Lyn-marie Birkholtz | University of Pretoria (original) (raw)

Papers by Lyn-marie Birkholtz

Research paper thumbnail of Integration and mining of malaria molecular, functional and pharmacological data: how far are we from a chemogenomic knowledge space

Malaria Journal, 2006

The organization and mining of malaria genomic and post-genomic data is important to significantl... more The organization and mining of malaria genomic and post-genomic data is important to significantly increase the knowledge of the biology of its causative agents, and is motivated, on a longer term, by the necessity to predict and characterize new biological targets and new drugs. Biological targets are sought in a biological space designed from the genomic data from Plasmodium falciparum, but using also the millions of genomic data from other species. Drug candidates are sought in a chemical space containing the millions of small molecules stored in public and private chemolibraries. Data management should, therefore, be as reliable and versatile as possible. In this context, five aspects of the organization and mining of malaria genomic and post-genomic data were examined: 1) the comparison of protein sequences including compositionally atypical malaria sequences, 2) the high throughput reconstruction of molecular phylogenies, 3) the representation of biological processes, particularly metabolic pathways, 4) the versatile methods to integrate genomic data, biological representations and functional profiling obtained from X-omic experiments after drug treatments and 5) the determination and prediction of protein structures and their molecular docking with drug candidate structures. Recent progress towards a grid-enabled chemogenomic knowledge space is discussed.

Research paper thumbnail of Drug-resistant and mixed species malaria infections in Mpumalanga, South Africa

South African Journal of Science

Research paper thumbnail of Birkholtz L, Williams M, Reeksting S, Wells G, Roux S, Walter RD and AI Louw. (2008) A unique bifunctional enzyme complex controlling polyamine biosynthesis in Plasmodium falciparum is regulated by parasite-specific inserts. Int. J. Parasitol., 38

Research paper thumbnail of Van Brummelen AC, Llinas M, Louw AI and Birkholtz L. (2008) Co-inhibition of S-adenosylmethionine decarboxylase / ornithine decarboxylase of Plasmodium falciparum reveal compensatory mechanisms in the transcriptome. Int. J. Parasitol., 38

Polyamines are ubiquitous components of all living cells, and their depletion usually causes cyto... more Polyamines are ubiquitous components of all living cells, and their depletion usually causes cytostasis, a strategy employed for treatment of West African trypanosomiasis. To evaluate polyamine depletion as an anti-malarial strategy, cytostasis caused by the co-inhibition of S-adenosylmethionine decarboxylase/ ornithine decarboxylase in Plasmodium falciparum was studied with a comprehensive transcriptome, proteome, and metabolome investigation. Highly synchronized cultures were sampled just before and during cytostasis, and a novel zero time point definition was used to enable interpretation of results in lieu of the developmentally regulated control of gene expression in P. falciparum. Transcriptome analysis revealed the occurrence of a generalized transcriptional arrest just prior to the growth arrest due to polyamine depletion. However, the abundance of 538 transcripts was differentially affected and included three perturbation-specific compensatory transcriptional responses as follows: the increased abundance of the transcripts for lysine decarboxylase and ornithine aminotransferase and the decreased abundance of that for S-adenosylmethionine synthetase. Moreover, the latter two compensatory mechanisms were confirmed on both protein and metabolite levels confirming their biological relevance. In contrast with previous reports, the results provide evidence that P. falciparum responds to alleviate the detrimental effects of polyamine depletion via regulation of its transcriptome and subsequently the proteome and metabolome.

Research paper thumbnail of Morphological and Molecular Descriptors of the Developmental Cycle of Babesia divergens Parasites in Human Erythrocytes

PLOS Neglected Tropical Diseases, 2015

Human babesiosis, especially caused by the cattle derived Babesia divergens parasite, is on the i... more Human babesiosis, especially caused by the cattle derived Babesia divergens parasite, is on the increase, resulting in renewed attentiveness to this potentially life threatening emerging zoonotic disease. The molecular mechanisms underlying the pathophysiology and intra-erythrocytic development of these parasites are poorly understood. This impedes concerted efforts aimed at the discovery of novel anti-babesiacidal agents. By applying sensitive cell biological and molecular functional genomics tools, we describe the intra-erythrocytic development cycle of B. divergens parasites from immature, mono-nucleated ring forms to bi-nucleated paired piriforms and ultimately multi-nucleated tetrads that characterizes zoonotic Babesia spp. This is further correlated for the first time to nuclear content increases during intra-erythrocytic development progression, providing insight into the part of the life cycle that occurs during human infection. High-content temporal evaluation elucidated the contribution of the different stages to life cycle progression. Moreover, molecular descriptors indicate that B. divergens parasites employ physiological adaptation to in vitro cultivation. Additionally, differential expression is observed as the parasite equilibrates its developmental stages during its life cycle. Together, this information provides the first temporal evaluation of the functional transcriptome of B. divergens parasites, information that could be useful in identifying biological processes essential to parasite survival for future anti-babesiacidal discoveries.

