Toona sinensis Mediated Green Synthesis of Silver Nanoparticles (original) (raw)

Green Synthesis of Silver Nanoparticles Using Alagaw Leaf Extract

Green Synthesis of Silver Nanoparticles Using Alagaw (Premna odorata) Leaf Extract, 2019

Abstract. There is a worldwide interest in silver nanoparticles (AgNPs) synthesize by various chemical reactions for use in applications. Silver nanoparticles have gained significant interest due to their unique optical, antimicrobial, electrical, physical properties and their possible application. However, it is necessary to develop environmental friendly methods for their syntheses. To avoid chemically toxicity, biosynthesis of metal silver nanoparticles is proposed as a cost-effective and environmental friendly alternative. This study aimed to find out whether Alagaw plant can potentially act as a reducing agent for the biosynthesis of silver nanoparticles and whether the concentration of the leaf extract can affect the absorbance spectrum, size and shape of the synthesized silver nanoparticles. The synthesized silver nanoparticles were characterized using the UV-vis spectroscopy for its absorbance spectrum and Transmission Electron Microscope Analysis for its morphology and size. The experimental method of research was used using three treatments and replicates of the different concentrations of Alagaw leaf extract: Treatment A (0.2 g/mL), Treatment B (0.4 g/mL) and Treatment C (0.6 g/mL) with 10 minutes and 60 minutes interval of observation under UV-vis spectrophotometer. Based on the findings of the study, Alagaw plant can potentially act as a good reducing agent for the biosynthesis of silver nanoparticles. The results recorded from UV-vis spectrophotometer support the biosynthesis and characterization of silver nanoparticles that as the concentration of the leaf extract increases it significantly affect the wavelength peaks and absorbance peaks of the synthesized silver nanoparticles. Using the high-resolution Transmission Electron Microscopy, the size of silver nanoparticles measured 50 nm – 100 nm having near-spherical in shape. Keywords: Nanoparticles, Biosynthesis, Spectroscopy, Absorbance Spectrum

Silver Nanoparticles Ecofriendly Green Synthesis by Using Two Medicinal Plant Extract

TJPRC, 2013

Nanotechnology in present era gaining value due to capability of modulating metals in to their nanoparticles. There are few studies which are paying attention on the effects and mechanisms of nanomaterials on plants. The present research prominence on the biological synthesis of silver nanoparticle using herbal extract a natural biopolymer, acting as a reducing and stabilizing agent. In green synthesis we used natural reducing agents to synthesize nanoparticles (in this case silver nanoparticles). The leaves were found to be a good reducing as well as capping agent which can rapidly reduces silver ions (Ag+ to Ag). The characteristic color changes from pale yellow to dark brown in the reaction due to their specific properties (Surface Plasmon Resonance). Characterization of newly synthesized silver nanoparticle was made using UV – Visible spectroscopic technique. The UV-Vis spectrum of green synthesized silver nanoparticle from Jasminum grandiflorum and Cymbopogon citrullus have maximum absorbance peaks at 206.50 and 199.00 respectively. This study focus on a cost efficient ecofriendly and safe technique for the synthesis of silver nanoparticle using leaves of important medicinal plants.

Biosynthesis of silver nanoparticles using Rice grass (Oryza sativa) aqueous leaf extract

Journal of Current Pharma Research

The wide-scale application of silver nanoparticles (AgNPs) in areas such as nanomedicine, and environmental cleaning has led to their increased demand. Chemical methods of AgNPs synthesis involve the use of toxic reagents and solvents. The present study reports a green method where silver nanoparticles are synthesized using aqueous extract of rice grass (Oryza sativa) from aqueous silver nitrate solution. To identify the compounds present in the plant extract which is responsible for reduction of silver ions, the functional groups present in plant extract were investigated by FTIR. The techniques used to characterize synthesized nanoparticles are XRD analysis, FTIR and UV-visible spectrophotometer. UV-Visible spectrophotometer showed absorbance peak in range of 359nm-457nm.

Role of Synthetic Plant Extracts on the Production of Silver-Derived Nanoparticles

Plants

The main antioxidants present in plant extracts—quercetin, β-carotene, gallic acid, ascorbic acid, hydroxybenzoic acid, caffeic acid, catechin and scopoletin—are able to synthesize silver nanoparticles when reacting with a Ag NO3 solution. The UV-visible absorption spectrum recorded with most of the antioxidants shows the characteristic surface plasmon resonance band of silver nanoparticles. Nanoparticles synthesised with ascorbic, hydroxybenzoic, caffeic, and gallic acids and scopoletin are spherical. Nanoparticles synthesised with quercetin are grouped together to form micellar structures. Nanoparticles synthesised by β-carotene, were triangular and polyhedral forms with truncated corners. Pentagonal nanoparticles were synthesized with catechin. We used Fourier-transform infrared spectroscopy to check that the biomolecules coat the synthesised silver nanoparticles. X-ray powder diffractograms showed the presence of silver, AgO, Ag2O, Ag3O4 and Ag2O3. Rod-like structures were obtai...

A review on green synthesis of silver nanoparticle through plant extract and its medicinal applications

2020

Department of Chemistry, Kalinga University, Naya Raipur-492 101, Chhattisgarh, India<br> Department of Chemistry, Rungta College of Engineering & Technology, Bhilai-490 024, Chhattisgarh, India<br> Department of Chemical Engineering, National Institute of Technology Raipur, Raipur-492 010, Chhattisgarh, India<br> E-mail: dr.manisha.agrawal@rungta.ac.in<br> Manuscript received online 30 March 2020, accepted 01 June 2020 Silver nanoparticles (AgNPs) are gaining attention because of its wide application in medical science as antimicrobial and<br> antibacterial properties. A conventional method for synthesis of AgNPs consumes hazardous chemicals and during production<br> of NPs harmful by-products may also form. Proposed review suggests "greener technology" for synthesis of silver<br> nanoparticles with the help of easily available plants. Aqueous extract of leaf or roots of Impatiens balsamina, Lantana camara,<br> Eriobotrya ja...

