The crystal chemistry of Bi6TP2O15+x, T=Fe, Ni, Zn: Isomorphism and polymorphism, structural relationship to Bi6TiP2O16 (original) (raw)

Journal of Solid State Chemistry, 2007

Abstract

The crystal structures of compounds with nominal compositions Bi6FeP2O15+x (I), Bi6NiP2O15+x (II) and Bi6ZnP2O15+x (III) were determined from single-crystal X-ray diffraction data. They are monoclinic, space group I2, Z=2. The lattice parameters for (I) are a=11.2644(7), b=5.4380(3), c=11.1440(5)Å, β=96.154(4)°; for (II) a=11.259(7), b=5.461(4), c=11.109(7)Å, β=96.65(1)°; for (III) a=19.7271(5), b=5.4376(2), c=16.9730(6)Å, β=131.932(1)°. Least squares refinements on F2 converged for (I) to

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