Free-radical cross-linking copolymerization of methyl methacrylate and ethylene glycol dimethacrylate in the presence of trimethoxyvinylsilane (original) (raw)

Journal of Physics and Chemistry of Solids, 2008

Abstract

Free-radical cross-linking copolymerization of methyl methacrylate (MMA), ethylene glycol dimethacrylate (EGDM), and trimethoxyvinylsilane (TMVS) has been investigated in toluene at a total monomer concentration of 4molL−1 and at 70°C. Conversion of monomer, volume swelling ratio, weight fraction, and gel point were measured as a function of the reaction time, TMVS concentration, toluene content, temperature, and chain transfer agents up to

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