Splitting of the Magnetic Loss Peak of Composites under External Magnetic Field (original) (raw)
Related papers
Journal of Magnetism and Magnetic Materials, 2019
A new method of studying microwave magnetic properties of metal particles and films is developed. The method is based on measurements with swept frequency under magnetic bias in a coaxial line. Application of the technique is illustrated by the data obtained for two types of samples, washershaped rolls of thin ferromagnetic films and composites filled with flake Sendust particles. The treatment of the measured data is performed with an account for sample demagnetization and anisotropy. The values of the anisotropy field and the saturation magnetization of thin iron films are calculated considering demagnetization of the sample. Because of the anisotropy of the composite samples, permeability depends slightly on the length of samples, and the saturation magnetization and the anisotropy field cannot be determined.
Frequency dependence of microwave complex permeability under magnetic bias
EPJ Web of Conferences, 2018
Measurement of the frequency dependence of the permeability under magnetic bias is proposed as a new method for studying the microwave magnetic properties of magnetic materials. The samples under study are either rolls of thin ferromagnetic films or the composites filled with sendust particles. It is shown that the permeability measured under external magnetic bias depends on sample thickness. The correct interpretation of the measured data is possible only when sample demagnetization is accounted for. The values of the anisotropy field and the saturation magnetization of thin nitrogen doped iron films and flake-shaped sendust particles are calculated considering demagnetization of the washer-shaped sample.
High-frequency behavior of magnetic composites
Journal of Magnetism and Magnetic Materials, 2009
The paper reviews recent progress in the field of microwave magnetic properties of composites. The problem under discussion is developing composites with high microwave permeability that are needed in many applications. The theory of magnetic composites is briefly sketched with the attention paid to the laws governing the magnetic frequency dispersion in magnetic materials and basic mixing rules for composites. Recent experimental reports on the microwave performance of magnetic composites, as well as data on the agreement of the mixing rules with the measured permeability of composites that are available from the literature are discussed. From the data, a conclusion is made that the validity of a mixing rule is determined by the permeability contrast in the composite, i.e., the difference between permeability of inclusions and that of the host matrix. When the contrast is low, the Maxwell Garnet mixing rule is frequently valid. When the contrast is high, which is of the most interest for obtaining high microwave permeability of a composite, no conventionally accepted theory is capable of accurately predicting the permeability of the composites. Therefore, the mixing rules do not allow the microwave properties of magnetic composites to be predicted when the permeability of inclusions is high, that is the case of the most interest. Because of that, general limitations to the microwave performance of composites are of importance. In particular, an important relation constraining the microwave permeability of composites follows from Kittel's theory of ferromagnetic resonance and analytical properties of frequency dependence of permeability. Another constraint concerning the bandwidth of electromagnetic wave absorbers follows from the Kramers-Kronig relations for the reflection coefficient. The constraints are of importance in design and analysis of electromagnetic wave absorbers and other devices that employ the microwave magnetic properties of composites, such as magnetic substrates for microwave antennas, microwave inductors, etc.
Physical Review B, 2002
The high-frequency permittivity of composites consisting of a lattice of ferromagnetic wires is investigated. Experimental results using free space or coaxial line microwave measurements are reported. It is shown that the dielectric response is strongly dependent on the magnetic properties of the wires. Negative real permittivity is observed over a wide frequency range for wires with circumferential magnetization, while a resonant behavior is observed on wires with an axially magnetized core. In addition, it is shown that a moderate external field can induce large changes in the dielectric response. We prove that the underlying physics of these composites made of oriented magnetic wires is basically the same as the giant magnetoimpedance ͑GMI͒ effect. A model based on GMI equations is proposed which predicts this unusual dielectric phenomenon.
Microwave permeability of Co[sub 2]Z composites
Journal of Applied Physics, 2005
The microwave permittivity and permeability of Co 2 Z barium ferrite composite samples are measured as functions of frequency and volume fraction of the ferrite. Magnetostatic properties of the bulk ferrite are determined. This allows Snoek's law [J. L. Snoek, Physica 14, 204 (1948)] to be verified by comparing the microwave and magnetostatic Snoek's constants. The modification of Snoek's law for hexagonal ferrites suggested recently by Acher et al. [Phys. Rev. B 62, 11324 (2000)] is also verified. Acher's constant is found from microwave measurements to agree with the value calculated from the magnetostatic properties of bulk ferrite, but microwave and magnetostatic Snoek's constant do not agree. This may be attributed to the effect due to demagnetizing factors of ferrite inclusions that are not considered in the derivation of Snoek's and Acher's laws. The measured frequency-dependent permeability of composites satisfies the Lorentzian dispersion law and is consistent with the Maxwell Garnett approximation [J. C. Maxwell Garnett, Philos. Trans. R. Soc. London 203, 385 (1904)]. According to the theoretical analysis based on the Lorentzian dispersion law and the Maxwell Garnet mixing rule, both Snoek's and Acher's constants must be linear functions of the volume fraction, independent of whether microwave values of the constants are in agreement with the magnetostatic values. In contrast, the experimental measurements reveal a steady decrease of both constants with the volume fraction. The disagreement is discussed in terms of the influence of effective medium in composite on the inherent permeability of ferrite particles.
