Micro-manufacturing of micro-scale porous surface structures for enhanced heat transfer applications: an experimental process optimization study (original) (raw)

Engineered Porous Materials EXPO ′93

Materials Technology, 1994

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Fabrication of High Aspect Ratio Porous Microfeatures Using Hot Compaction Technique

2008

High aspect ratio porous microfeatures are becoming more important in the modern industry. However, the fabrication of such features under a mass production environment remains a challenge when robustness, cost effectiveness, and high productivity requirements are required. In this study, the forming of such porous microfeatures using hot compaction was investigated. A hot compaction experimental setup was designed and fabricated that is capable of performing high temperature operation (700°C), quick heatup, and avoiding oxidation. 3D thermal simulation of the experimental setup was conducted to investigate the heat transfer performance and internal temperature distribution, which was then used as a reference for the experiment. Hot compaction experiments were carried out, and the effects of compression force and temperature on the quality in terms of powder consolidation strength and porosity were investigated. In addition, the achievable aspect ratio and taper angle were also discussed.

An assessment of the process of Self-propagating High-Temperature Synthesis for the fabrication of porous copper composite

Journal of Alloys and Compounds, 2009

The present article describes the process of Self-propagating High-temperature Synthesis (SHS) that is employed for fabricating open cell copper-alumina composite foam. This foam was fabricated by the reactions between the powders of CuO, Al and C. The gas released during these reactions as well as the initial porosity of the green powder compact were suggested to be the sources of the produced pores. Further, the effect of C content and the precursor compressing pressure on the porosity content and morphology of the SHS product was determined. Optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction (XRD) were utilized to characterize the porous samples. The optimum weight fractions for blending the initial powders were determined to be 84 wt.% CuO, 9.5 wt.% Al, and 6.5 wt.% C, and the SHS reaction was sustainable only if the initial compacting pressure of the powders was between 100 and 300 MPa.

Design, manufacture and testing of porous materials with ordered and random porosity: Application to porous medium burners

Applied Thermal Engineering, 2019

Digital replicas of three types of SiSiC ceramic foams (10, 30, and 60 pores per inch, PPI) were obtained by means of X-ray computed tomography. Equivalent pore diameters were determined using a combination of the 3D Watershed analysis (VG Studio Max software) and an analytical tetrakaidecahedron model of a cellular structure and compared to those provided by the manufacturer. Upon investigation, it was found that pore diameters provided by the manufacturer were underestimated and the discrepancies between them and the CT-measured values were 10% for 10 PPI, 60% for 30 PPI and 120% for 60 PPI specimens. Next, diamond lattice structures equivalent to 10, 30, and 60 PPI foams in terms of their porosity and permeability were designed and some of them 3D-printed from metallic CoCr alloy. A two-section porous medium burner test bench was then used to measure the temperature, pollutant emissions and pressure drop for six different setups containing, in the upstream and downstream sections, different arrangements of the foam and lattice structures made of either ceramic or metal materials. In all the setups, pollutant emissions were low and at the detection limit of the equipment, which agrees with previous research. The application of CoCr alloy in the upstream section was determined to be advantageous, ensuring higher flame stability and structural strength. The diamond lattice was found to be a good candidate for replacement of the foam geometry by providing both the better control of porosity and higher structural stiffness. Further research with ordered porous materials is recommended for a broad range of lean combustion regimes with metallic alloys in the upstream section, and ceramic materials in the downstream section.

High porosity media with directional oriented pores View project

2010

This chapter deals with the concept of graded material and main technologies for their production. The technologies for metallic graded materials are divided into two general groups. A sequence of eighth basic production methods is discussed in more details. I.1 Materials of Graded Structure The idea of Functionally Graded Materials (FGMs) was substantially advanced in the early 1980’s in Japan, where this new material concept was proposed to increase adhesion and minimize the thermal stresses in metallic-ceramic composites developed for reusable rocket engines [1]. Meanwhile, FGMs concepts have triggered world-wide research activity and are applied to metals, ceramics and organic composites to generate improved components with superior physical properties [2]. Depending on the application and the specific loading conditions, varying approaches can be followed to generate the structure gradients. Consequently, coatings have been deposited by different techniques involving physical v...

Fabrication and thermo-mechanical behavior of ultra-fine porous copper

Journal of Material Science, 2014

Porous materials with ligament sizes in the submicrometer to nanometer regime have a high potential for future applications such as catalysts, actuators, or radiation tolerant materials, which require properties like high strength-to-weight ratio, high surface-to-volume ratio, or large interface density as for radiation tolerance. The objective of this work was to manufacture ultra-fine porous copper, to determine the thermo-mechanical properties, and to elucidate the deformation behavior at room as well as elevated temperatures via nanoindentation. The experimental approach for manufacturing the foam structures used high pressure torsion, subsequent heat treatments, and selective dissolution. Nanoindentation at different temperatures was successfully conducted on the ultra-fine porous copper, showing a room temperature hardness of 220 MPa. During high temperature experiments, oxidation of the copper occurred due to the high surface area. A model, taking into account the mechanical ...