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Papers by Wissem Aidi Wannes

Research paper thumbnail of Optimizing Ethanol Extraction of Rosemary Leaves and Their Biological Evaluations

Journal of exploratory research in pharmacology, Mar 11, 2022

Background and objectives: Rosemary (Rosmarinus officinalis L.) extract is widely used in food, c... more Background and objectives: Rosemary (Rosmarinus officinalis L.) extract is widely used in food, cosmetic and pharmaceutical industries. This study centered on the optimization of ethanolic extraction of rosemary leaves and evaluated the bioactivity of the extract. Methods: The optimized rosemary extract was analyzed using high-performance liquid chromatography. The antioxidant activity of the rosemary extract was measured using 2,2′-Azinobis-(3-ethylBenzoThiazoline-6-Sulfonic) acid, 2,2-DiPhenyl-1-Picryl-Hydrazyl-hydrate, and ferric reducing antioxidant power assays. The antibacterial activity of the rosemary extract was tested using the disk diffusion method. Toxicity was tested using mice. Nitrite production by RAW 264.7 cells was used to determine the anti-inflammatory activity of the rosemary extract. The construction and statistical analysis of the experimental design was done using NemrodW (LPRAI, version 2000) software. Results: We found that ethanol extraction of rosemary leaves depended on optimizing heating temperature and time. The maximum yields of carnosic and rosmarinic acids were obtained after optimizing these parameters according to the modelling software. The rosemary leaf extract had high antioxidant, anti-inflammatory, and antibacterial properties with low acute toxicity. Conclusions: Ethanol extraction of rosemary leaves could potentially be used in several industrial applications.

Research paper thumbnail of Le myrte (Myrtus communis L.)

Le myrte (Myrtus communis L.), arbrisseau perenne spontane de la famille des Myrtacees, est tres ... more Le myrte (Myrtus communis L.), arbrisseau perenne spontane de la famille des Myrtacees, est tres connu par ses nombreuses vertus medicinales, nutritionnelles et ses nombreuses utilisations culinaires ce qui intensifie sa demande par les industries agroalimentaire et pharmaceutique. L’existence de deux varietes de myrte (Myrtus communis italica L. et Myrtus communis baetica L.) dans la flore de la Tunisie nous a incite a realiser ce travail de recherche afin d'evaluer biochimiquement la richesse des differents organes de ces deux varietes en composes bioactifs tels que les huiles essentielles, les acides gras et les polyphenols et de determiner leur activite antioxydante.

Research paper thumbnail of Fatty Acid and Glycerolipid Changes During Tunisian Myrtle (Myrtus Communis Var. Italica) Fruit Ripening

Journal of Food Biochemistry, 2010

Research paper thumbnail of A review of Tunisian medicinal plants with anticancer activity

Journal of Complementary and Integrative Medicine

Cancer is a major public health problem in the world. The use of the medicinal plants in cancer p... more Cancer is a major public health problem in the world. The use of the medicinal plants in cancer prevention and management is frequent in Africa, especially in Tunisia, and it is transmitted from generation to generation within cultures. Many previous studies showed that a wide range of Tunisian medicinal plants exerted cytotoxic and anticancer activity. A comprehensive review was conducted to collect information from scientific journal articles, including indigenous knowledge researches, about Tunisian medicinal plants used for the prevention and management of cancer. The aim of this review article is to provide the reader with information concerning the importance of Tunisian medicinal plants in the prevention and management of cancer and to open the door for the health professionals and scientists working in the field of pharmacology and therapeutics to produce new drug formulations to treat different types of cancer.

Research paper thumbnail of On the effect of initial drying techniques on essential oil composition, phenolic compound and antioxidant properties of anise (Pimpinella anisum L.) seeds

The effect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms o... more The effect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of their essential oils, phenolics and antioxidant activities. The optimum yield of essential oil was found in shade drying (2.62%). Fourteen volatile compounds were determined in all samples with variation of the main component proportions depending on drying methods. Thus, trans-anethole (84.21%) and estragole (3.82%) proportions significantly increased in shade drying. The highest total phenol and flavonoid contents of aniseeds were recorded in shade drying (42.70 mg of GAE/g and 53.55 mg of QE/g, respectively) while the lowest contents in oven drying at 60 °C (31.15 mg of GAE/g and 46.20 mg of QE/g, respectively). In all drying methods, naringin (41.04–43.76%), chloroginic acid (23.13–27.19%) and rosmarinic acid (12.26–15.95%) were the predominant phenol compounds. Although shade drying increased the antioxidant activity, aniseed extracts exhibited higher radical scavenging (IC50 = 10...

