1,3-Stereocontrol with Bromoallenes. Synthesis of N-Boc-ADDA, the Unique Amino Acid Present in Several Inhibitors of Serine/Threonine Phosphatases (original) (raw)

The Journal of Organic Chemistry, 1996

Abstract

... c) MeC CLi, THF, −78 °C, (89%); (d) K-Selectride, THF, −100 °C (72%); (e) BuLi, LiBr, TosCl, THF, then CuBr·DMS, LiBr, −60 °C (75%: 5 and epi-5); (f) MeCuCNLi, THF, −78 °C (76% of 3 and 4% of epi-3); (g) Cp 2 ... First Enantiocontrolled Formal Synthesis of (+)-Neovibsanin B, A ...

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