Synthesis of Titanium and Zirconium Complexes That Contain the Tridentate Diamido Ligand, [(( t Bu d 6 )N- o -C 6 H 4 ) 2 O] 2 - ([NON] 2 - ) and the Living Polymerization of 1Hexene by Activated [NON]ZrMe 2 (original) (raw)

Journal of The American Chemical Society, 1997

Richard Schrock

W. Davis

Abstract

... 13) Cloke, FGN; Hitchcock ... The reaction mixture was stirred for 1 h in a 0 °C bath, and the reaction was quenched by addition of HCl in diethyl ether (4 mL, 1.0 M). Most of the solvent was removed at 15 Torr (water aspirator) and 45 °C. The viscous oil was dried at 100 mTorr at 50 ...

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