Sukhveer singh - Academia.edu (original) (raw)

Sukhveer singh

Phone: 9266057705
Address: Delhi, Delhi, India

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Research paper thumbnail of Comparative study of structural and magnetic properties of nano-crystalline Li 0.5Fe 2.5O 4 prepared by various methods

Physica B-condensed Matter, 2009

Lithium ferrite has been considered as one of the highly strategic magnetic material. Nano-crysta... more Lithium ferrite has been considered as one of the highly strategic magnetic material. Nano-crystalline Li 0.5 Fe 2.5 O 4 was prepared by four different techniques and characterized by X-ray diffraction, vibrating sample magnetometer (VSM), transmission electron microscope (TEM) and Fourier transform infrareds (FTIR). The effect of annealing temperature (700, 900 and 1050 1C) on microstructure has been correlated to the magnetic properties. From X-ray diffraction patterns, it is confirmed that the pure phase of lithium ferrite began to form at 900 1C annealing. The particle size of as-prepared lithium ferrite was observed around 40, 31, 22 and 93 nm prepared by flash combustion, sol-gel, citrate precursor and standard ceramic technique, respectively. Lithium ferrite prepared by citrate precursor method shows a maximum saturation magnetization 67.6 emu/g at 5 KOe.

Research paper thumbnail of Comparative study of structural and magnetic properties of nano-crystalline Li 0.5Fe 2.5O 4 prepared by various methods

Physica B-condensed Matter, 2009

Lithium ferrite has been considered as one of the highly strategic magnetic material. Nano-crysta... more Lithium ferrite has been considered as one of the highly strategic magnetic material. Nano-crystalline Li 0.5 Fe 2.5 O 4 was prepared by four different techniques and characterized by X-ray diffraction, vibrating sample magnetometer (VSM), transmission electron microscope (TEM) and Fourier transform infrareds (FTIR). The effect of annealing temperature (700, 900 and 1050 1C) on microstructure has been correlated to the magnetic properties. From X-ray diffraction patterns, it is confirmed that the pure phase of lithium ferrite began to form at 900 1C annealing. The particle size of as-prepared lithium ferrite was observed around 40, 31, 22 and 93 nm prepared by flash combustion, sol-gel, citrate precursor and standard ceramic technique, respectively. Lithium ferrite prepared by citrate precursor method shows a maximum saturation magnetization 67.6 emu/g at 5 KOe.

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