Sidra Amin - Academia.edu (original) (raw)

Papers by Sidra Amin

Research paper thumbnail of Synthesis of Sheet Like Morphology of NiO for Sensitive and Selective Determination of Urea

Sensor Letters

An efficient and simple method has been demonstrated for the synthesis of nickel oxide nanostruct... more An efficient and simple method has been demonstrated for the synthesis of nickel oxide nanostructures using urea as a capping agent. The nanosheet-like morphology was confirmed by scanning electron microscopy, crystalline nature was studied by using the X-ray diffraction (XRD) and surface area of nanomaterial was investigated by automated sorption analyzer. Then synthesized NiO nanostructures were used to fabricate the surface of glassy carbon electrode (GCE). The electrocatalytic parameters of modified NiO/GCE electrode were investigated by using various techniques such as electrochemical impedance spectroscopy (EIS), square wave voltammetry (SWV), differential pulse voltammetry (DPV), normal pulse voltammetry (NPV) and cyclic voltammetry (CV) and chronoamperometry. Various working experimental conditions were optimized in order to attain the highest sensitivity for the determination of urea and the highest peak current 1032 A of response were obtained at 100 M concentration of urea. A linear calibration plot was obtained for peak current versus concentration of urea in the range of 10 M urea to 80 M urea with a good detection limit of 2 M. The proposed working strategy was successfully employed for the estimation of urea in human urine samples and the obtained results are found satisfactory. The newly functional urea sensor can be exploited at large scale as an alternative analytical device beside to the other reported urea sensors.

Research paper thumbnail of Recent Trends in Development of Nanomaterials Based Green Analytical Methods for Environmental Remediation

Current Analytical Chemistry

Background: In recent years, the occurrence and fate of environmental pollutants has been recogni... more Background: In recent years, the occurrence and fate of environmental pollutants has been recognized as one of the emerging issues in environmental chemistry. A survey documented about a wide variety of these pollutants, which are often detected in our environment and these are major cause of shortened life spans and the global warming. These pollutants include toxic metal, pesticides, fertilizers, drugs and dyes released into soil and major water bodies. The presence of these contaminants causes major disturbance in eco-system’s balance. To tackle these issues many technological improvements are made to detect minute contaminations. The latest issue being answered by the scientists is the use of green nano materials as sensors which are economical, instant and give much better results at low concentrations and can be used for the field measurements resulting in no dangerous by-product that could lead to more environmental contamination. Nano materials are known for their wide band ...

Research paper thumbnail of Functional Nickel Oxide Nanostructures for Ethanol Oxidation in Alkaline Media

Research paper thumbnail of A review on detection of heavy metals from aqueous media using nanomaterial-based sensors

Environmental Science and Pollution Research

Research paper thumbnail of Impact of Tariff on Income: Cross Country Analysis

Journal of Independent Studies and Research-Management, Social Sciences and Economics

The purpose of the study is to assess the significance of import tariff on the economic growth of... more The purpose of the study is to assess the significance of import tariff on the economic growth of ten countries divided into two groups; developing and developed economies. The developed countries included in the sample are

Research paper thumbnail of Focused Ion Beam Tomography

Ion Beam [Working Title]

To study the fundamental effect of shape and morphology of any material on its properties, it is ... more To study the fundamental effect of shape and morphology of any material on its properties, it is very essential to know and study its morphology. Focused ion beam (FIB) tomography is a 3D chemical and structural relationship studying technique. The instrumentation of FIB looks like that of the scanning electron microscopy (SEM), but there is a major difference in the beam used for scanning. For SEM, a beam of electrons is used with scanning medium whereas in FIB, a much focused beam of ions is used for scanning. FIB can be used for lithography and ablation purposes, but due to advancements and high-energy focused beam, it is nowadays being used as a tomographic technique. Tomography is defined as imaging by sectoring or cross-sectioning any desired area. The hyphenation of FIB with energydispersive spectrometry or secondary ion mass spectrometry can give us elemental analysis with very high-resolution 3D images for a sample. This technique contributes to acquaintance of qualitative and quantitative analyses, 3D volume creations, and image processing. In this chapter, we will discuss the advancements in FIB instrumentation and its use as 3D imaging tool for different samples ranging from nanometer (nm)-sized materials to micrometer (μm)-sized biological samples.

Research paper thumbnail of A sensitive enzyme-free lactic acid sensor based on NiO nanoparticle for practical applications

Analytical Methods

A facile and efficient electrochemical sensing platform has been successfully exploited for the f... more A facile and efficient electrochemical sensing platform has been successfully exploited for the first time for the determination of lactic acid using a nickel oxide (NiO) nanoparticle-modified glassy carbon electrode...