Research paper thumbnail of Biochemical characterization of fennel (Ferula communis L.) different parts through their essential oils, fatty acids and phenolics

The intention of this study was to compare the different parts of Tunisian Ferula communis via th... more The intention of this study was to compare the different parts of Tunisian Ferula communis via their fatty acids, essential oils and phenolic compounds. Results showed that the lipid fraction of fruits and leaves was characterized by the predominance of oleic acid. Erucic and linoleic acids were the most abundant in stems while linoleic and palmitic acids in flowers. F. communis essential oils were defined by four chemotypes, namely isoshyobunone/6-tert-butyl-4-methylcoumarin in stems; α-eudesmol/caryophyllene oxide in leaves; caryophyllene/myrcene in flowers and α-gurjunene/hexadecanoic acid in fruits. So, oxygenated sesquiterpenes and sesquiterpene hydrocarbons represented the major classes of stem essential oil. Monoterpene hydrocarbons were the predominant classes of leaves and flowers. Fruit essential oil was predominated by sesquiterpene hydrocarbons. Resorcinol and ferulic acid were the main phenolic compounds in flowers but chlorogenic and ferulic acides in leaves. Stems wer...

Research paper thumbnail of Antioxidant Activity of Opuntia spp.: A Review

Opuntia spp.: Chemistry, Bioactivity and Industrial Applications

Research paper thumbnail of Phytochemical composition and health properties of Lycium europaeum L.: A review

Research paper thumbnail of Can medicinal plants contribute to the cure of Tunisian COVID-19 patients?

Journal of Medicinal Plants Studies

Research paper thumbnail of Effect of Environmental Conditions on the Chemical Composition and Antioxidant Activity of Essential Oils from Rosmarinus officinalis L. Growing Wild in Tunisia

Journal of Essential Oil Bearing Plants

Research paper thumbnail of Antidiabetic, antihyperlipidemic and antioxidant influences of the spice cinnamon ( Cinnamomum zeylanicumon ) in experimental rats

Brazilian Journal of Pharmaceutical Sciences

The present study investigates the effect of cinnamon (Cinnamomum zeylanicumon) powder supplement... more The present study investigates the effect of cinnamon (Cinnamomum zeylanicumon) powder supplementation on glucose levels, lipid profiles, and oxidative stress parameters in alloxan-induced diabetic rats. Diabetes was induced in adult male Wistar rats via a single subcutaneous alloxan injection (15 mg/kg). Cinnamon powder was mixed with the standard feed of the rats in an amount of 5% for 28 consecutive days. Serum concentrations of total cholesterol (TC) and triglycerides (TG) were assayed at the end of the experimental period in all investigated groups. Anti-oxidative enzymes such as glutathione peroxidase (GPx), catalase (CAT) and superoxide dismutase (SOD) were sought in the serum and pancreas. Alloxan caused the fasting blood sugar level to increase. The administration of cinnamon blocked the increase of blood glucose. There was also a significant difference in the TG and TC levels between control and treated diabetic rats. In diabetic rats, cinnamon treatment restored the activities of SOD, CAT and GPx. These findings suggested that cinnamon has an anti-hyperglycemic effect, improves lipid profiles, and protect against damage induced by oxidative stress in the diabetic state.

