Effect of different surface treatments on resin-matrix CAD/CAM ceramics bonding to dentin: in vitro study (original) (raw)
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Bond strength of modern self-adhesive resin cements to human dentin and different CAD/CAM ceramics
Acta of Bioengineering and Biomechanics, 2020
Purpose: The aim of the study was to evaluate the shear bond strength of CAD/CAM ceramics to dentin after cementation with conventional or self-adhesive resin cements. Methods: Three self-adhesive, self-etching cements (Panavia SA, RelyX U200, Maxcem Elite), and one conventional cement (Panavia V5), were selected to lute three CAD/CAM ceramics (IPS Empress CAD, IPS e.max CAD, IPS e.max ZirCAD) onto the dentin. The bond strength was evaluated using a shear strength test according to the PN-EN ISO 29022:2013-10. Evaluation of the differences was performed using the Statistica software. Failure modes were analyzed using a light microscope. Results: All the studied cements differed (regardless of the ceramic type) in the bond strength. The highest bond strength was observed in Panavia V5, lower – in RelyX U200 and Panavia SA, and the lowest – in Maxcem. For IPS e.max ZirCAD, it was observed that compared to Panavia V5, the other cements were characterized by a significantly higher bond ...
Microtensile bond strength of CAD/CAM materials to dentin under different adhesive strategies
Brazilian Oral Research, 2017
The present study aimed to evaluate the microtensile bond strength (µTBS) of novel computer-aided design/computer-aided manufacturing (CAD/CAM) restorative materials to dentin using different adhesive strategies. Thirty-two crowns were milled using CAD/CAM materials (Vita Mark II as control, Vita Suprinity, Vita Enamic and Lava Ultimate) and luted to dentin using different resin cements (RelyX ARC, RelyX Unicem 2 and RelyX Ultimate). The specimens were stored in 100% relative humidity at 37°C for 24 h and sectioned. The samples (n = 16) with cross-sectional areas of approximately 0.90 mm², were submitted to a µTBS test in a universal testing machine with a crosshead speed of 0.5 mm/min. The samples were analyzed with SEM to determinate the failure mode. According to 2-way ANOVA and Tukey's test (α=0.05), the interaction effect (material x luting strategy) was significant (p=0.001). Regardless of the luting strategy, a higher µTBS was obtained with Lava Ultimate and Vita Enamic, which were significantly different from Vita Mark II and Vita Suprinity (p<0.05). For Vita Mark II, Vita Suprinity, Vita Enamic, and Lava Ultimate, the µTBS obtained with RelyX Unicem 2 was not significantly different from that obtained with RelyX ARC or RelyX Ultimate. All groups obtained at least three types of failure. The adhesive strategy with self-adhesive resin cement was comparable to conventional resin cement with total-etch or self-etch adhesive techniques in the bond of novel CAD/CAM materials to dentin.
International Journal of Molecular Sciences, 2022
The aim of the study was to evaluate the influence of thermocycling on the shear bond strength of self-adhesive, self-etching resin cements luted to human dentin and computer-aided design/computer-aided manufacturing (CAD/CAM) ceramics. Three modern self-adhesive dental cements (Maxcem Elite, RelyX U200, Panavia SA) were used to lute three CAD/CAM ceramics (IPS Empress CAD, IPS e.max CAD, IPS e.max ZirCAD) onto the dentin. One conventional cement (Panavia V5) served as a control. After preparation, the samples were subjected to thermocycling as a method of artificial aging of dental materials applied to simulate long-term use in oral conditions. Shear bond strength was evaluated according to PN-EN ISO 29022:2013-10 and failure modes were observed under a light microscope. Statistical analysis was performed. The study demonstrated that a combination of ceramics and cements directly impacts the bond strength. The highest bond strength was observed in Panavia V5, lower in Panavia SA an...
Introduction: Ceramics are still the most aesthetically pleasing materials available for restorative dentistry. However, due to the metal infrastructure of metal-supported ceramic systems, which were developed to increase the physical properties, esthetic and biological adaptations cannot be fully obtained. Objective of the study: The main objective of the study is to find the evidence on resin bonding related to long-term clinical outcomes of tooth-and implant-supported high-strength ceramic restorations. Methodology of the study: Four different surface processes were used as surface-treatment procedures. The first three procedures were applied to samples of IPS Empress and IPS Empress 2 ceramic discs. Sandblasting with Al2O3, blasting with soda and glass beads, and the Bateman etch retention system were applied to samples of In-Ceram ceramic discs. The discs were cemented to composite bars. Two types of cement were used; Rely X adhesive resin cement and Rely X modified glass ionomer cement and, all the samples were subjected to a shear test to evaluate their bond strengths. Results: With the IPS Empress and the IPS Empress 2 ceramic discs, the best bonding was obtained in the group etched with Al2O3 sandblasting and hydrofluoric acid after cementation using the Rely X adhesive resin cement. Conclusion: The in vitro findings from this study indicate that surface-treatment procedures applied to the IPS Empress and the IPS Empress 2 full-ceramic systems are important when cement types are considered. In contrast, cement types and surface-treatment methods had no effect on changing the bond strength of the In-Ceram ceramic system.
