Dale Barkey - Academia.edu (original) (raw)

Papers by Dale Barkey

Research paper thumbnail of Pattern Formation in Anodic Aluminum Oxide Growth by Flow Instability and Dynamic Re-Stabilization

ECS transactions, Dec 17, 2019

The viscous flow of oxide driven by the electrostriction force during growth of anodic aluminum o... more The viscous flow of oxide driven by the electrostriction force during growth of anodic aluminum oxide is treated by linear stability analysis and scale analysis. It is shown that a uniform oxide film is unstable to a periodic deformation. The re-stabilization of pore growth is examined by scale analysis of the steady pore diameter. The pattern spatial period and pore radius predicted by the analysis is compared with experimental observations reported in the literature.

Research paper thumbnail of Corrosion of Steel Reinforcement in Concrete Adjacent to Surface Repairs

American Concrete Institute, Journal of, 2004

Reinforced concrete may be damaged by chloride-induced corrosion of steel reinforcement, resultin... more Reinforced concrete may be damaged by chloride-induced corrosion of steel reinforcement, resulting in spalling and delamination as corrosion products accumulate. A surface repair entails removal of damaged concrete and its replacement with repair material. The resulting inhomogeneity between the repair material and remaining chloride-contaminated concrete, however, may produce active-passive corrosion macrocells that drive rapid anodic dissolution of the metal. This experimental study was conducted to characterize the geometry, current distribution, and controlling resistance of corrosion macrocells driven by differences in the electrochemical environment in repair material and contaminated concrete. Additional influences such as galvanic contact between the test reinforcement bar and remote cathode bars were also considered. The tests were based on ASTM G 109, with modifications to incorporate simulated repairs.

Research paper thumbnail of Influence of Additives on the Growth Velocity and Morphology of Branching Copper Electrodeposits

Journal of The Electrochemical Society, 2005

... SK Chawla, Polyhedron, 18, 1397 (1999). GB McFadden, SR Coriell, TP Moffat, D. Josell, D. Whe... more ... SK Chawla, Polyhedron, 18, 1397 (1999). GB McFadden, SR Coriell, TP Moffat, D. Josell, D. Wheeler, W. Schwarzacher, and J. Mallet, “A Mechanism for Brightening,” J. Electrochem. ... MAPasquale, SL Marchiano, and AJ Arvia, J. Electroanal. Chem., 532, 255 (2002). ...

Research paper thumbnail of High-Aspect-Ratio Copper-Via-Filling for Three-Dimensional Chip Stacking

Journal of The Electrochemical Society, 2005

Research paper thumbnail of Adsorption of Benzyl Viologen Dichloride and Its Displacement By 3-Mercapto-1-Propanesulfonate during Copper Electrodeposition

Research paper thumbnail of Studies on High Speed Electroforming

Research paper thumbnail of Nucleation of Tin and Tin–Silver Alloy on Copper and Nickel in Acid Plating Baths

Journal of The Electrochemical Society, 2007

The rate of nucleation and number density of nuclei of tin and tin-silver deposits on copper and ... more The rate of nucleation and number density of nuclei of tin and tin-silver deposits on copper and nickel substrates in acid sulfate and acid methanesulfonate baths were measured by application of a nucleation model to chronoamperometric data. Based on the dependence of nucleation rate on overpotential, the critical Gibbs free energy of nucleation and the critical nucleation size were calculated. A mechanism of alloy nucleation in the presence of thiourea is proposed.

Research paper thumbnail of Studies on Through-Chip Via Filling for Wafer-Level 3D Packaging

ECS Meeting Abstracts, 2006

not Available.

Research paper thumbnail of Polyol Silver Nanowire Synthesis and the Outlook for a Green Process

Journal of Nanomaterials, 2020

Silver nanowires (AgNWs) have a broad range of applications including nanoelectronics, energy con... more Silver nanowires (AgNWs) have a broad range of applications including nanoelectronics, energy conversion, health care, solar cells, touch screens, sensors and biosensors, wearable electronics, and drug delivery systems. As their characteristics depend strongly on their size and morphology, it is essential to find the optimal and most cost-effective synthesis method with precise control over the size and morphology of the wires. Various methods for AgNW synthesis have been reported along with process optimization and novel techniques to increase the yield and aspect ratios of synthesized AgNWs. The most promising processes for synthesis of AgNWs are wet chemical techniques, in which the polyol process is low cost and simple and provides high yield compared to other chemical methods. Reaction mechanism is one of the most important factors in strategies to control the process. Our purpose here is to provide an overview on the main findings regarding synthesis, preparation, and characte...