Research paper thumbnail of Does Lycium europaeum leaf have antihyperglycemic, antihyperlipidemic and antioxidant effects

Brazilian Journal of Pharmaceutical Sciences

The purpose of the present investigation is to assess, for the first time, the antidiabetic, anti... more The purpose of the present investigation is to assess, for the first time, the antidiabetic, antihyperlipidemic and antioxidant activities of Lycium europaeum extract in alloxan-induced diabetic rats. Diabetes was induced in adult male Wistar rats via a single subcutaneous alloxan injection (120 mg/kg). Lycium europaeum aqueous extract was orally administered at a dose of 20 mg/kg for 28 consecutive days. Serum concentrations of total cholesterol (TC), low-density lipoprotein cholesterol (LDL-C), high-density lipoprotein cholesterol (HDL-C) and triglycerides (TG) were assayed at the end of the experimental period in all investigated groups. Antioxidant enzymes such as glutathione peroxidase (GPx), catalase (CAT) and superoxide dismutase (SOD) were sought in the serum and pancreas. Lycium europaeum extract significantly increased HDL-C and reduced blood glucose, TC, LDL-C and TG as compared to the alloxan-control group. Lycium europaeum extract was also efficient in reducing oxidative stress in diabetic rats by increasing SOD, CAT and GPx activities both in the pancreas and the plasma of the animals. Moreover, Lycium europaeum extract contained considerable levels of polyphenols and flavonoids. It also exhibited an important antioxidant capacity and a remarkable ability to quench DPPH radicals and reduce irons. The obtained results highlight potentially relevant health beneficial effects of Lycium europaeum extract, reversing hyperglycemic, hyperlipidemic and oxidative stress effects in rats with alloxan-induced diabetes. Therefore, it may be considered as a promising alternative or complementary agent to diabetes treatment.

Research paper thumbnail of On the effect of initial drying techniques on essential oil composition, phenolic compound and antioxidant properties of anise (Pimpinella anisum L.) seeds

Journal of Food Measurement and Characterization

The efect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of... more The efect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of their essential oils, phenolics and antioxidant activities. The optimum yield of essential oil was found in shade drying (2.62%). Fourteen volatile compounds were determined in all samples with variation of the main component proportions depending on drying methods. Thus, trans-anethole (84.21%) and estragole (3.82%) proportions signiicantly increased in shade drying. The highest total phenol and lavonoid contents of aniseeds were recorded in shade drying (42.70 mg of GAE/g and 53.55 mg of QE/g, respectively) while the lowest contents in oven drying at 60 °C (31.15 mg of GAE/g and 46.20 mg of QE/g, respectively). In all drying methods, naringin (41.04-43.76%), chloroginic acid (23.13-27.19%) and rosmarinic acid (12.26-15.95%) were the predominant phenol compounds. Although shade drying increased the antioxidant activity, aniseed extracts exhibited higher radical scavenging (IC 50 = 10.15 µg/mL), reducing power (EC 50 = 187.24 µg/mL) and chelating (IC 50 = 6.85 mg/mL) capacities than essential oils (IC 50 = 114.87 µg/mL, EC 50 = 548.05 µg/mL and IC 50 = 58.65 mg/mL, respectively). In conclusion, Shade drying method was found to enhance essential oils, phenols and antioxidant activities in aniseeds.

Research paper thumbnail of Screening for amyloid-β aggregation inhibitor and neuronal toxicity of eight Tunisian medicinal plants

Industrial Crops and Products

Research paper thumbnail of Green Extraction of Fennel and Anise Edible Oils Using Bio-Based Solvent and Supercritical Fluid: Assessment of Chemical Composition, Antioxidant Property, and Oxidative Stability

Food and Bioprocess Technology

Research paper thumbnail of Does unsaponifiable fraction of grape seed oil attenuate nitric oxide production, oxidant and cytotoxicity activities

Journal of Food Biochemistry

Research paper thumbnail of Effect of bioclimatic area and season on phenolics and antioxidant activities of rosemary (Rosmarinus officinalis L.) leaves

Journal of Essential Oil Research

Research paper thumbnail of Does Curcuma longa root powder have an effect against CCl4-induced hepatotoxicity in rats: a protective and curative approach

Food Science and Biotechnology

Research paper thumbnail of Bioactive compounds and antioxidant activity of Pimpinella anisum L. accessions at different ripening stages

Research paper thumbnail of Antioxidant and hepatoprotective effects of Asparagus albus leaves in carbon tetrachloride-induced liver injury rats