2020
Aim of the study: The aim of this study was to evaluate the shear bond strength of three different CAD/CAM ceramic blocks repaired with Nano-hybrid composite resin using three different repair adhesives, and to Compare and determine which bonding systems achieve superior bond strength with each type of ceramic materials tested. Materials and methods: A total of 72 specimens (10 × 10 × 2 mm) of ceramic mini-blocks will be prepared and divided into three groups (n=24) according to the type of ceramic materials as: Group A: A resin Nano ceramic (VITA Enamic EM-14 2m2HT). Group B: A feldspar ceramic (Cerec block CPC-14 A2C; Sirona Dental, Germany). Group C: A lithium disilicate reinforced ceramic (IPS e.max HTA2 CAD; IVOCLAR), then each type was subjected to surface roughness using silicon carbide paper with a grit size of 120 p. Thermo-cycled (500 cycles, 5 °C to 55 °C). Each group was divided into three subgroups treated with three types of repair adhesives as: (1) Ceramic repair kit ...
The Journal of Advanced Prosthodontics, 2017
PURPOSE. To evaluate the effects of different surface treatments on the bond strength of novel CAD/CAM restorative materials to resin cement by four point bending test. MATERIALS AND METHODS. The CAD/CAM materials under investigation were e.max CAD, Mark II, Lava Ultimate, and Enamic. A total of 400 bar specimens (4×1.2×12 mm) (n=10) milled from the CAD/CAM blocks underwent various pretreatments (no pretreatment (C), hydrofluoric acid (A), hydrofluoric acid + universal adhesive (Scotchbond) (AS), sandblasting (Sb), and sandblasting + universal adhesive (SbS)). The bars were luted end-to-end on the prepared surfaces with a dual curing adhesive resin cement (Variolink N, Ivoclar Vivadent) on the custom-made stainless steel mold. Ten test specimens for each treatment and material combination were performed with four point bending test method. Data were analyzed using ANOVA and Tukey's test. RESULTS. The surface treatment and type of CAD/CAM restorative material showed a significant effect on the four point bending strength (FPBS) (P<.001). For LDC, AS surface treatment showed the highest FPBS results (100.31 ± 10.7 MPa) and the lowest values were obtained in RNC (23.63 ± 9.0 MPa) for control group. SEM analyses showed that the surface topography of CAD/CAM restorative materials was modified after treatments. CONCLUSION. The surface treatment of sandblasting or HF acid etching in combination with a universal adhesive containing MDP can be suggested for the adhesive cementation of the novel CAD/CAM restorative materials.
Effect of alumina-blasting pressure on adhesion of CAD/CAM resin block to dentin
Dental materials journal, 2018
The aim of this study was to evaluate how alumina-blasting pressure affects the bond strength of CAD/CAM resin blocks (CRBs) to bovine dentin using two different types of resin cements. CRB slices were divided into three groups by alumina-blasting pressure, namely, untreated and 0.1 MPa and 0.2 MPa, and further divided into three subgroups by combination of CRBs surface treatment and types of cement: Scotchbond Universal and RelyX ultimate (RXB), Scotchbond Universal and RelyX unicem2 (U2B), ceramic primer and RelyX unicem2 (U2C). The CRB slices were then cemented to bovine dentin, microtensile bond strength test was performed and evaluated. Regardless of the alumina-blasting pressure, RXB group have the highest µTBS and bond strength tends to increase with increasing alumina-blasting pressure. Alumina-blasting to CRB surface by at an appropriate pressure and use of conventional resin cement were required to obtain strong adhesion with the tooth structure.
Dental Materials Journal, 2007
To increase the bond strength of CAD/CAM-fabricated, leucite-reinforced glass ceramics with a resin cement, the effects of the following were investigated: surface modification by tribochemical (TBC) treatment, followed by combined application of a silane coupling agent and a functional monomer as a primer. Bond strength was evaluated by a shear bond test. It was found that a silane coupling agent was useful for all the surfaces, particularly for the TBC-treated surface. This was because of the presence of a silica layer on the modified surface. The combination of a silane coupling agent and a functional monomer on the TBC surface allowed marked improvement in bonding, whereby the bonding endured 20,000 cycles of thermal cycling. Therefore, TBC treatment in combination with a silane coupling agent and a functional monomer as a primer substantially increased the bond strength of CAD/CAM-fabricated glass ceramics with resin cement, if the treatment conditions were appropriate.