Manufacturing and characterization of a ceramic microcombustor with integrated oxygen storage and release element (original) (raw)

Design and Fabrication of an LTCC Structure for a Microceramic Combustor

Journal of Microelectronics and Electronic Packaging, 2012

Advanced microsystems or macrosystems are in some cases made with multilayer ceramic technology. Low-temperature cofired ceramic (LTCC) technology is considered to be one of the more suitable technologies for the fabrication of ceramic microsystems that integrate screen-printed, thick-film electronic components as well as three-dimensional buried structures, for example, cavities and channels. One of the applications is a ceramic combustor. The chemical energy of the fuel is converted into thermal energy in a chemical microcombustor through a burning process, while the accompanying high temperatures and, frequently, high pressures, impose harsh conditions on the combustor structure. Therefore, the combustor must be carefully designed not only from the functional, thermal, and chemical points of view, but also with respect to the mechanical strength. The combustor device was prepared by lamination of Du Pont 951PX LTCC green tapes. The fabricated 3D LTCC structures with buried caviti...

Realization of a Solid-Propellant based Microthruster using Low Temperature Co-fired Ceramics

2010

The introduction of micro-spacecrafts in the space industry has led to the development of various micro-propulsion techniques. Microthrusters are micropropulsion devices used in a microspacecraft for precise station keeping, orbit adjustment, attitude control, drag compensation and apogee kicking. The principle of operation of a solid propellant thruster is based on the combustion of a solid energetic material stored in a microfabricated chamber. In the current work, Low-Temperature Co-fired Ceramic (LTCC) technology has been used for the realization of a solid propellant based microthruster structure. Hydroxyl Terminated Poly-Butadiene/Ammonium Perchlorate (HTPB/AP) is used as the propellant. It is shown that geometric and dimensional variations in design, depending on the application requirements, can be easily implemented. Preliminary testing for micro-combustion has been done to verify the basic operation of the microthruster. A thrust value of 19.5 mN has been measured.

Fine structuration of low-temperature co-fired ceramic (LTCC) microreactors

Lab on a chip, 2015

The development of microreactors that operate under harsh conditions is always of great interest for many applications. Here we present a microfabrication process based on low-temperature co-fired ceramic (LTCC) technology for producing microreactors which are able to perform chemical processes at elevated temperature (>400 °C) and against concentrated harsh chemicals such as sodium hydroxide, sulfuric acid and hydrochloric acid. Various micro-scale cavities and/or fluidic channels were successfully fabricated in these microreactors using a set of combined and optimized LTCC manufacturing processes. Among them, it has been found that laser micromachining and multi-step low-pressure lamination are particularly critical to the fabrication and quality of these microreactors. Demonstration of LTCC microreactors with various embedded fluidic structures is illustrated with a number of examples, including micro-mixers for studies of exothermic reactions, multiple-injection microreactors...

High Channel Density Ceramic Microchannel Reactor for Syngas Production

Energies, 2020

Solid oxide fuel cells can operate with carbonaceous fuels, such as syngas, biogas, and methane, using either internal or external reforming, and they represent a more efficient alternative to internal combustion engines. In this work, we explore, for the first time, an alumina membrane containing straight, highly packed (461,289 cpsi), parallel channels of a few micrometers (21 µm) in diameter as a microreformer. As a model reaction to test the performance of this membrane, the dry reforming of methane was carried out using nickel metal and a composite nickel/ceria as catalysts. The samples with intact microchannels were more resistant to carbon deposition than those with a powdered sample, highlighting the deactivation mitigation effect of the microchannel structure. The coke content in the microchannel membrane was one order of magnitude lower than in the powder catalyst. Overall, this work is a proof of concept on the use of composite alumina membrane as microchannel reactors fo...