Research paper thumbnail of A 2-methoxyestradiol bis-sulphamoylated derivative induces apoptosis in breast cell lines

Cell & Bioscience, 2015

Introduction: Research involving antimitotic compounds identified 2-methoxyestradiol (2ME2), as a... more Introduction: Research involving antimitotic compounds identified 2-methoxyestradiol (2ME2), as a promising anticancer endogenous metabolite. Owing to its low bioavailability, several in silico-designed 2ME2 analogues were synthesized. Structure-activity relationship studies indicated that an already existing 17-β-estradiol analogue, namely (8R,13S,14S,17S)-2-ethyl- 13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthrane-3,17-diyl bis(sulphamate) (EMBS) to exert potential in vitro anticancer activity. Methods: This study investigated the in vitro apoptotic influence of EMBS in an estrogen receptor-positive breast adenocarcinoma epithelial cell line (MCF-7); an estrogen receptor-negative breast epithelial cell line (MDA-MB-231) and a non-tumorigenic breast cell line (MCF-12A). Cell cycle progression, a phosphatidylserine flip, caspase 6-, 7-and 8 enzyme activity levels, Bcl-2 phosphorylation status at serine 70 and Bcl-2-and p53 protein levels were investigated to identify a possible action mechanism for apoptotic induction. Results: The xCELLigence real-time label-independent approach revealed that EMBS exerted antiproliferative activity in all three cell lines after 24 h of exposure. A G 2 M block was observed and apoptosis induction was verified by means of flow cytometry using propidium iodide and Annexin V-FITC respectively. EMBS-treated cells demonstrated a reduced mitochondrial membrane potential. EMBS exposure resulted in a statistically significant increase in p53 protein expression, decreased Bcl-2 protein expression and a decrease in pBcl-2(s70) phosphorylation status in all three cell lines. Results support the notion that EMBS induces apoptosis in all three cell lines. Conclusion: This study includes investigation into the apoptotic hallmarks exerted by EMBS after exposure of three cell lines namely MCF-7-, MDA-MDA-231-and MCF-12A cells. Increased caspase 6-, caspase 7-and caspase 8 activities, upregulation of p53 protein expression and a decrease in phosphorylation status of Bcl-2 at serine 70 in tumorigenic and non-tumorigenic lines were demonstrated.

Research paper thumbnail of The prevalence of mixed-species and antifolate-resistant malaria infections in Mpumalanga

South African medical journal = Suid-Afrikaanse tydskrif vir geneeskunde, 1998

To the Editor: A study was undertaken to establish the prevalence of mixed-species malaria infect... more To the Editor: A study was undertaken to establish the prevalence of mixed-species malaria infections and of antifolate-resistant parasites in the Mpumalanga province of South Africa. Blood samples from 56 infected patients were subjected to PCR amplification of the small-subunit ribosomal RNA genes for species identification. The PCRamplified gene of the antifolate target enzyme, dihydrofolate reductase (DHFR) in single Plasmodium falciparum-infected samples were subjected to restriction enzyme analysis to identify point mutations, which are known to confer resistance to pyrimethamine and proguanil.'

Research paper thumbnail of Synthesis and in vitro biological evaluation of dihydroartemisinyl-chalcone esters

European journal of medicinal chemistry, Jan 27, 2015

A series of dihydroartemisinyl-chalcone esters were synthesized through esterification of chalcon... more A series of dihydroartemisinyl-chalcone esters were synthesized through esterification of chalcones with dihydroartemisinin (DHA). The hybrids were screened against chloroquine (CQ) sensitive (3D7) and CQ resistant (W2) strains of intraerythrocytic Plasmodium falciparum parasites, and were all found to be active, with IC50 values ranging between 1.5 and 11 nM against both strains, with SI values over 5800. The esters featuring oxygenated aryl rings (7, 10 and 11), were found to be equipotent to DHA, but were 2-3 times more active than artesunate against the 3D7 and W2 strains of the malaria parasites. They were also screened in vitro against a panel of three cancer cell lines consisting of TK-10, UACC-62 and MCF-7. Compound 7, bearing a furan ring, displayed the most potent overall antitumor activity against all three cancer cell lines. TGA revealed that the targeted hybrids were all thermally more stable than DHA, which may be beneficial to the high temperature storage conditions t...