Green Synthesis of Silver Nanoparticles Using Alagaw (Premna odorata) Leaf Extract

2021

There is a worldwide interest in silver nanoparticles (AgNPs) synthesize by various chemical reactions for use in applications. Silver nanoparticles have gained significant interest due to their unique optical, antimicrobial, electrical, physical properties and their possible application. However, it is necessary to develop environmental friendly methods for their syntheses. To avoid chemically toxicity, biosynthesis of metal silver nanoparticles is proposed as a cost-effective and environmental friendly alternative. This study aimed to find out whether Alagaw plant can potentially act as a reducing agent for the biosynthesis of silver nanoparticles and whether the concentration of the leaf extract can affect the absorbance spectrum, size and shape of the synthesized silver nanoparticles. The synthesized silver nanoparticles were characterized using the UV-vis spectroscopy for its absorbance spectrum and Transmission Electron Microscope Analysis for its morphology and size. The expe...

Influence of Different Plants Extracts on Silver Nanopar ticles Green Synthesis

Archives of Metallurgy and Materials, 2019

Three plants extracts were used for biosynthesis of Ag nanoparticles (AgNPs). AgNPs nucleation process requires effective reduction agents which secure Ag+ to Ag0 reduction and also stabilizing/capping agents. The UV-vis and TEM observation revealed that the best results were obtained by R. officinalis leaf extract. The strong SPR band peak appeared at the wavelength 418 nm. Synthetized AgNPs were globular, fine (~20 nm), uniform and stabile throughout the experiment. A rapid rate of AgNPs synthesis was also significant and economically advantageous factor. Fine (10-20 nm) and globular nanoparticles were synthetized also by U. dioica leaf extract, but the stability of nanoparticles was not permanent. Despite V. vitis-idaea fruit extract contains a lot of reducing agents, UV-vis did not confirm the presence of AgNPs in solution. Synthetized Ag particles were very unstable, Ag particles agglomerated very fast and clearly indicated sediment was formed.

Green Synthesis of Silver Nanoparticles Using Some Medicinal Plants

International Research Journal of Pure and Applied Chemistry

Aims: The green synthesis of silver nanoparticles in an eco-friendly, economical and more effective approach using (Acacia cyanophylla, Phlomis syriaca and Scolymus hispanicus) plants extracts and describing their main chemical properties and study the effect of its chemical composition on producing silver nanoparticles. Methodology: In this study, aqueous and ethanolic extracts of the three plants were evaluated for antioxidant activity using 2,2-diphenyl-l-picrylhydrazyl (DPPH) assay, Total polyphenol and flavonoid contents were determined using spectrophotometric method, but total saponins were determined by weight method, The synthesis of silver nanoparticles was performed by a reduction method using aqueous silver nitrate solution and aqueous extracts of the three plants. Then study its characterization in a number of ways, such as visual inspection, UV-Vis spectroscopy and dynamic light scattering. Results: The results showed that the total phenolic content ranged in extracts...

Green synthesis of silver nanoparticles using plant extracts

Proceedings of The 4th International Virtual Conference on Advanced Scientific Results, 2016

The use of silver nanoparticles in the field of nanomedicine is keeping pace and innovating with the ever expanding horizon of Nanobiotechnology. Ipomea species is widely cultivated and use for different purposes, such as, nutritional, medicinal, ritual and agricultural. The present study deals with the synthesis and characterization of silver nanoparticles using methonolic extract of Ipomoea indica flowers. UV-visible spectroscopy studies were carried out to assess the formation silver nanoparticles. The formation of Ag-NPs was confirmed by Scanning Electron Microscopy (SEM) and X-Ray Diffraction (XRD) studies. SEM image revealed that silver nanoparticles are quite polydispersed, the size ranging from 10nm to 50nm. The formation of crystalline silver nanoparticles was confirmed using X-ray diffraction analysis. Extracellular synthesis of Ag nanoparticles using dried biomass appears to be cost effective, eco-friendly to that of conventional methods of nanoparticles synthesis.

Biosynthesis of silver nanoparticles by plants crude extracts and their characterization using UV, XRD, TEM and EDX

Plant extract are very cost effective and eco-friendly, thus can be an economic and efficient alternate for the large-scale synthesis of nanoparticles. The preparation of stable, uniform silver nanoparticles by reduction of silver ions with Emblica officinalis, Terminalia catappa and Eucalyptus hybrida extract is reported in the present paper. It is a simple process of global research interest for obtaining silver nanoparticles in least amount of time. These nanoparticles were characterized with UV-Vis spectroscopy, X-ray diffraction (XRD), transmission electron microscopy (TEM) and energy different X- ray (EDX) analysis which revealed that the silver nanoparticles are polydisperse and of different morphologies ranging from 20 to 80 nm in size. XRD results reveal that these nanostructures exhibits a face-centered cubic crystal structure. The UV/Vis spectra absorption peak confirms their production. Pioneering of reliable and eco-friendly process for synthesis of metallic nanoparticles biologically is an important step in the field of application of nanobiotechnology. Thus, these silver nanoparticles (Ag-NPs) may prove as a better candidate for drugs and can potentially eliminate the problem of chemical agents because of their biogenic nature. The indiscriminate use of antibiotics has fueled the development of drug resistance at an alarming rate. To overpower this burning problem, the AgNPs may prove to be a universal solution.