paper thumbnail of Atmosphere-Mediated Superhydrophobicity of Rationally Designed Micro/Nanostructured Surfaces

ACS Nano

Superhydrophobicity has received significant attention over the past three decades owing to its s... more Superhydrophobicity has received significant attention over the past three decades owing to its significant potential in self-cleaning and anti-icing surfaces, drag reduction, energy harvesting devices, anti-bacterial coatings, and enhanced heat transfer applications. Superhydrophobicity can be obtained via the roughening of an intrinsically hydrophobic surface, the creation of a re-entrant geometry, or by the roughening of a hydrophilic surface followed by a conformal coating of a hydrophobic material. Intrinsically hydrophobic surfaces have poor thermophysical properties such as thermal conductivity, and thus are not suitable for heat transfer applications. Re-entrant geometries, although versatile in applications where droplets are deposited, break down during spatially random nucleation and flood the surface. Chemical functionalization of rough metallic substrates, although promising, is not utilized due to the poor durability of conformal hydrophobic coatings. Here we develop a radically different approach to achieve stable superhydrophobicity. By utilizing laser processing and thermal oxidation of copper (Cu) to create a high surface energy hierarchical copper oxide (CuO), followed by repeatable and passive atmospheric adsorption of hydrophobic volatile organic compounds (VOCs), we show that stable superhydrophobicity with apparent advancing contact angles ≈ 160° and contact angle hysteresis as low as ≈ 20° can be achieved. We exploit the structure length scale and structure geometry dependent VOC adsorption dynamics to rationally design CuO nanowires with enhanced superhydrophobicity. To gain an understanding of the VOC adsorption physics, we utilized X-Ray Photoelectron and Ion Mass Spectroscopy to identify the chemical species deposited on our surfaces in two distinct locations: Urbana, IL, USA and Beijing, China. To test the stability of the atmosphere-mediated superhydrophobic surfaces during heterogeneous nucleation, we used high-speed optical microscopy to demonstrate the occurrence of dropwise condensation and stable coalescenceinduced droplet jumping. Our work not only provides rational design guidelines for developing passively-durable superhydrophobic surfaces with excellent flooding-resistance and self-healing capability, but also sheds light on the key role played by the atmosphere in governing wetting.

Research paper thumbnail of Droplet Jumping: Effects of Droplet Size, Surface Structure, Pinning, and Liquid Properties

Research paper thumbnail of Droplet Evaporation on Functional Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of Atmosphere-Mediated and Roughness-Variation-Induced Biphilic Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of Coalescence-Induced Droplet Jumping on Atmospheric-Mediated Superhydrophobic Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of On the nature of the superspreaders

Advances in Colloid and Interface Science

Research paper thumbnail of Superhydrophobic Surfaces Made from Naturally Derived Hydrophobic Materials

ACS Sustainable Chemistry & Engineering

Research paper thumbnail of Lubricant-Infused Surfaces for Low-Surface-Tension Fluids: Promise versus Reality

ACS applied materials & interfaces, Jan 18, 2017

The past few decades have seen substantial effort for the design and manufacturing of hydrophobic... more The past few decades have seen substantial effort for the design and manufacturing of hydrophobic structured surfaces for enhanced steam condensation in water-based applications. Such surfaces promote dropwise condensation and easy droplet removal. However, less priority has been given to applications utilizing low-surface-tension fluids as the condensate. Lubricant-infused surfaces (LISs) or slippery liquid-infused porous surfaces (SLIPSs) have recently been developed, where the atomically smooth, defect-free slippery surface leads to reduced pinning of water droplets and omniphobic characteristics. The remarkable results of LISs and SLIPSs with a range of working fluid droplets give hope of their viability with low-surface-tension condensates. However, the presence of the additional liquid in the form of lubricant brings other issues to consider. Here, in an effort to study the dropwise condensation potential of LISs and SLIPSs, we investigate the miscibility of a range of low-sur...