Research paper thumbnail of 2. Morris, E.J., Ngcete, Z., Birkholtz, L-M. and Louw, A.I. (2010) New Drugs to Fight Malaria. In Biovision 2008. From promises to practice: applications of science and technology in food, healthcare, energy and environment. Ed Ismail Serageldin, Ehsan Masood, with Mohamed El-Faham and Marwa El-W...

2. Morris, E.J., Ngcete, Z., Birkholtz, L-M. and Louw, A.I. (2010) New Drugs to Fight Malaria. In Biovision 2008. From promises to practice: applications of science and technology in food, healthcare, energy and environment. Ed Ismail Serageldin, Ehsan Masood, with Mohamed El-Faham and Marwa El-W...

Research paper thumbnail of Visagie MH, Stander BA, Birkholtz L-M, Joubert AM. Effects of a 17-beta estradiol analogue on gene expression and morphology in a breast epithelial adenocarcinoma cell line: A potential antiproliferative agent. Biomedical Research 2013; 24 (4): 525-530

Biomedical Research

that the estradiol analogue acts as an antimitotic agent in this highly metastatic breast cell li... more that the estradiol analogue acts as an antimitotic agent in this highly metastatic breast cell line. Data also showed that the newly designed estrogen analogue exerts an antiproliferative effect in this cancer cell line culminating in both apoptosis and autophagy as type of cell death paving the way for further investigations into its potential as anticancer agent.

Research paper thumbnail of Polyamine uptake in the malaria parasite, Plasmodium falciparum, is dependent on the parasite's membrane potential

Research paper thumbnail of Antimalarial drug discovery: in silico structural biology and rational drug design

Malaria remains one of the most burdensome human infectious diseases, with a high rate of resista... more Malaria remains one of the most burdensome human infectious diseases, with a high rate of resistance outbreaks and a constant need for the discovery of novel antimalarials and drug targets. For several reasons, Plasmodial proteins are difficult to characterise structurally using traditional physical approaches. However, these problems can be partially overcome using a number of in silico approaches. This review describes the peculiarities of malaria proteins and then details various in silico strategies to select and allow descriptions of the molecular structures of drug target candidates as well as subsequent rational approaches for drug design. Chiefly, homology modelling with specific focus on unique aspects of malaria proteins including low homology, large protein size and the presence of parasite-specific inserts is addressed and alternative strategies including multiple sequence and structure-based prediction methods, samplingbased approaches that aim to reveal likely global or shared features of a Plasmodial structure and the value of molecular dynamics understanding of unique features of Plasmodial proteins are discussed. Once a detailed description of the drug target is available, in silico approaches to the specific design of an inhibitory drug thereof becomes invaluable as an economic and rational alternative to chemical library screening.

Research paper thumbnail of Comparative properties of a three-dimensional model of Plasmodium falciparum ornithine decarboxylase

Proteins, 2003

The ornithine decarboxylase (ODC) component of the bifunctional S-adenosylmethionine decarboxylas... more The ornithine decarboxylase (ODC) component of the bifunctional S-adenosylmethionine decarboxylase/ornithine decarboxylase enzyme (PfAdoMetDC-ODC) of Plasmodium falciparum was modeled on the crystal structure of the Trypanosoma brucei enzyme. The homology model predicts a doughnut-shaped active homodimer that associates in a head-to-tail manner. The monomers contain two distinct domains, an N-terminal ␣/␤barrel and a C-terminal modified Greek-key domain. These domains are structurally conserved between eukaryotic ODC enzymes and are preserved in distant analogs such as alanine racemase and triosephosphate isomerase-like proteins. Superimposition of the PfODC model on the crystal structure of the human enzyme indicates a significant degree of deviation in the carbon ␣-backbone of the solvent accessible loops. The surface locality of the ab initio modeled 38 amino acid parasite-specific insert suggests a role in the stabilization of the large bifunctional protein complex. The active site pockets of PfODC at the interface between the monomers appear to be conserved regarding the binding sites of the cofactor and substrate, but each contains five additional malaria-specific residues. The predicted PfODC homology model is consistent with mutagenesis results and biochemical studies concerning the active site residues and areas involved in stabilizing the dimeric form of the protein. Two competitive inhibitors of PfODC could be shown to interact with several parasite-specific residues in comparison with their interaction with the human ODC. The PfODC homology model contributes toward a structurebased approach for the design of novel malariaspecific inhibitors. Proteins 2003;50:464 -473.

Research paper thumbnail of Integration and mining of malaria molecular, functional and pharmacological data: how far are we from a chemogenomic knowledge space?

