A Convenient Synthesis of O-ETHYL-1-AMINOALKYLPHOSPHINATES (original) (raw)

Phosphorus, Sulfur, and Silicon and the Related Elements, 1993

Abstract

1-Aminoalkylphosphinates 4 have been obtained in good yields in a one-step transformation by the Mitsunobu reaction of 1-hydroxyalkylphosphinates 1 with hydrazoic acid, and subsequent treatment of the intermediate azides 2, with triphenylphosphine, followed by hydrolysis of the iminophosphoranes 3 with water.

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