Research paper thumbnail of Impact of aqueous suspension drops onto non-wettable porous membranes: Hydrodynamic focusing and penetration of nanoparticles

Colloids and Surfaces A: Physicochemical and Engineering Aspects

ABSTRACT The impacts and dynamic penetration of nanoparticle suspension drops into porous filter ... more ABSTRACT The impacts and dynamic penetration of nanoparticle suspension drops into porous filter membranes are studied experimentally and theoretically. This type of penetration is associated with hydrodynamic focusing and is radically different from the wettability-driven imbibition. In the case of hydrodynamic focusing water can penetrate into a non-wettable porous medium at very low values of the dynamic pressure associated with drop impact. Two types of membranes are used in the experiments: (i) glass fiber filter membrane wettable by the carrier fluid (water), and (ii) polytetrafluoroethylene (PTFE) depth filter membrane, non-wettable by the carrier fluid. The nanoparticle entrainment and deposition inside the membrane bulk is used to mostly visualize the ultimate penetration fronts by observing the cut cross-sections of the membranes, albeit also provide an insight into innovative applications like circuit printing on nonwovens. The deposition patterns inside the membranes are also linked to the drop splashing patterns at their front surfaces. The experimental results confirm that during the dynamic focusing water can penetrate into a non-wettable porous medium (PTFE). Water also penetrates by the same hydrodynamic focusing mechanism into the wettable glass fiber membrane, where it additionally spreads on a much longer time scale due to the wettability-driven flow. A theory explaining hydrodynamic focusing penetration of liquid into porous medium after drop impact is proposed. It is used to explain and predict water penetration into the non-wettable filter medium after drop impact, and the results are compared with the experimental data. Also the critical thickness of non-wettable membranes determined by dissipation of the kinetic energy in flow inside membrane is evaluated and compared with the experimental data.

Research paper thumbnail of Wettability-defined frosting dynamics between plane fins in quiescent air

International Journal of Heat and Mass Transfer

Research paper thumbnail of Dynamic Defrosting on Superhydrophobic and Biphilic Surfaces

Research paper thumbnail of Jumping droplets electronics cooling: Promise versus reality

Research paper thumbnail of Condensation of Satellite Droplets on Lubricant-Cloaked Droplets

ACS Applied Materials & Interfaces

Research paper thumbnail of “Dancing Droplets”: Partial Coalescence on Superhydrophobic Surfaces

Journal of Heat Transfer

Droplet coalescence has received significant attention due to its significant role in fluid mixin... more Droplet coalescence has received significant attention due to its significant role in fluid mixing, microfluidics, coalescence-induced droplet jumping, and heat and mass transfer applications. Coalescence of droplets has been extensively investigated from the perspectives of hydrodynamics and energy transfer. However, the study of coalescence characteristics of size-mismatched droplets on superhydrophobic surfaces remains a challenge due to visualization difficulty, limited droplet size control, and poor droplet manipulation. Here, in order to study coalescence dynamics of droplets with arbitrary initial sizes, a droplet dispensing and visualization system was developed. To control the size of droplets, monodispersed droplets with radii of ≈20 μm were dispensed using a frequency-controlled piezoelectric pulse injector onto a superhydrophobic surface, enabling the target droplets to accumulate in volume and grow in radii. The coalescence process of droplets having radii of ≈270 and ≈...

