C. Brera - Academia.edu (original) (raw)
Papers by C. Brera
Consiglio Nazionale delle Ricerche (CNR). Biblioteca Centrale / CNR - Consiglio Nazionale delle R... more Consiglio Nazionale delle Ricerche (CNR). Biblioteca Centrale / CNR - Consiglio Nazionale delle RichercheSIGLEITItal
EFSA Supporting Publications, 2020
Journal of AOAC INTERNATIONAL, 2003
A collaborative study was conducted to evaluate the effectiveness of an immunoaffinity column cle... more A collaborative study was conducted to evaluate the effectiveness of an immunoaffinity column cleanup liquid chromatography (LC) method for determination of aflatoxin B1 in cattle feed at a possible future European regulatory limit (1 ng/g). The test portion was extracted with acetone–water (85 + 15), filtered, diluted with water, and applied to an immunoaffinity column. The column was washed with water to remove interfering compounds, and the purified aflatoxin B1 was eluted with methanol. Aflatoxin B1 was separated and determined by reversed-phase liquid chromatography (RP–LC) and detected by fluorescence after post column derivatization (PCD) involving bromination. PCD was achieved with either pyridinium hydrobromide perbromide (PBPB), used by 14 laboratories, or an electrochemical cell and addition of bromide to the mobile phase, used by 7 laboratories. Both derivatization techniques were not significantly different when compared by the t-test; the method was statistically evalu...
Journal of Animal and Feed Sciences, 2016
Cancer epidemiology, biomarkers & prevention : a publication of the American Association for Cancer Research, cosponsored by the American Society of Preventive Oncology, 1999
Ochratoxin A (OTA), a mycotoxin widely contaminating staple foods and beverages, has been classif... more Ochratoxin A (OTA), a mycotoxin widely contaminating staple foods and beverages, has been classified as a "possible human carcinogen (Group 2B)" by the IARC. Serum levels of OTA were measured in a group of 138 healthy adults (age, 35-65 years) living in the area surrounding Florence (Tuscany, central Italy) and detected in all but four samples (97%). After the exclusion of one subject with a peak value of 57.2 ng/ml, OTA levels ranged between 0.12 and 2.84 ng/ml, with mean and median values of 0.56 and 0.48 ng/ml, respectively. OTA levels were significantly higher in men than in women (0.64 versus 0.50) and correlated positively with height. A strong association was found with the season in which blood samples were obtained, with summer values higher than autumn values. On the other hand, OTA levels tended to be negatively associated with blood pressure, either systolic or diastolic; no association was evident with age, weight, body mass index, and smoking history. The ass...
Animal Feed Contamination, 2012
Food Additives & Contaminants, 2005
Accreditation and Quality Assurance, 2006
This paper describes the interlaboratory study aimed at assessing the performance of 18 laborator... more This paper describes the interlaboratory study aimed at assessing the performance of 18 laboratories (14 national and 4 European) for Ochratoxin A (OTA) determination in cocoa powder samples. The study was tested at three levels of OTA covering the range in which presumably European regulatory limits could fall in the near future. For the extraction step, almost all laboratories used
Mycotoxins: detection methods, management, public health and agricultural trade, 2008
World Mycotoxin Journal, 2011
Italian journal of food …, 2005
Résumé/Abstract The aim of this study was to develop a sampling procedure to quantify genetically... more Résumé/Abstract The aim of this study was to develop a sampling procedure to quantify genetically-modified Round-up Ready (GM RR) soybeans in a lot. Seven lots (35 kg each) fortified with three different percentages of GM RR soybeans (4 lots at 1%, 2 lots at 10%, ...
Consiglio Nazionale delle Ricerche (CNR). Biblioteca Centrale / CNR - Consiglio Nazionale delle R... more Consiglio Nazionale delle Ricerche (CNR). Biblioteca Centrale / CNR - Consiglio Nazionale delle RichercheSIGLEITItal
EFSA Supporting Publications, 2020
Journal of AOAC INTERNATIONAL, 2003
A collaborative study was conducted to evaluate the effectiveness of an immunoaffinity column cle... more A collaborative study was conducted to evaluate the effectiveness of an immunoaffinity column cleanup liquid chromatography (LC) method for determination of aflatoxin B1 in cattle feed at a possible future European regulatory limit (1 ng/g). The test portion was extracted with acetone–water (85 + 15), filtered, diluted with water, and applied to an immunoaffinity column. The column was washed with water to remove interfering compounds, and the purified aflatoxin B1 was eluted with methanol. Aflatoxin B1 was separated and determined by reversed-phase liquid chromatography (RP–LC) and detected by fluorescence after post column derivatization (PCD) involving bromination. PCD was achieved with either pyridinium hydrobromide perbromide (PBPB), used by 14 laboratories, or an electrochemical cell and addition of bromide to the mobile phase, used by 7 laboratories. Both derivatization techniques were not significantly different when compared by the t-test; the method was statistically evalu...
Journal of Animal and Feed Sciences, 2016
Cancer epidemiology, biomarkers & prevention : a publication of the American Association for Cancer Research, cosponsored by the American Society of Preventive Oncology, 1999
Ochratoxin A (OTA), a mycotoxin widely contaminating staple foods and beverages, has been classif... more Ochratoxin A (OTA), a mycotoxin widely contaminating staple foods and beverages, has been classified as a "possible human carcinogen (Group 2B)" by the IARC. Serum levels of OTA were measured in a group of 138 healthy adults (age, 35-65 years) living in the area surrounding Florence (Tuscany, central Italy) and detected in all but four samples (97%). After the exclusion of one subject with a peak value of 57.2 ng/ml, OTA levels ranged between 0.12 and 2.84 ng/ml, with mean and median values of 0.56 and 0.48 ng/ml, respectively. OTA levels were significantly higher in men than in women (0.64 versus 0.50) and correlated positively with height. A strong association was found with the season in which blood samples were obtained, with summer values higher than autumn values. On the other hand, OTA levels tended to be negatively associated with blood pressure, either systolic or diastolic; no association was evident with age, weight, body mass index, and smoking history. The ass...
Animal Feed Contamination, 2012
Food Additives & Contaminants, 2005
Accreditation and Quality Assurance, 2006
This paper describes the interlaboratory study aimed at assessing the performance of 18 laborator... more This paper describes the interlaboratory study aimed at assessing the performance of 18 laboratories (14 national and 4 European) for Ochratoxin A (OTA) determination in cocoa powder samples. The study was tested at three levels of OTA covering the range in which presumably European regulatory limits could fall in the near future. For the extraction step, almost all laboratories used
Mycotoxins: detection methods, management, public health and agricultural trade, 2008
World Mycotoxin Journal, 2011
Italian journal of food …, 2005
Résumé/Abstract The aim of this study was to develop a sampling procedure to quantify genetically... more Résumé/Abstract The aim of this study was to develop a sampling procedure to quantify genetically-modified Round-up Ready (GM RR) soybeans in a lot. Seven lots (35 kg each) fortified with three different percentages of GM RR soybeans (4 lots at 1%, 2 lots at 10%, ...