Research paper thumbnail of Parametric Study, Sensitivity Analysis, and Optimization of Polyol Synthesis of Silver Nanowires

ECS Journal of Solid State Science and Technology, 2017

Research paper thumbnail of Nonlinear evolution of a thin anodic film

Proceedings of the Royal Society A: Mathematical, Physical and Engineering Science, 2017

Research paper thumbnail of Rheological behavior of silver nanowire conductive inks during screen printing

Journal of Nanoparticle Research, 2016

The rheological behavior of silver nanowire (AgNW) suspensions adapted for screen printing inks w... more The rheological behavior of silver nanowire (AgNW) suspensions adapted for screen printing inks was investigated. Aqueous silver nanowire inks consisting of AgNW (length of 30 μm, and diameter of 40 and 90 nm), dispersant and binder were formulated. The effect of AgNW content on the rheological behavior of the ink and the build-up of ink structure after screen printing were examined as they depend on applied shear and temperature. Rheological measurements under conditions that mimic the screen printing process were done to assess viscoelastic properties induced by flow alignment of the wires and the subsequent recovery of the low shear structure. The Stretched Exponential model (SEmo) was used to model the recovery process after screen printing to obtain the characteristic time of the recovery or build-up process. The characteristic time was determined at several temperatures to obtain the activation energy of recovery. The domination of Brownian motion or non-Brownian motion behavior can be characterized by a Peclet number, which is the ratio of shear rate to the rotational diffusion coefficient. The Peclet number and the dimensionless concentration of wires were used to assess the recovery mechanism. The steady viscosity at low and high shear rates was also treated by an activation energy analysis.

Research paper thumbnail of Studies on high-speed electroforming

Ph D Thesis California Univ Berkeley Lawrence Berkeley Lab, Aug 1, 1987

Research paper thumbnail of Corrosion of copper in acid-sulfate plating baths with additives

Plating and Surface Finishing, 2003

Acid copper plating baths exposed to air present a corrosive environment for copper. With feature... more Acid copper plating baths exposed to air present a corrosive environment for copper. With feature sizes in some plating applications falling well below the micrometer scale, dissolution of metal at open circuit potential may become a consideration in process design. This paper presents a reaction-zone model of the corrosion process that can be used to estimate corrosion rates based on process parameters and open-circuit potential measurements. Corrosion of copper in acid-sulfate plating baths with additives chloride, benzotriazole and bis (3-sulfopropyl) disulfide is examined experimentally with the aid of the model.

Research paper thumbnail of Erratum to: Acceleration Effect

Nanostructure Science and Technology, 2014

Research paper thumbnail of Laplace- and diffusion-field-controlled growth in electrochemical deposition

Physical review letters, Jan 5, 1989

Research paper thumbnail of Structure and Pattern Formation in Electrodeposition

Advances in Electrochemical Science and Engineering, Volume 7

Research paper thumbnail of Acceleration Effect

Nanostructure Science and Technology, 2013

Research paper thumbnail of Copper Electrodeposition for Nanofabrication of Electronics Devices

Nanostructure Science and Technology, 2014

Preface (Kazuo Kondo) PART 1 Copper electrodepositon and additive chemistry Chapter 1 - Copper el... more Preface (Kazuo Kondo) PART 1 Copper electrodepositon and additive chemistry Chapter 1 - Copper electrodeposition (Masayuki Yokoi) Chapter 2 - Suppression effect and Additive Chemistry (Masayuki Yokoi) Chapter 3- Acceleration effect (Dale P. Barkey) Chapter 4- Modeling and Simulation ( Yutaka Kaneko) PART 2 Copper on chip metallization Chapter 5- Frontiers of Cu Electrodeposition and Electroless Plating for On-Chip Interconnects (James R. Rohan) Chapter 6- Microstructure of Evolution of Copper in Nano-scale Interconnect Features (James Kelly, Christopher Parks, James Demarest, and Christopher Penny) Chapter 7- Direct Copper Plating (Aleksandar Radisic and Philippe M. Vereecken) Part 3 - Through Silicon Via and Other Methods Chapter 8- Through Silicon Via (Kazuo Kondo) Chapter 9- Build-up Printed Wiring board (Kiyoshi Takagi a and Toshkazu Okubo) Chapter 10- Copper Foil Smooth on Both Sides for Lithium Ion Battery (Akitoshi Suzuki and Jun Shinozaki) Chapter 11- Through hole plating (Wei-Ping Dow)

Research paper thumbnail of Kinetic selection of morphology and growth velocity in electrochemical deposition

