A Novel Approach to Extract Morphological Variables in Crystalline Polymers from Time-Resolved Synchrotron SAXS Data (original) (raw)

Use of SAXS and linear correlation functions for the determination of the crystallinity and morphology of semi‐crystalline polymers. Application to linear polyethylene

Michel Koch

Journal of Polymer Science Part B: Polymer Physics, 1999

View PDFchevron_right

Synchrotron studies of polymers at high spatial and temporal resolution

Arumugam Mahendrasingam

View PDFchevron_right

Structural changes in isothermal crystallization processes of synthetic polymers studied by time-resolved measurements of synchrotron-sourced X-ray scatterings and vibrational spectra

Hisakatsu HAMA

Macromolecular Research, 2004

View PDFchevron_right

DSC/SAXS analysis of the thickness of lamellae of semicrystalline polymers-restrictions in the case of materials with swollen amorphous phase

Marta Safandowska

Polymer Testing, 2018

View PDFchevron_right

A direct method to determine the degree of crystallinity and lamellar thickness of polymers: application to polyethylene

Wim Bras

Polymer, 1994

View PDFchevron_right

Use of time-resolved X-ray scattering methods for investigation of structural formation in polymer liquid crystals

Ginka Exner

2011

View PDFchevron_right

Small-Angle X-ray Scattering of Polymers

Benjamin Hsiao

Chemical Reviews, 2001

View PDFchevron_right

Adaptation of the Rietveld Method for the Characterization of the Lamellar Microstructure of Polymers

Alain Jonas

Journal of Applied Crystallography, 1997

View PDFchevron_right

Investigation of structural changes in semi-crystalline polymers during deformation by synchrotron X-ray scattering

Konrad Schneider

Journal of Polymer Science Part B: Polymer Physics, 2010

View PDFchevron_right

Polymer processing: Using synchrotron radiation to follow structure development in commercial and novel polymer materials

Wim Bras

Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 2005

View PDFchevron_right

ToF-SIMS and principal component analysis: Effect of film thickness on crystal surfaces of polymers

Yiu Ting Richard Lau

Surface and Interface Analysis, 2010

View PDFchevron_right

Time-resolved X-ray wide angle scattering studies of the effect of draw rate and temperature on the development of orientation and crystallinity in PET

Arumugam Mahendrasingam

Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 1995

View PDFchevron_right

Simultaneous measurements of small angle x-ray scattering, wide angle x-ray scattering, and dielectric spectroscopy during crystallization of polymers

Zlatan Denchev

Review of Scientific Instruments, 2000

View PDFchevron_right

Phase densities and lamellar morphologies of semicrystalline polyethylenesviaabsolute small-angle X-ray scattering measurements

Jan Skov Pedersen

Journal of Applied Crystallography, 2015

View PDFchevron_right

Time-Resolved Saxs/Waxs Study of Phase Behavior and Crystallization in Polymer Blends

Peter Laggner

Journal of Macromolecular Science, Part B, 2002

View PDFchevron_right

Time-Resolved Two-Dimensional Small Angle X-ray Scattering Studies of Oriented Poly(ethylene terephthalate) (PET) Using Paracrystalline Modeling Techniques

Arumugam Mahendrasingam

Macromolecules, 1995

View PDFchevron_right

Time-resolved X-ray diffraction studies of structural transitions in organic polymers using synchrotron radiation

Arumugam Mahendrasingam

Le Journal de Physique IV, 1994

View PDFchevron_right

Structural changes in isothermal crystallization process of polyoxymethylene investigated by time-resolved FTIR, SAXS and WAXS measurements

Hisakatsu HAMA

Polymer, 2003

View PDFchevron_right

Experimental separation of the coherent component of X-ray scattering prior to RDF analysis of non-crystalline polymers

Alan Windle

Journal of Applied Crystallography, 1980

View PDFchevron_right

Combining X-ray scattering with dielectric and calorimetric experiments for monitoring polymer crystallization

Christoph Schick

European Polymer Journal, 2009

View PDFchevron_right

Probing the Early Stages of Melt Crystallization in Polypropylene by Simultaneous Small- and Wide-Angle X-ray Scattering and Laser Light Scattering

Srivatsan Srinivas

Macromolecules, 2000

View PDFchevron_right

Multistep Crystallization Process Involving Sequential Formations of Density Fluctuations, “Intermediate Structures”, and Lamellar Crystallites: Poly(3-hydroxybutyrate) As Investigated by Time-Resolved Synchrotron SAXS and WAXD

Nicolas Spegazzini

Macromolecules, 2012

View PDFchevron_right

Interplay between amorphous and crystalline domains in semicrystalline polymers by simultaneous SAXS, WAXS and Dielectric Spectroscopy

Alejandro Romero Sanz

IOP Conference Series: Materials Science and Engineering, 2010

View PDFchevron_right

Study of temperature dependence of crystallisation transitions of a symmetric PEO-PCL diblock copolymer using simultaneous SAXS and WAXS measurements with synchrotron radiation

Sergio Funari

The European Physical Journal E, 2008

View PDFchevron_right

A non-isothermal technique using thermal x-ray diffraction to follow the kinetics of polymer crystallization, solid state phase transformations and the determination of the length of the crystalline segment

Rafiq Redwan Abou-Shaaban

Thermochimica Acta, 1978

View PDFchevron_right

SEM, ToF-SIMS and LFM morphological study of an heterogeneous polymeric surface

Claude Poleunis

Microscopy Microanalysis Microstructures, 1994

View PDFchevron_right

Time-averaged normal coordinate analysis of polymer particles and crystals

Bobby Sumpter

Chemical Physics Letters, 2000

View PDFchevron_right

Isothermal and non-isothermal crystallization kinetics of branched and partially crosslinked PET

Dimitris Achilias

Journal of Thermal Analysis and Calorimetry, 2006

View PDFchevron_right

Energy-dispersive small-angle x-ray scattering for investigating polymer morphology: Static and time-resolved experiments

Andrea Martinelli

Applied Physics Letters, 2004

View PDFchevron_right

Free and constrained amorphous phases in polyethylene: Interpretation of 1H NMR and SAXS data over a broad range of crystallinity

Juraj Kosek

Polymer, 2015

View PDFchevron_right

Simultaneous crystalline-amorphous phase evolution during crystallization of polymer systems

Z. Denchev

Europhysics Letters (EPL), 2002

View PDFchevron_right

X-ray Diffraction Analysis of Polymeric Solid Using Bragg-Brentano Geometry

Biswajit Mallick

View PDFchevron_right

Evolution of density fluctuations to lamellar crystals in linear polyethylene

Yvonne Kielhorn

Journal of Chemical Physics, 1999

View PDFchevron_right

Fourier analysis of polymer x-ray diffraction patterns

B. Crist

1979

View PDFchevron_right

Lamellar Thickness of a Syndiotactic Polystyrene Determined from Small-angle X-ray Scattering and Transmission Electron Microscopy

Ea-mor Woo

2002

View PDFchevron_right