Research paper thumbnail of Fundamental limits of jumping droplet heat transfer

Research paper thumbnail of Dropwise condensation on solid hydrophilic surfaces

Science Advances

Droplet nucleation and condensation are ubiquitous phenomena in nature and industry. Over the pas... more Droplet nucleation and condensation are ubiquitous phenomena in nature and industry. Over the past century, research has shown dropwise condensation heat transfer on nonwetting surfaces to be an order of magnitude higher than filmwise condensation heat transfer on wetting substrates. However, the necessity for nonwetting to achieve dropwise condensation is unclear. This article reports stable dropwise condensation on a smooth, solid, hydrophilic surface (θa = 38°) having low contact angle hysteresis (<3°). We show that the distribution of nano- to micro- to macroscale droplet sizes (about 100 nm to 1 mm) for coalescing droplets agrees well with the classical distribution on hydrophobic surfaces and elucidate that the wettability-governed dropwise-to-filmwise transition is mediated by the departing droplet Bond number. Our findings demonstrate that achieving stable dropwise condensation is not governed by surface intrinsic wettability, as assumed for the past eight decades, but ra...

Research paper thumbnail of “Swimming Jellyfish“: Visualizing Jet-Like Internal Flow in Coalescing Droplets

Journal of Heat Transfer

Surface-tension-driven droplet coalescence has received significant attention due to its signific... more Surface-tension-driven droplet coalescence has received significant attention due to its significant role in microfluidics, coalescence-induced droplet jumping, fluid mixing, and microscale heat and mass transfer. However, the study of internal flow characteristics of merging droplets remains a challenge due to visualization difficulty, limited droplet size control, poor droplet manipulation, and insufficient droplet front tracking. Here, in order to study droplet coalescence dynamics, a droplet dispensing and visualization system was developed. To control the size of droplets, monodispersed droplets with diameters of ≈ 40 μm were dispensed onto a superhydrophobic surface, enabling the target droplets to accumulate in volume and grow in radii. To track the internal flow front, an ethanol (20 wt %)-water mixture was used as the working fluid. Due to the unequal evaporation rate of water and ethanol, a density gradient was introduced at the liquid-gas interface of the droplets, result...

Research paper thumbnail of Stable Dropwise Condensation of Ethanol and Hexane on Rationally-Designed Ultra-Scalable Nanostructured Lubricant-Infused Surfaces

Research paper thumbnail of Hierarchical Condensation

Research paper thumbnail of Supplemental Material for Dynamic Defrosting on Superhydrophobic and Biphilic Surfaces

Research paper thumbnail of Atmosphere-Mediated Superhydrophobicity of Rationally Designed Micro/Nanostructured Surfaces

ACS Nano

Superhydrophobicity has received significant attention over the past three decades owing to its s... more Superhydrophobicity has received significant attention over the past three decades owing to its significant potential in self-cleaning and anti-icing surfaces, drag reduction, energy harvesting devices, anti-bacterial coatings, and enhanced heat transfer applications. Superhydrophobicity can be obtained via the roughening of an intrinsically hydrophobic surface, the creation of a re-entrant geometry, or by the roughening of a hydrophilic surface followed by a conformal coating of a hydrophobic material. Intrinsically hydrophobic surfaces have poor thermophysical properties such as thermal conductivity, and thus are not suitable for heat transfer applications. Re-entrant geometries, although versatile in applications where droplets are deposited, break down during spatially random nucleation and flood the surface. Chemical functionalization of rough metallic substrates, although promising, is not utilized due to the poor durability of conformal hydrophobic coatings. Here we develop a radically different approach to achieve stable superhydrophobicity. By utilizing laser processing and thermal oxidation of copper (Cu) to create a high surface energy hierarchical copper oxide (CuO), followed by repeatable and passive atmospheric adsorption of hydrophobic volatile organic compounds (VOCs), we show that stable superhydrophobicity with apparent advancing contact angles ≈ 160° and contact angle hysteresis as low as ≈ 20° can be achieved. We exploit the structure length scale and structure geometry dependent VOC adsorption dynamics to rationally design CuO nanowires with enhanced superhydrophobicity. To gain an understanding of the VOC adsorption physics, we utilized X-Ray Photoelectron and Ion Mass Spectroscopy to identify the chemical species deposited on our surfaces in two distinct locations: Urbana, IL, USA and Beijing, China. To test the stability of the atmosphere-mediated superhydrophobic surfaces during heterogeneous nucleation, we used high-speed optical microscopy to demonstrate the occurrence of dropwise condensation and stable coalescenceinduced droplet jumping. Our work not only provides rational design guidelines for developing passively-durable superhydrophobic surfaces with excellent flooding-resistance and self-healing capability, but also sheds light on the key role played by the atmosphere in governing wetting.