Research paper thumbnail of Pattern Formation in Anodic Aluminum Oxide Growth by Flow Instability and Dynamic Re-Stabilization

ECS transactions, Dec 17, 2019

The viscous flow of oxide driven by the electrostriction force during growth of anodic aluminum o... more The viscous flow of oxide driven by the electrostriction force during growth of anodic aluminum oxide is treated by linear stability analysis and scale analysis. It is shown that a uniform oxide film is unstable to a periodic deformation. The re-stabilization of pore growth is examined by scale analysis of the steady pore diameter. The pattern spatial period and pore radius predicted by the analysis is compared with experimental observations reported in the literature.

Research paper thumbnail of Corrosion of Steel Reinforcement in Concrete Adjacent to Surface Repairs

American Concrete Institute, Journal of, 2004

Reinforced concrete may be damaged by chloride-induced corrosion of steel reinforcement, resultin... more Reinforced concrete may be damaged by chloride-induced corrosion of steel reinforcement, resulting in spalling and delamination as corrosion products accumulate. A surface repair entails removal of damaged concrete and its replacement with repair material. The resulting inhomogeneity between the repair material and remaining chloride-contaminated concrete, however, may produce active-passive corrosion macrocells that drive rapid anodic dissolution of the metal. This experimental study was conducted to characterize the geometry, current distribution, and controlling resistance of corrosion macrocells driven by differences in the electrochemical environment in repair material and contaminated concrete. Additional influences such as galvanic contact between the test reinforcement bar and remote cathode bars were also considered. The tests were based on ASTM G 109, with modifications to incorporate simulated repairs.

Research paper thumbnail of Influence of Additives on the Growth Velocity and Morphology of Branching Copper Electrodeposits

Journal of The Electrochemical Society, 2005

... SK Chawla, Polyhedron, 18, 1397 (1999). GB McFadden, SR Coriell, TP Moffat, D. Josell, D. Whe... more ... SK Chawla, Polyhedron, 18, 1397 (1999). GB McFadden, SR Coriell, TP Moffat, D. Josell, D. Wheeler, W. Schwarzacher, and J. Mallet, “A Mechanism for Brightening,” J. Electrochem. ... MAPasquale, SL Marchiano, and AJ Arvia, J. Electroanal. Chem., 532, 255 (2002). ...

Research paper thumbnail of High-Aspect-Ratio Copper-Via-Filling for Three-Dimensional Chip Stacking

Journal of The Electrochemical Society, 2005

Research paper thumbnail of Adsorption of Benzyl Viologen Dichloride and Its Displacement By 3-Mercapto-1-Propanesulfonate during Copper Electrodeposition

Research paper thumbnail of Studies on High Speed Electroforming

Research paper thumbnail of Nucleation of Tin and Tin–Silver Alloy on Copper and Nickel in Acid Plating Baths

Journal of The Electrochemical Society, 2007

The rate of nucleation and number density of nuclei of tin and tin-silver deposits on copper and ... more The rate of nucleation and number density of nuclei of tin and tin-silver deposits on copper and nickel substrates in acid sulfate and acid methanesulfonate baths were measured by application of a nucleation model to chronoamperometric data. Based on the dependence of nucleation rate on overpotential, the critical Gibbs free energy of nucleation and the critical nucleation size were calculated. A mechanism of alloy nucleation in the presence of thiourea is proposed.

Research paper thumbnail of Studies on Through-Chip Via Filling for Wafer-Level 3D Packaging

ECS Meeting Abstracts, 2006

not Available.

Research paper thumbnail of Polyol Silver Nanowire Synthesis and the Outlook for a Green Process

Journal of Nanomaterials, 2020

Silver nanowires (AgNWs) have a broad range of applications including nanoelectronics, energy con... more Silver nanowires (AgNWs) have a broad range of applications including nanoelectronics, energy conversion, health care, solar cells, touch screens, sensors and biosensors, wearable electronics, and drug delivery systems. As their characteristics depend strongly on their size and morphology, it is essential to find the optimal and most cost-effective synthesis method with precise control over the size and morphology of the wires. Various methods for AgNW synthesis have been reported along with process optimization and novel techniques to increase the yield and aspect ratios of synthesized AgNWs. The most promising processes for synthesis of AgNWs are wet chemical techniques, in which the polyol process is low cost and simple and provides high yield compared to other chemical methods. Reaction mechanism is one of the most important factors in strategies to control the process. Our purpose here is to provide an overview on the main findings regarding synthesis, preparation, and characte...