Malar J, 2006

The organization and mining of malaria genomic and post-genomic data is important to significantl... more The organization and mining of malaria genomic and post-genomic data is important to significantly increase the knowledge of the biology of its causative agents, and is motivated, on a longer term, by the necessity to predict and characterize new biological targets and new drugs. Biological targets are sought in a biological space designed from the genomic data from Plasmodium falciparum, but using also the millions of genomic data from other species. Drug candidates are sought in a chemical space containing the millions of small molecules stored in public and private chemolibraries. Data management should, therefore, be as reliable and versatile as possible. In this context, five aspects of the organization and mining of malaria genomic and post-genomic data were examined: 1) the comparison of protein sequences including compositionally atypical malaria sequences, 2) the high throughput reconstruction of molecular phylogenies, 3) the representation of biological processes, particularly metabolic pathways, 4) the versatile methods to integrate genomic data, biological representations and functional profiling obtained from Xomic experiments after drug treatments and 5) the determination and prediction of protein structures and their molecular docking with drug candidate structures. Recent progress towards a grid-enabled chemogenomic knowledge space is discussed.

Research paper thumbnail of In silico discovery of Chemotherapeutic agents

Research paper thumbnail of Novel S-adenosyl-L-methionine decarboxylase inhibitors as potent antiproliferative agents against intraerythrocytic Plasmodium falciparum parasites

International Journal for Parasitology: Drugs and Drug Resistance, 2014

Research paper thumbnail of Biochemical characterisation and novel classification of monofunctional S-adenosylmethionine decarboxylase of Plasmodium falciparum

Molecular and Biochemical Parasitology, 2011

Plasmodium falciparum like other organisms is dependent on polyamines for proliferation.

Research paper thumbnail of Deletion mutagenesis of large areas in Plasmodium falciparum genes: a comparative study

Malaria Journal, 2007

The increasing emergence of Plasmodium falciparum parasites resistant to most of the cost-effecti... more The increasing emergence of Plasmodium falciparum parasites resistant to most of the cost-effective drugs has necessitated the identification of novel leads and drug targets. Parasitespecific inserts in enzymes that are essential for the differentiation and proliferation of malarial parasites have received considerable interest since it distinguishes these proteins from their human counterparts. The functions of these inserts, which include mediations of protein activities or protein-protein interactions, are being investigated by several strategies including deletion mutagenesis. A comparative study of five widely used PCR-based mutagenesis methods identified a modified inverse PCR method as particularly suitable for the deletion of large areas (>100 bp) in malaria parasite genes.

Research paper thumbnail of Sustainable malaria control: transdisciplinary approaches for translational applications

Malaria Journal, 2012

With the adoption of the Global Malaria Action Plan, several countries are moving from malaria co... more With the adoption of the Global Malaria Action Plan, several countries are moving from malaria control towards elimination and eradication. However, the sustainability of some of the approaches taken may be questionable. Here, an overview of malaria control and elimination strategies is provided and the sustainability of each in context of vector-and parasite control is assessed. From this, it can be concluded that transdisciplinary approaches are essential for sustained malaria control and elimination in malaria-endemic communities.

Research paper thumbnail of Proteomic Profiling of Plasmodium falciparum through Improved, Semiquantitative Two-Dimensional Gel Electrophoresis

Journal of Proteome Research, 2010

Two-dimensional gel electrophoresis (2-DE) is one of the most commonly used technologies to obtai... more Two-dimensional gel electrophoresis (2-DE) is one of the most commonly used technologies to obtain a snapshot of the proteome at any specific time. However, its application to study the Plasmodial (malaria parasite) proteome is still limited due to inefficient extraction and detection methods and the extraordinarily large size of some proteins. Here, we report an optimized protein extraction method, the most appropriate methods for Plasmodial protein quantification and 2-DE detection, and finally protein identification by mass spectrometry (MS). Linear detection of Plasmodial proteins in a optimized lysis buffer was only possible with the 2-D Quant kit, and of the four stains investigated, Flamingo Pink was superior regarding sensitivity, linearity, and excellent MS-compatibility. 2-DE analyses of the Plasmodial proteome using this methodology resulted in the reliable detection of 349 spots and a 95% success rate in MS/MS identification. Subsequent application to the analyses of the Plasmodial ring and trophozoite proteomes ultimately resulted in the identification of 125 protein spots, which constituted 57 and 49 proteins from the Plasmodial ring and trophozoite stages, respectively. This study additionally highlights the presence of various isoforms within the Plasmodial proteome, which is of significant biological importance within the Plasmodial parasite during development in the intraerythrocytic developmental cycle.