Research paper thumbnail of A practical non-enzymatic urea sensor based on NiCo2O4 nanoneedles

RSC Advances

We propose a new facile electrochemical sensing platform for determination of urea, based on a gl... more We propose a new facile electrochemical sensing platform for determination of urea, based on a glassy carbon electrode (GCE) modified with nickel cobalt oxide (NiCo2O4) nanoneedles.

Research paper thumbnail of Facile Non‐enzymatic Lactic Acid Sensor Based on Cobalt Oxide Nanostructures

Research paper thumbnail of Etiology of acute viral respiratory infections common in Pakistan: A review

Reviews in Medical Virology

Respiratory infections, especially those of the lower respiratory tract, remain a foremost cause ... more Respiratory infections, especially those of the lower respiratory tract, remain a foremost cause of mortality and morbidity of children greater than 5 years in developing countries including Pakistan. Ignoring these acute-level infections may lead to complications. Particularly in Pakistan, respiratory infections account for 20% to 30% of all deaths of children. Even though these infections are common, insufficiency of accessible data hinders development of a comprehensive summary of the problem. The purpose of this study was to determine the prevalence rate in various regions of Pakistan and also to recognize the existing viral strains responsible for viral respiratory infections through published data. Respiratory viruses are detected more frequently among rural dwellers in Pakistan. Lower tract infections are found to be more lethal. The associated pathogens comprise respiratory syncytial virus (RSV), human metapneumovirus (HMPV), coronavirus, enterovirus/rhinovirus, influenza virus, parainfluenza virus, adenovirus, and human bocavirus. RSV is more dominant and can be subtyped as RSV-A and RSV-B (BA-9, BA-10, and BA-13). Influenza A (H1N1, H5N1, H3N2, and H1N1pdm09) and Influenza B are common among the Pakistani population. Generally, these strains are detected in a seasonal pattern with a high incidence during spring and winter time. The data presented include pneumonia, bronchiolitis, and influenza. This paper aims to emphasise the need for standard methods to record the incidence and etiology of associated pathogens in order to provide effective treatment against viral infections of the respiratory tract and to reduce death rates.

Research paper thumbnail of Synthesis of Sheet Like Morphology of NiO for Sensitive and Selective Determination of Urea

Sensor Letters

An efficient and simple method has been demonstrated for the synthesis of nickel oxide nanostruct... more An efficient and simple method has been demonstrated for the synthesis of nickel oxide nanostructures using urea as a capping agent. The nanosheet-like morphology was confirmed by scanning electron microscopy, crystalline nature was studied by using the X-ray diffraction (XRD) and surface area of nanomaterial was investigated by automated sorption analyzer. Then synthesized NiO nanostructures were used to fabricate the surface of glassy carbon electrode (GCE). The electrocatalytic parameters of modified NiO/GCE electrode were investigated by using various techniques such as electrochemical impedance spectroscopy (EIS), square wave voltammetry (SWV), differential pulse voltammetry (DPV), normal pulse voltammetry (NPV) and cyclic voltammetry (CV) and chronoamperometry. Various working experimental conditions were optimized in order to attain the highest sensitivity for the determination of urea and the highest peak current 1032 A of response were obtained at 100 M concentration of urea. A linear calibration plot was obtained for peak current versus concentration of urea in the range of 10 M urea to 80 M urea with a good detection limit of 2 M. The proposed working strategy was successfully employed for the estimation of urea in human urine samples and the obtained results are found satisfactory. The newly functional urea sensor can be exploited at large scale as an alternative analytical device beside to the other reported urea sensors.

Research paper thumbnail of Recent Trends in Development of Nanomaterials Based Green Analytical Methods for Environmental Remediation

Current Analytical Chemistry

Background: In recent years, the occurrence and fate of environmental pollutants has been recogni... more Background: In recent years, the occurrence and fate of environmental pollutants has been recognized as one of the emerging issues in environmental chemistry. A survey documented about a wide variety of these pollutants, which are often detected in our environment and these are major cause of shortened life spans and the global warming. These pollutants include toxic metal, pesticides, fertilizers, drugs and dyes released into soil and major water bodies. The presence of these contaminants causes major disturbance in eco-system’s balance. To tackle these issues many technological improvements are made to detect minute contaminations. The latest issue being answered by the scientists is the use of green nano materials as sensors which are economical, instant and give much better results at low concentrations and can be used for the field measurements resulting in no dangerous by-product that could lead to more environmental contamination. Nano materials are known for their wide band ...