Procedia Engineering, 2017
The paper considers the application of mixing rules to the analysis of the microwave effective material parameters, the permittivity and permeability, of composites. It is suggested to perform the analysis in terms of the normalized inverse susceptibility defined as the volume fraction of inclusions divided by the effective dielectric or magnetic susceptibility of the composite. This allows the volume fraction dependence of the effective material parameters to be represented in a form that is convenient for the analysis, so that distinguishing features of the dependence become more pronounced and helpful for understanding the factors that affect the effective properties of the composite. The proposed approach is illustrated by the analysis of the measured data on the microwave material parameters of composites comprising Sendust powder with either spherical or platelet powder particles, and Permalloy powders with particles of the stone-like shape. The microwave material parameters are measured with paraffin-based composite samples in the 7/3-mm coaxial air-filled waveguide by the Nicolson-Ross-Weir technique. It is shown that for Sendust particles, the interaction between inclusions is low. For the composites comprising spherical particles, the Maxwell Garnet mixing rule is a good approximation of the volume fraction dependence of microwave permeability. For the platelet powder particles, the magnetic performance is governed by the Wiener mixing rule. For composites filled with Permalloy powder, the contribution of the interaction between inclusions to the effective permeability is essential. Therefore, the suggested approach allows the type of mixing rule suitable for description of material parameters of a given composite to be determined.
Modeling the Composites for Magnetoelectric Microwave Devices
Sensors
Many studies of the ME effect have been carried out in the microwave range in connection with the possibility of creating new electronic devices. One of the main microwave ME effects is the FMR line shift in an electric field, and the purpose of this article is to compare the FMR line shift in the ME structure in an electric field for a number of ferromagnetic metals, their alloys, and YIG ferrite using various piezoelectrics. This article discusses the regimes when the bias field is directed along the main axes of the magnetic component, while, as is known, the observed effect is due only to deformation. As a result of the study, ME structures with maximum and minimum microwave ME effects were found. In addition, the “substrate effect” in the piezoelectric YIG-GGG structure is considered.
Technical Physics, 2009
The structure and microwave magnetic properties of Fe powders grounded in argon or acetone and also of Fe-Si-C and amorphous Fe-Co-Si-C powders mechanically alloyed in argon are studied using X-ray diffraction, Mössbauer spectroscopy, granulometric and microscopic analyses, magnetostatic measurements, and microwave spectroscopy. The goal of investigation is to determine the influence of factors (shape, size, and chemical and phase compositions of grains) governing the microwave material parameters of composites based on these alloys in the frequency range 0.1-3.0 GHz. It is shown that the difference in the grain shape is the basic reason for the difference in the microwave permeability at low frequencies (3 GHz or lower). At higher frequencies, the magnetic properties are related to the skin effect and depend largely on the grain size. The differences in the microwave properties of the composites are not significant and are concealed by the above effects. PACS numbers: 41.20.-q
Microwave permeability of Co2Z composites
Journal of Applied Physics, 2005
The microwave permittivity and permeability of Co 2 Z barium ferrite composite samples are measured as functions of frequency and volume fraction of the ferrite. Magnetostatic properties of the bulk ferrite are determined. This allows Snoek's law [J. L. Snoek, Physica 14, 204 (1948)] to be verified by comparing the microwave and magnetostatic Snoek's constants. The modification of Snoek's law for hexagonal ferrites suggested recently by Acher et al. [Phys. Rev. B 62, 11324 (2000)] is also verified. Acher's constant is found from microwave measurements to agree with the value calculated from the magnetostatic properties of bulk ferrite, but microwave and magnetostatic Snoek's constant do not agree. This may be attributed to the effect due to demagnetizing factors of ferrite inclusions that are not considered in the derivation of Snoek's and Acher's laws. The measured frequency-dependent permeability of composites satisfies the Lorentzian dispersion law and is consistent with the Maxwell Garnett approximation [J. C. Maxwell Garnett, Philos. Trans. R. Soc. London 203, 385 (1904)]. According to the theoretical analysis based on the Lorentzian dispersion law and the Maxwell Garnet mixing rule, both Snoek's and Acher's constants must be linear functions of the volume fraction, independent of whether microwave values of the constants are in agreement with the magnetostatic values. In contrast, the experimental measurements reveal a steady decrease of both constants with the volume fraction. The disagreement is discussed in terms of the influence of effective medium in composite on the inherent permeability of ferrite particles.
Predicting of wideband electromagnetic responses of composites containing magnetic inclusions
2010 IEEE International Symposium on Electromagnetic Compatibility, 2010
Engineering of absorbing bulk and sheet composite materials, including nanocomposites, for various EMI applications, requires adequate prediction of frequency and concentration behavior of these composites. This paper proposes two simple analytical formulations for effective permittivity and permeability of magneto-dielectric composites as functions of frequency and concentration. The first new proposed mixing rule is based on the GhoshíFuchs theory, which gives good agreement with the measured permittivity and permeability for composites containing magnetic alloy powders. This approach employs the Bergman-Milton concept of spectral function. Herein, the spectral function typical for the Bruggeman effective medium theory, also known as the Bruggeman symmetric rule (BSR), is chosen. This spectral function is composed using two fitting parameters: an averaged shape factor of inclusions, and the percolation threshold. These fitting parameters are found from the concentration dependence of permittivity, and then they are used to retrieve frequency dependence of permeability. The proposed mixing law is valid for nearly spherical inclusions in the composite, e.g., crumbs. Another analytical model proposed in this work can be applied to predict effective permeability of composites containing magnetic inclusions. It is based on the Bruggeman asymmetric rule (BAR), which has been modified in such a way that it takes into account shape factors of magnetic inclusions, in particular, randomly oriented platelets.