Effect of cooling rate on solidification characteristics of aluminium alloy AA 5182 (original) (raw)

Computer-aided cooling curve thermal analysis used to predict the quality of aluminum alloys

Journal of Thermal Analysis and Calorimetry, 2011

The effects of bismuth (Bi), antimony (Sb) and strontium (Sr) additions on the characteristic parameters of the evolution of aluminium dendrites in a near eutectic Al-11.3Si-2Cu-0.4Fe alloy during solidification at different cooling rates (0.6-2°C) were investigated by computer-aided cooling curve thermal analysis (CA-CCTA). Nucleation temperature (T aÀAl N ) is defined with a new approach based on second derivative cooling curve. The results showed that T aÀAl N increased with increasing cooling rate but both the growth temperature (T aÀAl G ) and the coherency temperature (T DCP ) decreased. Increase in the temperature difference for dendrite coherency (T aÀAl N À T DCP ) with increasing cooling rate indicate a wider range of temperature before the dendrite can impinge on each other and higher fraction solid (f DCP S ). Additions of Bi, Sb and Sr to the base alloy produced only a minor effect on T aÀAl N . Additions of Bi and Sb resulted in an increase in fraction solid and an increase of 30 % in the value of T aÀAl N À T aÀAl G to almost 13°C.

Determination of the Dendrite Coherency Point during Solidification by Means of Thermal Diffusivity Analysis

Metallurgical and Materials Transactions A-physical Metallurgy and Materials Science, 2007

Dendrite coherency point in an aluminum-silicon-copper casting alloy was determined by analyses of the variation of the thermal diffusivity. The analysis was carried out using the readings of three thermocouples inserted at equal distances in a mould holding the alloy left to solidify. The values obtained by this method are confirmed by metallographic observations on samples left to solidify to the coherency point before plunging them in water.

Correlation between unsteady-state solidification conditions, dendrite spacings, and mechanical properties of Al-Cu alloys

Metallurgical and Materials Transactions A-physical Metallurgy and Materials Science, 2000

The wide range of operational conditions existing in foundry and casting processes generates as a direct consequence a diversity of solidification microstructures. Structural parameters such as grain size and interdendritic spacings are strongly influenced by the thermal behavior of the metal/mold system during solidification, imposing, as a consequence, a close correlation between this system and the resulting microstructure. Mechanical properties depend on the microstructural arrangement defined during solidification. Expressions correlating the mechanical behavior with microstructure parameters should be useful for future planning of solidification conditions in terms of a determined level of mechanical strength, which is intended to be attained. In the present work, analytical expressions have been developed describing thermal gradients and tip growth rate during one-dimensional unsteadystate solidification of alloys. Experimental results concerning the solidification of Al-4.5 wt pct Cu and Al-15 wt pct Cu alloys and dendritic growth models have permitted the establishment of general expressions correlating microstructure dendrite spacings with solidification processing variables. The correlation of these expressions with experimental equations relating mechanical properties and dendrite spacings provides an insight into the preprogramming of solidification in terms of casting mechanical properties. JOSÉ M.V. QUARESMA, formerly Graduate Research Assisant, Departdrite arm spacings have been linked to other solidification ment of Materials Engineering, State University of Campinas, UNICAMP, is Associate Professor, Department of Mechanical Engineering, Federal thermal parameters, such as dendritic tip velocity and tempera-University of Para, Para, Brazil. CARLOS A. SANTOS, Research Assistant, ture gradient in the solidifying material, as a function of and AMAURI GARCIA, Professor, are with the Department of Materials distance from the chill surface. Based on mathematical models Engineering, State University of Campinas, UNICAMP, 13-083-970, Camof heat transfer and dendritic growth during unsteady-state pinas-SP, Brazil.

Thermal analysis as a microstructure prediction tool for A356 aluminium parts solidified under various cooling conditions

2011

Thermal analysis technique has been used for a long time, in both ferrous and nonferrous industries for evaluating the metallurgical quality of the liquid metal before casting. However, obtaining a proper microstructure in a standard cup does not ensure that the microstructure is correct in real parts which may solidify at very different cooling rates. For this study, alloy A356 with different metal quality in terms of modification and grain refinement was tested. Different cooling rates were obtained by using cylindrical test samples with various diameters cast in sand and metallic moulds. The correlation between microstructure features such as grain size, modification rate and secondary dendrite arm spacing (SDAS) measured in the standard thermal analysis cup with those obtained in the cylindrical test parts has been investigated. Thus, knowing the thermal modulus and the mould type it is possible to establish the required grain size and modification rate in the standard cup in or...

Solidification phenomena related to direct chill casting of aluminium alloys: fundamental studies and future challenges

Materials Technology: Advanced Performance Materials, 2009

The principal mechanisms of structure and defect formation during solidification of direct chill (DC) cast billets are reviewed, drawing largely on the results of studies carried out over the past 10 years at Delft University of Technology and the Materials innovation institute. These studies have demonstrated the complexity of mechanisms involved in the formation of structure, macrosegregation and hot tearing and the power of coupled modelling and experimental work in elucidating these phenomena, e.g. relating as cast microstructure to the temperature distribution and flow patterns in the sump of a billet. Control over structure formation and elimination of casting defects can be achieved only when the contributions of all the mechanisms involved and the ratio of these contributions are taken into account. Some immediate challenges for future research are identified.