Journal of Food Biochemistry

Research paper thumbnail of Optimizing Ethanol Extraction of Rosemary Leaves and Their Biological Evaluations

Journal of exploratory research in pharmacology, Mar 11, 2022

Background and objectives: Rosemary (Rosmarinus officinalis L.) extract is widely used in food, c... more Background and objectives: Rosemary (Rosmarinus officinalis L.) extract is widely used in food, cosmetic and pharmaceutical industries. This study centered on the optimization of ethanolic extraction of rosemary leaves and evaluated the bioactivity of the extract. Methods: The optimized rosemary extract was analyzed using high-performance liquid chromatography. The antioxidant activity of the rosemary extract was measured using 2,2′-Azinobis-(3-ethylBenzoThiazoline-6-Sulfonic) acid, 2,2-DiPhenyl-1-Picryl-Hydrazyl-hydrate, and ferric reducing antioxidant power assays. The antibacterial activity of the rosemary extract was tested using the disk diffusion method. Toxicity was tested using mice. Nitrite production by RAW 264.7 cells was used to determine the anti-inflammatory activity of the rosemary extract. The construction and statistical analysis of the experimental design was done using NemrodW (LPRAI, version 2000) software. Results: We found that ethanol extraction of rosemary leaves depended on optimizing heating temperature and time. The maximum yields of carnosic and rosmarinic acids were obtained after optimizing these parameters according to the modelling software. The rosemary leaf extract had high antioxidant, anti-inflammatory, and antibacterial properties with low acute toxicity. Conclusions: Ethanol extraction of rosemary leaves could potentially be used in several industrial applications.

Research paper thumbnail of Le myrte (Myrtus communis L.)

Le myrte (Myrtus communis L.), arbrisseau perenne spontane de la famille des Myrtacees, est tres ... more Le myrte (Myrtus communis L.), arbrisseau perenne spontane de la famille des Myrtacees, est tres connu par ses nombreuses vertus medicinales, nutritionnelles et ses nombreuses utilisations culinaires ce qui intensifie sa demande par les industries agroalimentaire et pharmaceutique. L’existence de deux varietes de myrte (Myrtus communis italica L. et Myrtus communis baetica L.) dans la flore de la Tunisie nous a incite a realiser ce travail de recherche afin d'evaluer biochimiquement la richesse des differents organes de ces deux varietes en composes bioactifs tels que les huiles essentielles, les acides gras et les polyphenols et de determiner leur activite antioxydante.

Research paper thumbnail of Fatty Acid and Glycerolipid Changes During Tunisian Myrtle (Myrtus Communis Var. Italica) Fruit Ripening

Journal of Food Biochemistry, 2010

Research paper thumbnail of A review of Tunisian medicinal plants with anticancer activity

Journal of Complementary and Integrative Medicine

Cancer is a major public health problem in the world. The use of the medicinal plants in cancer p... more Cancer is a major public health problem in the world. The use of the medicinal plants in cancer prevention and management is frequent in Africa, especially in Tunisia, and it is transmitted from generation to generation within cultures. Many previous studies showed that a wide range of Tunisian medicinal plants exerted cytotoxic and anticancer activity. A comprehensive review was conducted to collect information from scientific journal articles, including indigenous knowledge researches, about Tunisian medicinal plants used for the prevention and management of cancer. The aim of this review article is to provide the reader with information concerning the importance of Tunisian medicinal plants in the prevention and management of cancer and to open the door for the health professionals and scientists working in the field of pharmacology and therapeutics to produce new drug formulations to treat different types of cancer.

Research paper thumbnail of On the effect of initial drying techniques on essential oil composition, phenolic compound and antioxidant properties of anise (Pimpinella anisum L.) seeds

The effect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms o... more The effect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of their essential oils, phenolics and antioxidant activities. The optimum yield of essential oil was found in shade drying (2.62%). Fourteen volatile compounds were determined in all samples with variation of the main component proportions depending on drying methods. Thus, trans-anethole (84.21%) and estragole (3.82%) proportions significantly increased in shade drying. The highest total phenol and flavonoid contents of aniseeds were recorded in shade drying (42.70 mg of GAE/g and 53.55 mg of QE/g, respectively) while the lowest contents in oven drying at 60 °C (31.15 mg of GAE/g and 46.20 mg of QE/g, respectively). In all drying methods, naringin (41.04–43.76%), chloroginic acid (23.13–27.19%) and rosmarinic acid (12.26–15.95%) were the predominant phenol compounds. Although shade drying increased the antioxidant activity, aniseed extracts exhibited higher radical scavenging (IC50 = 10...