Research paper thumbnail of Integration and mining of malaria molecular, functional and pharmacological data: how far are we from a chemogenomic knowledge space

Malaria Journal, 2006

The organization and mining of malaria genomic and post-genomic data is important to significantl... more The organization and mining of malaria genomic and post-genomic data is important to significantly increase the knowledge of the biology of its causative agents, and is motivated, on a longer term, by the necessity to predict and characterize new biological targets and new drugs. Biological targets are sought in a biological space designed from the genomic data from Plasmodium falciparum, but using also the millions of genomic data from other species. Drug candidates are sought in a chemical space containing the millions of small molecules stored in public and private chemolibraries. Data management should, therefore, be as reliable and versatile as possible. In this context, five aspects of the organization and mining of malaria genomic and post-genomic data were examined: 1) the comparison of protein sequences including compositionally atypical malaria sequences, 2) the high throughput reconstruction of molecular phylogenies, 3) the representation of biological processes, particularly metabolic pathways, 4) the versatile methods to integrate genomic data, biological representations and functional profiling obtained from X-omic experiments after drug treatments and 5) the determination and prediction of protein structures and their molecular docking with drug candidate structures. Recent progress towards a grid-enabled chemogenomic knowledge space is discussed.

Research paper thumbnail of Drug-resistant and mixed species malaria infections in Mpumalanga, South Africa

South African Journal of Science

Research paper thumbnail of Birkholtz L, Williams M, Reeksting S, Wells G, Roux S, Walter RD and AI Louw. (2008) A unique bifunctional enzyme complex controlling polyamine biosynthesis in Plasmodium falciparum is regulated by parasite-specific inserts. Int. J. Parasitol., 38

Research paper thumbnail of Van Brummelen AC, Llinas M, Louw AI and Birkholtz L. (2008) Co-inhibition of S-adenosylmethionine decarboxylase / ornithine decarboxylase of Plasmodium falciparum reveal compensatory mechanisms in the transcriptome. Int. J. Parasitol., 38

Polyamines are ubiquitous components of all living cells, and their depletion usually causes cyto... more Polyamines are ubiquitous components of all living cells, and their depletion usually causes cytostasis, a strategy employed for treatment of West African trypanosomiasis. To evaluate polyamine depletion as an anti-malarial strategy, cytostasis caused by the co-inhibition of S-adenosylmethionine decarboxylase/ ornithine decarboxylase in Plasmodium falciparum was studied with a comprehensive transcriptome, proteome, and metabolome investigation. Highly synchronized cultures were sampled just before and during cytostasis, and a novel zero time point definition was used to enable interpretation of results in lieu of the developmentally regulated control of gene expression in P. falciparum. Transcriptome analysis revealed the occurrence of a generalized transcriptional arrest just prior to the growth arrest due to polyamine depletion. However, the abundance of 538 transcripts was differentially affected and included three perturbation-specific compensatory transcriptional responses as follows: the increased abundance of the transcripts for lysine decarboxylase and ornithine aminotransferase and the decreased abundance of that for S-adenosylmethionine synthetase. Moreover, the latter two compensatory mechanisms were confirmed on both protein and metabolite levels confirming their biological relevance. In contrast with previous reports, the results provide evidence that P. falciparum responds to alleviate the detrimental effects of polyamine depletion via regulation of its transcriptome and subsequently the proteome and metabolome.

Research paper thumbnail of Morphological and Molecular Descriptors of the Developmental Cycle of Babesia divergens Parasites in Human Erythrocytes

PLOS Neglected Tropical Diseases, 2015

Human babesiosis, especially caused by the cattle derived Babesia divergens parasite, is on the i... more Human babesiosis, especially caused by the cattle derived Babesia divergens parasite, is on the increase, resulting in renewed attentiveness to this potentially life threatening emerging zoonotic disease. The molecular mechanisms underlying the pathophysiology and intra-erythrocytic development of these parasites are poorly understood. This impedes concerted efforts aimed at the discovery of novel anti-babesiacidal agents. By applying sensitive cell biological and molecular functional genomics tools, we describe the intra-erythrocytic development cycle of B. divergens parasites from immature, mono-nucleated ring forms to bi-nucleated paired piriforms and ultimately multi-nucleated tetrads that characterizes zoonotic Babesia spp. This is further correlated for the first time to nuclear content increases during intra-erythrocytic development progression, providing insight into the part of the life cycle that occurs during human infection. High-content temporal evaluation elucidated the contribution of the different stages to life cycle progression. Moreover, molecular descriptors indicate that B. divergens parasites employ physiological adaptation to in vitro cultivation. Additionally, differential expression is observed as the parasite equilibrates its developmental stages during its life cycle. Together, this information provides the first temporal evaluation of the functional transcriptome of B. divergens parasites, information that could be useful in identifying biological processes essential to parasite survival for future anti-babesiacidal discoveries.

