John Caradonna - Academia.edu (original) (raw)
Papers by John Caradonna
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
Chemischer Informationsdienst, Jan 25, 1983
Advances in Molecular Relaxation and Interaction Processes, Aug 1, 1979
Abstract Structural and spectroscopic data are presented on the compound 1-methylcytosine hemihyd... more Abstract Structural and spectroscopic data are presented on the compound 1-methylcytosine hemihydroiodide hemihydrate. In the solid, a 1:1 triply hydrogenbonded complex consisting of one protonated and one neutral 1-methylcytosine base is observed. The hydrogen bonding in this complex is asymmetric, and the asymmetry in the interbase hydrogen bonding is stimulated, at least in part, by base stacking considerations. The hydrogen-bonded base pairs associate into dimers about a crystallographic center of symmetry; the base-base stacking mode is strong [mean stacking distance = 3.22A] and is such that the molecular overlap is between protonated and neutral 1-methylcytosine molecules. The asymmetric, interbase hydrogen bonding and the protonated over neutral base stacking mode coexist in a synergistic interrelationship which maximizes molecular association and crystal packing. Intermolecular hydrogen bonds involving the 1-methylcytosine bases, the water of crystallization and the iodide anion also contribute to the overall crystal stability. Infra-red and 1H nmr data are also presented.
Advances in Molecular Relaxation and Interaction Processes, Aug 1, 1979
Abstract The structural properties of the salts protonated 1-methylcytosine perchlorate and proto... more Abstract The structural properties of the salts protonated 1-methylcytosine perchlorate and protonated 1benzylcytosine nitrate are reported. In each of the salts, it has been definitively established that N(3) of the cytosine ring is the site of protonation. Cation-anion hydrogen-bonding interactions of the type seen in the hydrohalide salts of protonated, N(1)-substituted cytosine derivatives are also observed to some extent in these systems. In addition, the stability of both these salts depends on other factors. In particular, the interpyrimidine hydrogen bonding in the perchlorate salt is very strong and observed here for the first time. Cation-anion stacking forces in the nitrate salt are vital to the observed crystal packing.
Biochemistry, Apr 25, 2002
ABSTRACT
Chemischer Informationsdienst, May 6, 1980
Chemischer Informationsdienst, Sep 19, 1978
Platinum Coordination Complexes in Cancer Chemotherapy, 1984
Over a decade has passed since the initial observation that neutral platinum amine coordination c... more Over a decade has passed since the initial observation that neutral platinum amine coordination compounds with cis configuration of labile groups were effective chemotherapeutic agents.1 Subsequent studies built a strong case that DNA is the relevant biological target of these complexes.2,3 Substantial effort has therefore been directed towards defining and characterizing the interactions of cis-Pt(NH3)2Cl2 (cis-DDP) and the inactive trans-Pt(NH3)2Cl2 (trans-DDP),4 the structures of which are shown in Figure 1, with DNA at the molecular level.
Journal of Inorganic Biochemistry, 1993
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
An entry from the Cambridge Structural Database, the world's repository for small molecule cr... more An entry from the Cambridge Structural Database, the world's repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.
Chemischer Informationsdienst, Jan 25, 1983
Advances in Molecular Relaxation and Interaction Processes, Aug 1, 1979
Abstract Structural and spectroscopic data are presented on the compound 1-methylcytosine hemihyd... more Abstract Structural and spectroscopic data are presented on the compound 1-methylcytosine hemihydroiodide hemihydrate. In the solid, a 1:1 triply hydrogenbonded complex consisting of one protonated and one neutral 1-methylcytosine base is observed. The hydrogen bonding in this complex is asymmetric, and the asymmetry in the interbase hydrogen bonding is stimulated, at least in part, by base stacking considerations. The hydrogen-bonded base pairs associate into dimers about a crystallographic center of symmetry; the base-base stacking mode is strong [mean stacking distance = 3.22A] and is such that the molecular overlap is between protonated and neutral 1-methylcytosine molecules. The asymmetric, interbase hydrogen bonding and the protonated over neutral base stacking mode coexist in a synergistic interrelationship which maximizes molecular association and crystal packing. Intermolecular hydrogen bonds involving the 1-methylcytosine bases, the water of crystallization and the iodide anion also contribute to the overall crystal stability. Infra-red and 1H nmr data are also presented.
Advances in Molecular Relaxation and Interaction Processes, Aug 1, 1979
Abstract The structural properties of the salts protonated 1-methylcytosine perchlorate and proto... more Abstract The structural properties of the salts protonated 1-methylcytosine perchlorate and protonated 1benzylcytosine nitrate are reported. In each of the salts, it has been definitively established that N(3) of the cytosine ring is the site of protonation. Cation-anion hydrogen-bonding interactions of the type seen in the hydrohalide salts of protonated, N(1)-substituted cytosine derivatives are also observed to some extent in these systems. In addition, the stability of both these salts depends on other factors. In particular, the interpyrimidine hydrogen bonding in the perchlorate salt is very strong and observed here for the first time. Cation-anion stacking forces in the nitrate salt are vital to the observed crystal packing.
Biochemistry, Apr 25, 2002
ABSTRACT
Chemischer Informationsdienst, May 6, 1980
Chemischer Informationsdienst, Sep 19, 1978
Platinum Coordination Complexes in Cancer Chemotherapy, 1984
Over a decade has passed since the initial observation that neutral platinum amine coordination c... more Over a decade has passed since the initial observation that neutral platinum amine coordination compounds with cis configuration of labile groups were effective chemotherapeutic agents.1 Subsequent studies built a strong case that DNA is the relevant biological target of these complexes.2,3 Substantial effort has therefore been directed towards defining and characterizing the interactions of cis-Pt(NH3)2Cl2 (cis-DDP) and the inactive trans-Pt(NH3)2Cl2 (trans-DDP),4 the structures of which are shown in Figure 1, with DNA at the molecular level.
Journal of Inorganic Biochemistry, 1993