The effects of cooling slope on the semi-solid microstructures of Al4.8Si2.8Cu0.5Mg aluminium alloy

2018

Thixoforming process is a metal forming process in the semi-solid condition to produce near net shaped products. The key requirement of the thixoforming process is the production of feedstock materials that consists of solid spheroids in the liquid matrix, rather than dendrites. The solid spheroidal structure could not be generated if the gravity cast alloy that consists of the dendritic structure is directly subjected to partial remelting. Cooling slope casting process is one of the simplest and cheapest methods that can be utilised to produce the nondendritic structure. In the present study, the effects of cooling slope casting process on the microstructure of Al4.8Si2.8Cu0.5Mg aluminium alloy were investigated. The alloy was melted at a superheated temperature of 700 °C before cooled down to the selected pouring temperature (650 °C) and subsequently poured onto a stainless steel plate with the cooling length of 400 mm. The plate was tilted at 60° from horizontal and was cooled wi...

Optimization of processing parameters of cooling slope process for semi-solid casting of ADC 12 Al alloy

Journal of the Brazilian Society of Mechanical Sciences and Engineering, 2018

In the present work, the effect of processing parameters of cooling slope techniques (pouring temperature, slope angle and slope length) of ADC 12 Al alloy on its microstructural evolution has been studied in detail. A series of cooling slope casting experiments were conducted by varying the pouring temperature (580, 585 and 590°C), slope length (400, 500 and 600 mm) and slope angle (30°, 45°and 60°). The effect of processing parameters on the response factors, viz. degree of sphericity and particle size, has been investigated by applying analysis of variance (ANOVA), interaction graphs obtained using response surface methodology. The obtained results infer that optimum values of the degree of sphericity (0.865) and particle size (49.30) are observed for the following set of processing parameters, namely 585°C pouring temperature, 500 mm slope length and 45°slope angle. ANOVA results show that the pouring temperature is the most significant input variables that influence degree of sphericity and particle size followed by slope length and slope angle. The values of output variables obtained from confirmation experiment, performed at 95% confidence level, ensure that they are well within the permissible limits.

Evaluation of the effect of grain refiners on the solidification characteristics of an Sr-modified ADC12 die-casting alloy by cooling curve thermal analysis

The influence of grain refinement—with the addition of 6 mass% Al–5Ti–B and 10 mass% Al–3Ti–B master alloys—on the temperature-based parameters of a commercial ADC12 die-casting alloy, modified with 0.04 mass% Sr, was investigated using computer-aided cooling curve thermal analysis. Results show that the addition of grain refiners caused the reaction area of the aluminium dendrite to shift up. With the addition of refiner reagents, the nucleation temperature and growth temperature for the evolution of the primary Al dendrite increased, while the recalescence temperature decreased. The dendrite coherency temperature (TDCP), time (tDCP), temperature (TN– TDCP), and time (tN–tDCP) interval for dendrite coherency and solid fraction at coherency point increased with the addition of Al–3Ti–B and Al–5Ti–B grain refiners. Nevertheless, the growth temperature of the eutectic aluminium– silicon phase remained at the modified range (563.5–565 C) even after the addition of grain refiners. A grain-refined and modified structure was obtained after the addition of refiners, but no obvious mutual effect was found in terms of the coarsening of grain size or silicon demodification in the range of concentrations used in this study.

Effects of Solidification Range on the Structure of Aluminium Alloys Obtained under Conditions of Constant Melt Flow

Materials Science Forum, 2006

Effects of solidification range on macro- and microstructure of pure aluminium and binary Al–Cu alloys obtained under conditions of constant melt flow are studied experimentally. The solidification range of binary alloys was varied by changing the concentration of the alloying element. An electromagnetic pump with a specially designed melt-guiding system is used to organize controlled unidirectional melt flow along the solidification front. Temperature and melt flow velocity are controlled during the experiment. It is observed that the extent of solidification range changes the macro– and microstructure, affects width and deflection angle of columnar grains, and alters the dendrite arm spacing in the presence of melt flow. The melt flow itself is found to change the macro- and microstructure, e.g. the increase of melt flow velocity clearly decreases the dendrite arm spacing.

THE EFFECT OF MOULD TEMPERATURE AND COOLING CONDITIONS ON THE SIZE OF SECONDARY DENDRITE ARM SPACING IN Al-7Si-3Cu ALLOY

2009

The secondary dendrite arm spacing (SDAS) is one of the most important microstructure features of as-cast structure in hypoeutectic aluminum alloys. The size of SDAS depends on many factors such as liquid metal treatment, temperature gradient, cooling rate/solidification time and chemical composition of melt. Among them the cooling rate/solidification time have dominant impacts. In industrial production of castings, when the chemical composition of melt has been chosen, the cooling conditions will control the solidification process. In this paper the effect of various pre-heating mould temperatures and cooling conditions (with and without water cooling) on the SDAS in AlSi7Cu3 were studied. For that purpose the permanent metal mould with the cooling system incorporated in one die was designed. The solidification time was affected by the mould temperature. It was found that the influence of mould temperature on SDAS was less pronounced in the presence of water cooling. The experiment...