Research paper thumbnail of A 2-methoxyestradiol bis-sulphamoylated derivative induces apoptosis in breast cell lines

Cell & Bioscience, 2015

Introduction: Research involving antimitotic compounds identified 2-methoxyestradiol (2ME2), as a... more Introduction: Research involving antimitotic compounds identified 2-methoxyestradiol (2ME2), as a promising anticancer endogenous metabolite. Owing to its low bioavailability, several in silico-designed 2ME2 analogues were synthesized. Structure-activity relationship studies indicated that an already existing 17-β-estradiol analogue, namely (8R,13S,14S,17S)-2-ethyl- 13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthrane-3,17-diyl bis(sulphamate) (EMBS) to exert potential in vitro anticancer activity. Methods: This study investigated the in vitro apoptotic influence of EMBS in an estrogen receptor-positive breast adenocarcinoma epithelial cell line (MCF-7); an estrogen receptor-negative breast epithelial cell line (MDA-MB-231) and a non-tumorigenic breast cell line (MCF-12A). Cell cycle progression, a phosphatidylserine flip, caspase 6-, 7-and 8 enzyme activity levels, Bcl-2 phosphorylation status at serine 70 and Bcl-2-and p53 protein levels were investigated to identify a possible action mechanism for apoptotic induction. Results: The xCELLigence real-time label-independent approach revealed that EMBS exerted antiproliferative activity in all three cell lines after 24 h of exposure. A G 2 M block was observed and apoptosis induction was verified by means of flow cytometry using propidium iodide and Annexin V-FITC respectively. EMBS-treated cells demonstrated a reduced mitochondrial membrane potential. EMBS exposure resulted in a statistically significant increase in p53 protein expression, decreased Bcl-2 protein expression and a decrease in pBcl-2(s70) phosphorylation status in all three cell lines. Results support the notion that EMBS induces apoptosis in all three cell lines. Conclusion: This study includes investigation into the apoptotic hallmarks exerted by EMBS after exposure of three cell lines namely MCF-7-, MDA-MDA-231-and MCF-12A cells. Increased caspase 6-, caspase 7-and caspase 8 activities, upregulation of p53 protein expression and a decrease in phosphorylation status of Bcl-2 at serine 70 in tumorigenic and non-tumorigenic lines were demonstrated.

Research paper thumbnail of The prevalence of mixed-species and antifolate-resistant malaria infections in Mpumalanga

South African medical journal = Suid-Afrikaanse tydskrif vir geneeskunde, 1998

To the Editor: A study was undertaken to establish the prevalence of mixed-species malaria infect... more To the Editor: A study was undertaken to establish the prevalence of mixed-species malaria infections and of antifolate-resistant parasites in the Mpumalanga province of South Africa. Blood samples from 56 infected patients were subjected to PCR amplification of the small-subunit ribosomal RNA genes for species identification. The PCRamplified gene of the antifolate target enzyme, dihydrofolate reductase (DHFR) in single Plasmodium falciparum-infected samples were subjected to restriction enzyme analysis to identify point mutations, which are known to confer resistance to pyrimethamine and proguanil.'

Research paper thumbnail of Synthesis and in vitro biological evaluation of dihydroartemisinyl-chalcone esters

European journal of medicinal chemistry, Jan 27, 2015

A series of dihydroartemisinyl-chalcone esters were synthesized through esterification of chalcon... more A series of dihydroartemisinyl-chalcone esters were synthesized through esterification of chalcones with dihydroartemisinin (DHA). The hybrids were screened against chloroquine (CQ) sensitive (3D7) and CQ resistant (W2) strains of intraerythrocytic Plasmodium falciparum parasites, and were all found to be active, with IC50 values ranging between 1.5 and 11 nM against both strains, with SI values over 5800. The esters featuring oxygenated aryl rings (7, 10 and 11), were found to be equipotent to DHA, but were 2-3 times more active than artesunate against the 3D7 and W2 strains of the malaria parasites. They were also screened in vitro against a panel of three cancer cell lines consisting of TK-10, UACC-62 and MCF-7. Compound 7, bearing a furan ring, displayed the most potent overall antitumor activity against all three cancer cell lines. TGA revealed that the targeted hybrids were all thermally more stable than DHA, which may be beneficial to the high temperature storage conditions t...

