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Papers by Luisella Saba
This is an Open Access article distributed under the terms of the Creative Commons Attribution Li... more This is an Open Access article distributed under the terms of the Creative Commons Attribution License
The Italian journal of biochemistry
A peroxidase has been purified to homogeneity from Astragalus maritimus seeds using ammonium sulf... more A peroxidase has been purified to homogeneity from Astragalus maritimus seeds using ammonium sulfate precipitation and chromatography on DEAE-cellulose and hydroxylapatite. The purification obtained was 255 fold. The enzyme preparations were homogenous by the criteria of SDS-PAGE and analytical gel electrofocusing. The protein contained 0.11% of iron that corresponds to a minimum molecular size of 50,700. Determinations of molecular size by SDS-PAGE gave values of 48,000 +/- 1,000 while the one obtained by Sephadex gel filtration was 49,000. The pH optimum of the enzyme was 6.0. The activation energy was estimated to be 6 Kcal/mol. The prosthetic group was shown to be ferriprotoporphyrin IX. The presence of 13% neutral sugars was found. The spectrophotometric analysis showed the presence, in the visible region, of absorption maxima at 403, 490 and 633 nm. The Rz value (A403/A275) was 2.7.
Prenatal Diagnosis, 2014
Dipartimento di Sanità Pubblica e Medicina Clinica e Molecolare, Università degli Studi di Caglia... more Dipartimento di Sanità Pubblica e Medicina Clinica e Molecolare, Università degli Studi di Cagliari, Cagliari, Italy Struttura Complessa di Ostetricia e Ginecologia, Ospedale Microcitemico, Cagliari, Italy Servizio di Screening e Consulenza genetica, Ospedale Microcitemico, Cagliari, Italy *Correspondence to: Maria Cristina Rosatelli. E-mail: rosatelli@unica.it These authors equally contributed to the article.
Pharmacogenomics, 2010
Background: Pharmacogenetics is the study of genetic variations that cause alterations in drug le... more Background: Pharmacogenetics is the study of genetic variations that cause alterations in drug level, drug response and adverse drug reactions. SNPs found in CYP450 genes have the greatest genetic influences on interindividual variability in drug bioavailability. The polymorphic nature of these genes may modulate several enzyme levels that affect individual responses to pharmacological treatment. Among them, CYP3A4, CYP3A5, CYP2C9 and CYP2C19 isoforms of CYP450 enzymes are involved in the metabolism of many commonly prescribed drugs. Aims: In this study, we would like to develop a CYP450 genotyping platform that could lead a complete definition of a patient’s metabolic genotype in order to improve the clinical outcome of some drug treatments. Materials & methods: We used matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) (Sequenom®) to develop a SNP genotyping method. Results: This MALDI-TOF-based multiplexing system allows the simultaneous a...
Journal of Medical Genetics, 1997
This study reports the molecular characterisation of the bilirubin UDPglucuronosyl-transferase ge... more This study reports the molecular characterisation of the bilirubin UDPglucuronosyl-transferase gene (UGT1) in a group of patients of Sardinian descent with Crigler-Najjar syndrome type I and their relatives. Sequence analysis of both UGT1A exon 1 and common exons 2-5 was performed in all patients, leading to the detection of AF170 and a novel mutation (470insT), both residing in UGT1A exon 1. All but two heterozygotes for the AF170 mutation showed normal serum bilirubin levels. These two subjects were also heterozygous for the sequence variation A(TA)7TAA in the promoter region of the UGT1A gene.
This is an Open Access article distributed under the terms of the Creative Commons Attribution Li... more This is an Open Access article distributed under the terms of the Creative Commons Attribution License
The Italian journal of biochemistry
A peroxidase has been purified to homogeneity from Astragalus maritimus seeds using ammonium sulf... more A peroxidase has been purified to homogeneity from Astragalus maritimus seeds using ammonium sulfate precipitation and chromatography on DEAE-cellulose and hydroxylapatite. The purification obtained was 255 fold. The enzyme preparations were homogenous by the criteria of SDS-PAGE and analytical gel electrofocusing. The protein contained 0.11% of iron that corresponds to a minimum molecular size of 50,700. Determinations of molecular size by SDS-PAGE gave values of 48,000 +/- 1,000 while the one obtained by Sephadex gel filtration was 49,000. The pH optimum of the enzyme was 6.0. The activation energy was estimated to be 6 Kcal/mol. The prosthetic group was shown to be ferriprotoporphyrin IX. The presence of 13% neutral sugars was found. The spectrophotometric analysis showed the presence, in the visible region, of absorption maxima at 403, 490 and 633 nm. The Rz value (A403/A275) was 2.7.
Prenatal Diagnosis, 2014
Dipartimento di Sanità Pubblica e Medicina Clinica e Molecolare, Università degli Studi di Caglia... more Dipartimento di Sanità Pubblica e Medicina Clinica e Molecolare, Università degli Studi di Cagliari, Cagliari, Italy Struttura Complessa di Ostetricia e Ginecologia, Ospedale Microcitemico, Cagliari, Italy Servizio di Screening e Consulenza genetica, Ospedale Microcitemico, Cagliari, Italy *Correspondence to: Maria Cristina Rosatelli. E-mail: rosatelli@unica.it These authors equally contributed to the article.
Pharmacogenomics, 2010
Background: Pharmacogenetics is the study of genetic variations that cause alterations in drug le... more Background: Pharmacogenetics is the study of genetic variations that cause alterations in drug level, drug response and adverse drug reactions. SNPs found in CYP450 genes have the greatest genetic influences on interindividual variability in drug bioavailability. The polymorphic nature of these genes may modulate several enzyme levels that affect individual responses to pharmacological treatment. Among them, CYP3A4, CYP3A5, CYP2C9 and CYP2C19 isoforms of CYP450 enzymes are involved in the metabolism of many commonly prescribed drugs. Aims: In this study, we would like to develop a CYP450 genotyping platform that could lead a complete definition of a patient’s metabolic genotype in order to improve the clinical outcome of some drug treatments. Materials & methods: We used matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) (Sequenom®) to develop a SNP genotyping method. Results: This MALDI-TOF-based multiplexing system allows the simultaneous a...
Journal of Medical Genetics, 1997
This study reports the molecular characterisation of the bilirubin UDPglucuronosyl-transferase ge... more This study reports the molecular characterisation of the bilirubin UDPglucuronosyl-transferase gene (UGT1) in a group of patients of Sardinian descent with Crigler-Najjar syndrome type I and their relatives. Sequence analysis of both UGT1A exon 1 and common exons 2-5 was performed in all patients, leading to the detection of AF170 and a novel mutation (470insT), both residing in UGT1A exon 1. All but two heterozygotes for the AF170 mutation showed normal serum bilirubin levels. These two subjects were also heterozygous for the sequence variation A(TA)7TAA in the promoter region of the UGT1A gene.