Research paper thumbnail of Functional Nickel Oxide Nanostructures for Ethanol Oxidation in Alkaline Media

Research paper thumbnail of A review on detection of heavy metals from aqueous media using nanomaterial-based sensors

Environmental Science and Pollution Research

Research paper thumbnail of Impact of Tariff on Income: Cross Country Analysis

Journal of Independent Studies and Research-Management, Social Sciences and Economics

The purpose of the study is to assess the significance of import tariff on the economic growth of... more The purpose of the study is to assess the significance of import tariff on the economic growth of ten countries divided into two groups; developing and developed economies. The developed countries included in the sample are

Research paper thumbnail of Focused Ion Beam Tomography

Ion Beam [Working Title]

To study the fundamental effect of shape and morphology of any material on its properties, it is ... more To study the fundamental effect of shape and morphology of any material on its properties, it is very essential to know and study its morphology. Focused ion beam (FIB) tomography is a 3D chemical and structural relationship studying technique. The instrumentation of FIB looks like that of the scanning electron microscopy (SEM), but there is a major difference in the beam used for scanning. For SEM, a beam of electrons is used with scanning medium whereas in FIB, a much focused beam of ions is used for scanning. FIB can be used for lithography and ablation purposes, but due to advancements and high-energy focused beam, it is nowadays being used as a tomographic technique. Tomography is defined as imaging by sectoring or cross-sectioning any desired area. The hyphenation of FIB with energydispersive spectrometry or secondary ion mass spectrometry can give us elemental analysis with very high-resolution 3D images for a sample. This technique contributes to acquaintance of qualitative and quantitative analyses, 3D volume creations, and image processing. In this chapter, we will discuss the advancements in FIB instrumentation and its use as 3D imaging tool for different samples ranging from nanometer (nm)-sized materials to micrometer (μm)-sized biological samples.

Research paper thumbnail of A sensitive enzyme-free lactic acid sensor based on NiO nanoparticle for practical applications

Analytical Methods

A facile and efficient electrochemical sensing platform has been successfully exploited for the f... more A facile and efficient electrochemical sensing platform has been successfully exploited for the first time for the determination of lactic acid using a nickel oxide (NiO) nanoparticle-modified glassy carbon electrode...

Research paper thumbnail of A practical non-enzymatic urea sensor based on NiCo2O4 nanoneedles

RSC Advances

We propose a new facile electrochemical sensing platform for determination of urea, based on a gl... more We propose a new facile electrochemical sensing platform for determination of urea, based on a glassy carbon electrode (GCE) modified with nickel cobalt oxide (NiCo2O4) nanoneedles.

Research paper thumbnail of Facile Non‐enzymatic Lactic Acid Sensor Based on Cobalt Oxide Nanostructures

Research paper thumbnail of Etiology of acute viral respiratory infections common in Pakistan: A review

Reviews in Medical Virology

Respiratory infections, especially those of the lower respiratory tract, remain a foremost cause ... more Respiratory infections, especially those of the lower respiratory tract, remain a foremost cause of mortality and morbidity of children greater than 5 years in developing countries including Pakistan. Ignoring these acute-level infections may lead to complications. Particularly in Pakistan, respiratory infections account for 20% to 30% of all deaths of children. Even though these infections are common, insufficiency of accessible data hinders development of a comprehensive summary of the problem. The purpose of this study was to determine the prevalence rate in various regions of Pakistan and also to recognize the existing viral strains responsible for viral respiratory infections through published data. Respiratory viruses are detected more frequently among rural dwellers in Pakistan. Lower tract infections are found to be more lethal. The associated pathogens comprise respiratory syncytial virus (RSV), human metapneumovirus (HMPV), coronavirus, enterovirus/rhinovirus, influenza virus, parainfluenza virus, adenovirus, and human bocavirus. RSV is more dominant and can be subtyped as RSV-A and RSV-B (BA-9, BA-10, and BA-13). Influenza A (H1N1, H5N1, H3N2, and H1N1pdm09) and Influenza B are common among the Pakistani population. Generally, these strains are detected in a seasonal pattern with a high incidence during spring and winter time. The data presented include pneumonia, bronchiolitis, and influenza. This paper aims to emphasise the need for standard methods to record the incidence and etiology of associated pathogens in order to provide effective treatment against viral infections of the respiratory tract and to reduce death rates.