Research paper thumbnail of Biochemical characterization of fennel (Ferula communis L.) different parts through their essential oils, fatty acids and phenolics

The intention of this study was to compare the different parts of Tunisian Ferula communis via th... more The intention of this study was to compare the different parts of Tunisian Ferula communis via their fatty acids, essential oils and phenolic compounds. Results showed that the lipid fraction of fruits and leaves was characterized by the predominance of oleic acid. Erucic and linoleic acids were the most abundant in stems while linoleic and palmitic acids in flowers. F. communis essential oils were defined by four chemotypes, namely isoshyobunone/6-tert-butyl-4-methylcoumarin in stems; α-eudesmol/caryophyllene oxide in leaves; caryophyllene/myrcene in flowers and α-gurjunene/hexadecanoic acid in fruits. So, oxygenated sesquiterpenes and sesquiterpene hydrocarbons represented the major classes of stem essential oil. Monoterpene hydrocarbons were the predominant classes of leaves and flowers. Fruit essential oil was predominated by sesquiterpene hydrocarbons. Resorcinol and ferulic acid were the main phenolic compounds in flowers but chlorogenic and ferulic acides in leaves. Stems wer...

Research paper thumbnail of Antioxidant Activity of Opuntia spp.: A Review

Opuntia spp.: Chemistry, Bioactivity and Industrial Applications

Research paper thumbnail of Phytochemical composition and health properties of Lycium europaeum L.: A review

Research paper thumbnail of Can medicinal plants contribute to the cure of Tunisian COVID-19 patients?

Journal of Medicinal Plants Studies

Research paper thumbnail of Effect of Environmental Conditions on the Chemical Composition and Antioxidant Activity of Essential Oils from Rosmarinus officinalis L. Growing Wild in Tunisia

Journal of Essential Oil Bearing Plants

Research paper thumbnail of Antidiabetic, antihyperlipidemic and antioxidant influences of the spice cinnamon ( Cinnamomum zeylanicumon ) in experimental rats

Brazilian Journal of Pharmaceutical Sciences

The present study investigates the effect of cinnamon (Cinnamomum zeylanicumon) powder supplement... more The present study investigates the effect of cinnamon (Cinnamomum zeylanicumon) powder supplementation on glucose levels, lipid profiles, and oxidative stress parameters in alloxan-induced diabetic rats. Diabetes was induced in adult male Wistar rats via a single subcutaneous alloxan injection (15 mg/kg). Cinnamon powder was mixed with the standard feed of the rats in an amount of 5% for 28 consecutive days. Serum concentrations of total cholesterol (TC) and triglycerides (TG) were assayed at the end of the experimental period in all investigated groups. Anti-oxidative enzymes such as glutathione peroxidase (GPx), catalase (CAT) and superoxide dismutase (SOD) were sought in the serum and pancreas. Alloxan caused the fasting blood sugar level to increase. The administration of cinnamon blocked the increase of blood glucose. There was also a significant difference in the TG and TC levels between control and treated diabetic rats. In diabetic rats, cinnamon treatment restored the activities of SOD, CAT and GPx. These findings suggested that cinnamon has an anti-hyperglycemic effect, improves lipid profiles, and protect against damage induced by oxidative stress in the diabetic state.