Research paper thumbnail of 2. Morris, E.J., Ngcete, Z., Birkholtz, L-M. and Louw, A.I. (2010) New Drugs to Fight Malaria. In Biovision 2008. From promises to practice: applications of science and technology in food, healthcare, energy and environment. Ed Ismail Serageldin, Ehsan Masood, with Mohamed El-Faham and Marwa El-W...

2. Morris, E.J., Ngcete, Z., Birkholtz, L-M. and Louw, A.I. (2010) New Drugs to Fight Malaria. In Biovision 2008. From promises to practice: applications of science and technology in food, healthcare, energy and environment. Ed Ismail Serageldin, Ehsan Masood, with Mohamed El-Faham and Marwa El-W...

Research paper thumbnail of Visagie MH, Stander BA, Birkholtz L-M, Joubert AM. Effects of a 17-beta estradiol analogue on gene expression and morphology in a breast epithelial adenocarcinoma cell line: A potential antiproliferative agent. Biomedical Research 2013; 24 (4): 525-530

Biomedical Research

that the estradiol analogue acts as an antimitotic agent in this highly metastatic breast cell li... more that the estradiol analogue acts as an antimitotic agent in this highly metastatic breast cell line. Data also showed that the newly designed estrogen analogue exerts an antiproliferative effect in this cancer cell line culminating in both apoptosis and autophagy as type of cell death paving the way for further investigations into its potential as anticancer agent.

Research paper thumbnail of Polyamine uptake in the malaria parasite, Plasmodium falciparum, is dependent on the parasite's membrane potential

Research paper thumbnail of Antimalarial drug discovery: in silico structural biology and rational drug design

Malaria remains one of the most burdensome human infectious diseases, with a high rate of resista... more Malaria remains one of the most burdensome human infectious diseases, with a high rate of resistance outbreaks and a constant need for the discovery of novel antimalarials and drug targets. For several reasons, Plasmodial proteins are difficult to characterise structurally using traditional physical approaches. However, these problems can be partially overcome using a number of in silico approaches. This review describes the peculiarities of malaria proteins and then details various in silico strategies to select and allow descriptions of the molecular structures of drug target candidates as well as subsequent rational approaches for drug design. Chiefly, homology modelling with specific focus on unique aspects of malaria proteins including low homology, large protein size and the presence of parasite-specific inserts is addressed and alternative strategies including multiple sequence and structure-based prediction methods, samplingbased approaches that aim to reveal likely global or shared features of a Plasmodial structure and the value of molecular dynamics understanding of unique features of Plasmodial proteins are discussed. Once a detailed description of the drug target is available, in silico approaches to the specific design of an inhibitory drug thereof becomes invaluable as an economic and rational alternative to chemical library screening.

Research paper thumbnail of Comparative properties of a three-dimensional model of Plasmodium falciparum ornithine decarboxylase

Proteins, 2003

The ornithine decarboxylase (ODC) component of the bifunctional S-adenosylmethionine decarboxylas... more The ornithine decarboxylase (ODC) component of the bifunctional S-adenosylmethionine decarboxylase/ornithine decarboxylase enzyme (PfAdoMetDC-ODC) of Plasmodium falciparum was modeled on the crystal structure of the Trypanosoma brucei enzyme. The homology model predicts a doughnut-shaped active homodimer that associates in a head-to-tail manner. The monomers contain two distinct domains, an N-terminal ␣/␤barrel and a C-terminal modified Greek-key domain. These domains are structurally conserved between eukaryotic ODC enzymes and are preserved in distant analogs such as alanine racemase and triosephosphate isomerase-like proteins. Superimposition of the PfODC model on the crystal structure of the human enzyme indicates a significant degree of deviation in the carbon ␣-backbone of the solvent accessible loops. The surface locality of the ab initio modeled 38 amino acid parasite-specific insert suggests a role in the stabilization of the large bifunctional protein complex. The active site pockets of PfODC at the interface between the monomers appear to be conserved regarding the binding sites of the cofactor and substrate, but each contains five additional malaria-specific residues. The predicted PfODC homology model is consistent with mutagenesis results and biochemical studies concerning the active site residues and areas involved in stabilizing the dimeric form of the protein. Two competitive inhibitors of PfODC could be shown to interact with several parasite-specific residues in comparison with their interaction with the human ODC. The PfODC homology model contributes toward a structurebased approach for the design of novel malariaspecific inhibitors. Proteins 2003;50:464 -473.

Research paper thumbnail of Integration and mining of malaria molecular, functional and pharmacological data: how far are we from a chemogenomic knowledge space?