Research paper thumbnail of Droplet Jumping: Effects of Droplet Size, Surface Structure, Pinning, and Liquid Properties

Research paper thumbnail of Droplet Evaporation on Functional Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of Atmosphere-Mediated and Roughness-Variation-Induced Biphilic Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of Coalescence-Induced Droplet Jumping on Atmospheric-Mediated Superhydrophobic Surfaces

International Heat Transfer Conference 16

Research paper thumbnail of On the nature of the superspreaders

Advances in Colloid and Interface Science

Research paper thumbnail of Superhydrophobic Surfaces Made from Naturally Derived Hydrophobic Materials

ACS Sustainable Chemistry & Engineering

Research paper thumbnail of Lubricant-Infused Surfaces for Low-Surface-Tension Fluids: Promise versus Reality

ACS applied materials & interfaces, Jan 18, 2017

The past few decades have seen substantial effort for the design and manufacturing of hydrophobic... more The past few decades have seen substantial effort for the design and manufacturing of hydrophobic structured surfaces for enhanced steam condensation in water-based applications. Such surfaces promote dropwise condensation and easy droplet removal. However, less priority has been given to applications utilizing low-surface-tension fluids as the condensate. Lubricant-infused surfaces (LISs) or slippery liquid-infused porous surfaces (SLIPSs) have recently been developed, where the atomically smooth, defect-free slippery surface leads to reduced pinning of water droplets and omniphobic characteristics. The remarkable results of LISs and SLIPSs with a range of working fluid droplets give hope of their viability with low-surface-tension condensates. However, the presence of the additional liquid in the form of lubricant brings other issues to consider. Here, in an effort to study the dropwise condensation potential of LISs and SLIPSs, we investigate the miscibility of a range of low-sur...

Research paper thumbnail of Impact of aqueous suspension drops onto non-wettable porous membranes: Hydrodynamic focusing and penetration of nanoparticles

Colloids and Surfaces A: Physicochemical and Engineering Aspects

ABSTRACT The impacts and dynamic penetration of nanoparticle suspension drops into porous filter ... more ABSTRACT The impacts and dynamic penetration of nanoparticle suspension drops into porous filter membranes are studied experimentally and theoretically. This type of penetration is associated with hydrodynamic focusing and is radically different from the wettability-driven imbibition. In the case of hydrodynamic focusing water can penetrate into a non-wettable porous medium at very low values of the dynamic pressure associated with drop impact. Two types of membranes are used in the experiments: (i) glass fiber filter membrane wettable by the carrier fluid (water), and (ii) polytetrafluoroethylene (PTFE) depth filter membrane, non-wettable by the carrier fluid. The nanoparticle entrainment and deposition inside the membrane bulk is used to mostly visualize the ultimate penetration fronts by observing the cut cross-sections of the membranes, albeit also provide an insight into innovative applications like circuit printing on nonwovens. The deposition patterns inside the membranes are also linked to the drop splashing patterns at their front surfaces. The experimental results confirm that during the dynamic focusing water can penetrate into a non-wettable porous medium (PTFE). Water also penetrates by the same hydrodynamic focusing mechanism into the wettable glass fiber membrane, where it additionally spreads on a much longer time scale due to the wettability-driven flow. A theory explaining hydrodynamic focusing penetration of liquid into porous medium after drop impact is proposed. It is used to explain and predict water penetration into the non-wettable filter medium after drop impact, and the results are compared with the experimental data. Also the critical thickness of non-wettable membranes determined by dissipation of the kinetic energy in flow inside membrane is evaluated and compared with the experimental data.