Research paper thumbnail of Does Lycium europaeum leaf have antihyperglycemic, antihyperlipidemic and antioxidant effects

Brazilian Journal of Pharmaceutical Sciences

The purpose of the present investigation is to assess, for the first time, the antidiabetic, anti... more The purpose of the present investigation is to assess, for the first time, the antidiabetic, antihyperlipidemic and antioxidant activities of Lycium europaeum extract in alloxan-induced diabetic rats. Diabetes was induced in adult male Wistar rats via a single subcutaneous alloxan injection (120 mg/kg). Lycium europaeum aqueous extract was orally administered at a dose of 20 mg/kg for 28 consecutive days. Serum concentrations of total cholesterol (TC), low-density lipoprotein cholesterol (LDL-C), high-density lipoprotein cholesterol (HDL-C) and triglycerides (TG) were assayed at the end of the experimental period in all investigated groups. Antioxidant enzymes such as glutathione peroxidase (GPx), catalase (CAT) and superoxide dismutase (SOD) were sought in the serum and pancreas. Lycium europaeum extract significantly increased HDL-C and reduced blood glucose, TC, LDL-C and TG as compared to the alloxan-control group. Lycium europaeum extract was also efficient in reducing oxidative stress in diabetic rats by increasing SOD, CAT and GPx activities both in the pancreas and the plasma of the animals. Moreover, Lycium europaeum extract contained considerable levels of polyphenols and flavonoids. It also exhibited an important antioxidant capacity and a remarkable ability to quench DPPH radicals and reduce irons. The obtained results highlight potentially relevant health beneficial effects of Lycium europaeum extract, reversing hyperglycemic, hyperlipidemic and oxidative stress effects in rats with alloxan-induced diabetes. Therefore, it may be considered as a promising alternative or complementary agent to diabetes treatment.

Research paper thumbnail of On the effect of initial drying techniques on essential oil composition, phenolic compound and antioxidant properties of anise (Pimpinella anisum L.) seeds

Journal of Food Measurement and Characterization

The efect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of... more The efect of drying methods (sun, oven and shade drying) on aniseeds was investigated in terms of their essential oils, phenolics and antioxidant activities. The optimum yield of essential oil was found in shade drying (2.62%). Fourteen volatile compounds were determined in all samples with variation of the main component proportions depending on drying methods. Thus, trans-anethole (84.21%) and estragole (3.82%) proportions signiicantly increased in shade drying. The highest total phenol and lavonoid contents of aniseeds were recorded in shade drying (42.70 mg of GAE/g and 53.55 mg of QE/g, respectively) while the lowest contents in oven drying at 60 °C (31.15 mg of GAE/g and 46.20 mg of QE/g, respectively). In all drying methods, naringin (41.04-43.76%), chloroginic acid (23.13-27.19%) and rosmarinic acid (12.26-15.95%) were the predominant phenol compounds. Although shade drying increased the antioxidant activity, aniseed extracts exhibited higher radical scavenging (IC 50 = 10.15 µg/mL), reducing power (EC 50 = 187.24 µg/mL) and chelating (IC 50 = 6.85 mg/mL) capacities than essential oils (IC 50 = 114.87 µg/mL, EC 50 = 548.05 µg/mL and IC 50 = 58.65 mg/mL, respectively). In conclusion, Shade drying method was found to enhance essential oils, phenols and antioxidant activities in aniseeds.

Research paper thumbnail of Screening for amyloid-β aggregation inhibitor and neuronal toxicity of eight Tunisian medicinal plants

Industrial Crops and Products

Research paper thumbnail of Green Extraction of Fennel and Anise Edible Oils Using Bio-Based Solvent and Supercritical Fluid: Assessment of Chemical Composition, Antioxidant Property, and Oxidative Stability

Food and Bioprocess Technology

Research paper thumbnail of Does unsaponifiable fraction of grape seed oil attenuate nitric oxide production, oxidant and cytotoxicity activities

Journal of Food Biochemistry

Research paper thumbnail of Effect of bioclimatic area and season on phenolics and antioxidant activities of rosemary (Rosmarinus officinalis L.) leaves

Journal of Essential Oil Research

Research paper thumbnail of Does Curcuma longa root powder have an effect against CCl4-induced hepatotoxicity in rats: a protective and curative approach

Food Science and Biotechnology

Research paper thumbnail of Bioactive compounds and antioxidant activity of Pimpinella anisum L. accessions at different ripening stages

Research paper thumbnail of Antioxidant and hepatoprotective effects of Asparagus albus leaves in carbon tetrachloride-induced liver injury rats

Journal of Food Biochemistry