Research paper thumbnail of Parametric Study, Sensitivity Analysis, and Optimization of Polyol Synthesis of Silver Nanowires

ECS Journal of Solid State Science and Technology, 2017

Research paper thumbnail of Nonlinear evolution of a thin anodic film

Proceedings of the Royal Society A: Mathematical, Physical and Engineering Science, 2017

Research paper thumbnail of Rheological behavior of silver nanowire conductive inks during screen printing

Journal of Nanoparticle Research, 2016

The rheological behavior of silver nanowire (AgNW) suspensions adapted for screen printing inks w... more The rheological behavior of silver nanowire (AgNW) suspensions adapted for screen printing inks was investigated. Aqueous silver nanowire inks consisting of AgNW (length of 30 μm, and diameter of 40 and 90 nm), dispersant and binder were formulated. The effect of AgNW content on the rheological behavior of the ink and the build-up of ink structure after screen printing were examined as they depend on applied shear and temperature. Rheological measurements under conditions that mimic the screen printing process were done to assess viscoelastic properties induced by flow alignment of the wires and the subsequent recovery of the low shear structure. The Stretched Exponential model (SEmo) was used to model the recovery process after screen printing to obtain the characteristic time of the recovery or build-up process. The characteristic time was determined at several temperatures to obtain the activation energy of recovery. The domination of Brownian motion or non-Brownian motion behavior can be characterized by a Peclet number, which is the ratio of shear rate to the rotational diffusion coefficient. The Peclet number and the dimensionless concentration of wires were used to assess the recovery mechanism. The steady viscosity at low and high shear rates was also treated by an activation energy analysis.

Research paper thumbnail of Studies on high-speed electroforming

Ph D Thesis California Univ Berkeley Lawrence Berkeley Lab, Aug 1, 1987

Research paper thumbnail of Corrosion of copper in acid-sulfate plating baths with additives

Plating and Surface Finishing, 2003

Acid copper plating baths exposed to air present a corrosive environment for copper. With feature... more Acid copper plating baths exposed to air present a corrosive environment for copper. With feature sizes in some plating applications falling well below the micrometer scale, dissolution of metal at open circuit potential may become a consideration in process design. This paper presents a reaction-zone model of the corrosion process that can be used to estimate corrosion rates based on process parameters and open-circuit potential measurements. Corrosion of copper in acid-sulfate plating baths with additives chloride, benzotriazole and bis (3-sulfopropyl) disulfide is examined experimentally with the aid of the model.

Research paper thumbnail of Erratum to: Acceleration Effect

Nanostructure Science and Technology, 2014

Research paper thumbnail of Laplace- and diffusion-field-controlled growth in electrochemical deposition

Physical review letters, Jan 5, 1989

Research paper thumbnail of Structure and Pattern Formation in Electrodeposition

Advances in Electrochemical Science and Engineering, Volume 7

Research paper thumbnail of Acceleration Effect

Nanostructure Science and Technology, 2013

Research paper thumbnail of Copper Electrodeposition for Nanofabrication of Electronics Devices

Nanostructure Science and Technology, 2014

Preface (Kazuo Kondo) PART 1 Copper electrodepositon and additive chemistry Chapter 1 - Copper el... more Preface (Kazuo Kondo) PART 1 Copper electrodepositon and additive chemistry Chapter 1 - Copper electrodeposition (Masayuki Yokoi) Chapter 2 - Suppression effect and Additive Chemistry (Masayuki Yokoi) Chapter 3- Acceleration effect (Dale P. Barkey) Chapter 4- Modeling and Simulation ( Yutaka Kaneko) PART 2 Copper on chip metallization Chapter 5- Frontiers of Cu Electrodeposition and Electroless Plating for On-Chip Interconnects (James R. Rohan) Chapter 6- Microstructure of Evolution of Copper in Nano-scale Interconnect Features (James Kelly, Christopher Parks, James Demarest, and Christopher Penny) Chapter 7- Direct Copper Plating (Aleksandar Radisic and Philippe M. Vereecken) Part 3 - Through Silicon Via and Other Methods Chapter 8- Through Silicon Via (Kazuo Kondo) Chapter 9- Build-up Printed Wiring board (Kiyoshi Takagi a and Toshkazu Okubo) Chapter 10- Copper Foil Smooth on Both Sides for Lithium Ion Battery (Akitoshi Suzuki and Jun Shinozaki) Chapter 11- Through hole plating (Wei-Ping Dow)

Research paper thumbnail of Kinetic selection of morphology and growth velocity in electrochemical deposition