Two-step hard X-ray focusing combining Fresnel zone plate and single-bounce ellipsoidal capillary (original) (raw)
2007, Journal of Synchrotron Radiation
A two-step focusing set-up combining a Fresnel zone plate with an ellipsoidal capillary is presented. It is shown that, in addition to the anticipated gain in flux, the employment of the prefocusing micro-optic makes optimal use of the elliptical shape of the capillary by almost eliminating aberrations. A small cross section of the prefocused beam allows a tiny fraction of the capillary surface to be selected, thus reducing the influence of slope errors. An X-ray beam with a 15 keV energy was focused down to a spot size as small as 250 nm, demonstrating the best value that has been achieved up to now for singlebounce capillaries. The use of an ellipsoidal capillary as a micromirror under offaxis illumination by microfocusing optics may open up new opportunities in nanofocusing developments.
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Journal of Synchrotron Radiation, 2007
A two-step focusing set-up combining a Fresnel zone plate with an ellipsoidal capillary is presented. It is shown that, in addition to the anticipated gain in flux, the employment of the prefocusing micro-optic makes optimal use of the elliptical shape of the capillary by almost eliminating aberrations. A small cross section of the prefocused beam allows a tiny fraction of the capillary surface to be selected, thus reducing the influence of slope errors. An X-ray beam with a 15 keV energy was focused down to a spot size as small as 250 nm, demonstrating the best value that has been achieved up to now for singlebounce capillaries. The use of an ellipsoidal capillary as a micromirror under offaxis illumination by microfocusing optics may open up new opportunities in nanofocusing developments.
High-flux hard X-ray microbeam using a single-bounce capillary with doubly focused undulator beam
Journal of Synchrotron Radiation, 2009
A pre-focused X-ray beam at 12 keV and 9 keV has been used to illuminate a single-bounce capillary in order to generate a high-flux X-ray microbeam. The BioCAT undulator X-ray beamline 18ID at the Advanced Photon Source was used to generate the pre-focused beam containing 1.2 Â 10 13 photons s À1 using a sagittal-focusing double-crystal monochromator and a bimorph mirror. The capillary entrance was aligned with the focal point of the pre-focused beam in order to accept the full flux of the undulator beam. Two alignment configurations were tested: (i) where the center of the capillary was aligned with the pre-focused beam ('in-line') and (ii) where one side of the capillary was aligned with the beam ('off-line'). The latter arrangement delivered more flux (3.3 Â 10 12 photons s À1 ) and smaller spot sizes ( 10 mm FWHM in both directions) for a photon flux density of 4.2 Â 10 10 photons s À1 mm À2 . The combination of the beamline main optics with a large-working-distance (approximately 24 mm) capillary used in this experiment makes it suitable for many microprobe fluorescence applications that require a micrometer-size X-ray beam and high flux density. These features are advantageous for biological samples, where typical metal concentrations are in the range of a few ng cm À2 . Micro-XANES experiments are also feasible using this combined optical arrangement.
X-ray microfocusing by polycapillary optics
Advances in X-Ray/EUV Optics and Components III, 2008
In this work the results on X-ray micro-imaging by means of novel polycapillary optical elements will be presented. To simulate various radiation propagation processes in both single capillary and polycapillary systems, a PolyCAD code was developed.
Simple method for focusing x rays using tapered capillaries
Applied Optics, 1988
A new method of focusing x rays is described using appropriately tapered capillaries. The x rays are incident on the inner surface of the capillary below the critical glancing angle and reflect due to total external reflection. By appropriately narrowing the capillary, the x rays can thus be focused in a broad band of energies. The theory of the effect and optimum taper is described. A measurement verifying the focusing capability of the method is presented. The method appears practical for focusing bending magnet synchrotron radiation around 8 keV down to a diameter of 10 um from an initial dimension of 1-mm 2 incident cross section with an attenuation of the total energy of 2, i.e., an increase in the intensity per unit area of 6.5 X 103. Greater focusing is possible with softer x rays and from undulator sources. The wide-ranging applicability of the technique is discussed.
Microspot x-ray focusing using a short focal-length compound refractive lenses
Review of Scientific Instruments, 2004
We have fabricated and tested short focal-length compound refractive lenses (CRLs) composed of microbubbles embedded in epoxy encased in glass capillaries. The interface between the bubbles formed 90 to 350 spherical biconcave microlenses reducing the overall focal length inversely by the number of lenses or bubbles. When compared with CRLs manufactured using other methods, the microbubble lenses have shorter focal lengths with higher transmissions and larger gains for moderate energy x rays (e.g., 7-20 keV). We used beamline 2-3 at the Stanford Synchrotron Radiation Laboratory and beamline 5BM-D-DND at the Advanced Photon Source to measure focal lengths between 100-250 mm with lens apertures varying between 97 and 321 m. Transmission profiles were measured giving, for example, a peak transmission of 46% for a 240 mm focal length CRL at 20 keV. The focal-spot sizes were also measured yielding, for example, a vertical spot size of 1.2 m resulting from an approximate 20-fold demagnification of the APS 23 m source size. The measured gains in intensity over that of unfocused beam were between 9 and 26.
X-ray micro-imaging by capillary optics
2009
In this work the results on X-ray micro-imaging by means of novel polycapillary optical elements will be presented. To simulate various radiation propagation processes in both single capillary and polycapillary systems, a PolyCAD code was developed. The new experimental results on radiation redistribution by novel capillary lenses in comparison with simulated data will be reported. The images of characterized extended samples (~3 mm) were recorded with 6 μm resolution, the maximum provided by CCD. Polycapillary Optics CAD software X-ray tracing Imaging Confocal 02.60.Cb 02.70.-c 41.50. + h 42.15.-i 42.15.Dp 42.30.-d.
Advances in X-Ray/EUV Optics and Components VIII, 2013
Hard x-ray scanning microscopy relies on small and intensive nanobeams. Refractive x-ray lenses are well suited to generate hard x-ray beams with lateral dimensions of 100 nm and below. The diffraction limited beam size of refractive x-ray lenses mainly depends on the focal length and the attenuation inside the lens material. The numerical aperture of refractive lenses scales with the inverse square root of the focal length until it reaches the critical angle of total reflection. We have used nanofocusing refractive x-ray lenses made of silicon to focus hard x-rays at 8 and 20 keV to (sub-)100 nm dimensions. Using ptychographic scanning coherent diffraction imaging we have characterized these nanobeams with high accuracy and sensitivity, measuring the full complex wave field in the focus. This gives access to the full caustic and aberrations of the x-ray optics.
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