Malar J, 2006

The organization and mining of malaria genomic and post-genomic data is important to significantl... more The organization and mining of malaria genomic and post-genomic data is important to significantly increase the knowledge of the biology of its causative agents, and is motivated, on a longer term, by the necessity to predict and characterize new biological targets and new drugs. Biological targets are sought in a biological space designed from the genomic data from Plasmodium falciparum, but using also the millions of genomic data from other species. Drug candidates are sought in a chemical space containing the millions of small molecules stored in public and private chemolibraries. Data management should, therefore, be as reliable and versatile as possible. In this context, five aspects of the organization and mining of malaria genomic and post-genomic data were examined: 1) the comparison of protein sequences including compositionally atypical malaria sequences, 2) the high throughput reconstruction of molecular phylogenies, 3) the representation of biological processes, particularly metabolic pathways, 4) the versatile methods to integrate genomic data, biological representations and functional profiling obtained from Xomic experiments after drug treatments and 5) the determination and prediction of protein structures and their molecular docking with drug candidate structures. Recent progress towards a grid-enabled chemogenomic knowledge space is discussed.

Research paper thumbnail of In silico discovery of Chemotherapeutic agents

Research paper thumbnail of Novel S-adenosyl-L-methionine decarboxylase inhibitors as potent antiproliferative agents against intraerythrocytic Plasmodium falciparum parasites

International Journal for Parasitology: Drugs and Drug Resistance, 2014

Research paper thumbnail of Biochemical characterisation and novel classification of monofunctional S-adenosylmethionine decarboxylase of Plasmodium falciparum

Molecular and Biochemical Parasitology, 2011

Plasmodium falciparum like other organisms is dependent on polyamines for proliferation.

Research paper thumbnail of Deletion mutagenesis of large areas in Plasmodium falciparum genes: a comparative study

Malaria Journal, 2007

The increasing emergence of Plasmodium falciparum parasites resistant to most of the cost-effecti... more The increasing emergence of Plasmodium falciparum parasites resistant to most of the cost-effective drugs has necessitated the identification of novel leads and drug targets. Parasitespecific inserts in enzymes that are essential for the differentiation and proliferation of malarial parasites have received considerable interest since it distinguishes these proteins from their human counterparts. The functions of these inserts, which include mediations of protein activities or protein-protein interactions, are being investigated by several strategies including deletion mutagenesis. A comparative study of five widely used PCR-based mutagenesis methods identified a modified inverse PCR method as particularly suitable for the deletion of large areas (>100 bp) in malaria parasite genes.

Research paper thumbnail of Sustainable malaria control: transdisciplinary approaches for translational applications

Malaria Journal, 2012

With the adoption of the Global Malaria Action Plan, several countries are moving from malaria co... more With the adoption of the Global Malaria Action Plan, several countries are moving from malaria control towards elimination and eradication. However, the sustainability of some of the approaches taken may be questionable. Here, an overview of malaria control and elimination strategies is provided and the sustainability of each in context of vector-and parasite control is assessed. From this, it can be concluded that transdisciplinary approaches are essential for sustained malaria control and elimination in malaria-endemic communities.

Research paper thumbnail of Proteomic Profiling of Plasmodium falciparum through Improved, Semiquantitative Two-Dimensional Gel Electrophoresis

Journal of Proteome Research, 2010

Two-dimensional gel electrophoresis (2-DE) is one of the most commonly used technologies to obtai... more Two-dimensional gel electrophoresis (2-DE) is one of the most commonly used technologies to obtain a snapshot of the proteome at any specific time. However, its application to study the Plasmodial (malaria parasite) proteome is still limited due to inefficient extraction and detection methods and the extraordinarily large size of some proteins. Here, we report an optimized protein extraction method, the most appropriate methods for Plasmodial protein quantification and 2-DE detection, and finally protein identification by mass spectrometry (MS). Linear detection of Plasmodial proteins in a optimized lysis buffer was only possible with the 2-D Quant kit, and of the four stains investigated, Flamingo Pink was superior regarding sensitivity, linearity, and excellent MS-compatibility. 2-DE analyses of the Plasmodial proteome using this methodology resulted in the reliable detection of 349 spots and a 95% success rate in MS/MS identification. Subsequent application to the analyses of the Plasmodial ring and trophozoite proteomes ultimately resulted in the identification of 125 protein spots, which constituted 57 and 49 proteins from the Plasmodial ring and trophozoite stages, respectively. This study additionally highlights the presence of various isoforms within the Plasmodial proteome, which is of significant biological importance within the Plasmodial parasite during development in the intraerythrocytic developmental cycle.