Fast magic angle spinning NMR with heteronucleus detection for resonance assignments and structural characterization of fully protonated proteins (original) (raw)

Exclusively heteronuclear NMR experiments to obtain structural and dynamic information on proteins

Roberta Pierattelli

2010

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Efficient resonance assignment of proteins in MAS NMR by simultaneous intra-and inter-residue 3D correlation spectroscopy

Eugenio Daviso

2013

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Solid-State Protein-Structure Determination with Proton-Detected Triple-Resonance 3D Magic-Angle-Spinning NMR Spectroscopy

Donghua Zhou

Angewandte Chemie International Edition, 2007

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A Multidimensional NMR Experiment for Measurement of the Protein Dihedral Angle ψ Based on Cross-Correlated Relaxation between 1Hα−13Cα Dipolar and 13C‘ (Carbonyl) Chemical Shift Anisotropy Mechanisms

Robert Konrat

Journal of the American Chemical Society, 1997

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Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning

Andrew Pell, Moreno Lelli

Journal of the American Chemical Society, 2014

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Backbone Assignment of Fully Protonated Solid Proteins by 1 H Detection and Ultrafast Magic-Angle-Spinning NMR Spectroscopy

Alessandro Marchetti

Angewandte Chemie International Edition, 2012

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13 C-Detected Through-Bond Correlation Experiments for Protein Resonance Assignment by Ultra-Fast MAS Solid-State NMR

Roberta Pierattelli

ChemPhysChem, 2013

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Proton-Detected Solid-State NMR Spectroscopy of Fully Protonated Proteins at 40 kHz Magic-Angle Spinning

Chad Rienstra

Journal of The American Chemical Society, 2007

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Out-and-back 13C–13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS

Andrew Pell

J Biomol NMR, 2013

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Automated NMR determination of protein backbone dihedral angles from cross-correlated spin relaxation

Robert Konrat

Journal of biomolecular NMR, 2002

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13C-detected protonless NMR spectroscopy of proteins in solution

Roberta Pierattelli

2006

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Reduced dimensionality (4,3)D-hnCOCANH experiment: an efficient backbone assignment tool for NMR studies of proteins

Dinesh Kumar

Journal of Structural and Functional Genomics, 2013

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Pseudo 5D HN(C)N Experiment to Facilitate the Assignment of Backbone Resonances in Proteins Exhibiting High Backbone Shift Degeneracy

Himanshu Pandey

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Improved Resolution and Sensitivity of Triple-Resonance NMR Methods for the Structural Analysis of Proteins by Use of a Backbone-Labeling Strategy

Ed Oliver

Journal of the American Chemical Society, 1999

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A 4D HCC(CO)NNH experiment for the correlation of aliphatic side-chain and backbone resonances in 13C/15N-labelled proteins

Peter Domaille

Journal of Biomolecular NMR, 1993

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Multidimensional Magic Angle Spinning NMR Spectroscopy for Site-Resolved Measurement of Proton Chemical Shift Anisotropy in Biological Solids

Alexander Vega

Journal of the American Chemical Society, 2013

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A 3D triple-resonance NMR technique for qualitative measurement of carbonyl-Hβ J couplings in isotopically enriched proteins

G. Marius Clore FRS

Journal of Magnetic Resonance (1969), 1992

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Improved sensitivity in indirect monitoring of chemical shifts of proton-heteronuclear spin pairs (1H-13C and 1H-15N) in 3D and 4D NMR spectroscopy

G. Barbato

Journal of biomolecular NMR, 2001

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A Proton-Detected 4D Solid-State NMR Experiment for Protein Structure Determination

P. Schanda

ChemPhysChem, 2011

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Sequential resonance assignment of medium-sized 15 N/13 C-labeled proteins with projected 4D triple resonance NMR experiments

Bogdan Banecki

Journal of Biomolecular NMR, 1998

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Time-saving methods for heteronuclear multidimensional NMR of (13C, 15N) doubly labeled proteins

R. Kaptein

Journal of Biomolecular NMR, 1994

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TROSY-type Triple-Resonance Experiments for Sequential NMR Assignments of Large Proteins

Hans Senn

Journal of the American Chemical Society, 1999

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Applications of three- and four-dimensional heteronuclear NMR spectroscopy to protein structure determination

G. Marius Clore FRS

Progress in Nuclear Magnetic Resonance Spectroscopy, 1991

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Solid-state NMR triple-resonance backbone assignments in a protein

Ana Carolina Zeri

Journal of Biomolecular Nmr, 1999

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A Dipolar Coupling Based Strategy for Simultaneous Resonance Assignment and Structure Determination of Protein Backbones

Homayoun Valafar

Journal of the American Chemical Society, 2001

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TROSY in triple-resonance experiments: New perspectives for sequential NMR assignment of large proteins

Hans Senn

Proceedings of the National Academy of Sciences, 1998

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Rapid Analysis of Organic Compounds by Proton-Detected Heteronuclear Correlation NMR Spectroscopy with 40 kHz Magic-Angle Spinning

Donghua Zhou

Angewandte Chemie International Edition, 2008

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Complete backbone and DENQ side chain NMR assignments in proteins from a single experiment: implications to structure–function studies

Ramakrishna V Hosur

Journal of Structural and Functional Genomics, 2014

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Three-dimensional triple-resonance NMR of 13C/15N-enriched proteins using constant-time evolution

Robert Powers

Journal of Magnetic Resonance (1969), 1991

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Cross-Correlated Relaxation of Dipolar Coupling and Chemical-Shift Anisotropy in Magic-Angle Spinning R 1ρ NMR Measurements: Application to Protein Backbone Dynamics Measurements

Isabel Ayala

The Journal of Physical Chemistry B, 2016

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The Use of 2H, 13C, 15N Multidimensional NMR to Study the Structure and Dynamics of Proteins

Kevin Gardner

Annual Review of Biophysics and Biomolecular Structure, 1998

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Constant-Time Through-Bond 13C Correlation Spectroscopy for Assigning Protein Resonances with Solid-State NMR Spectroscopy

Ryan Olsen

Journal of the American Chemical Society, 2006

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Assignment of amide proton signals by combined evaluation of HN, NN and HNCA MAS-NMR correlation spectra

Huub de Groot

Journal of biomolecular NMR, 2003

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