One-pot self-assembly of sisal-like TiO 2 on graphene-like carbon sheets via a novel two-phase interface-facilitated route (original) (raw)

2018, Journal of Alloys and Compounds

A Sisal-Like TiO 2 /Graphene-Like Carbon Sheets (SL-TiO 2 /GLCSs) composite was fabricated via a facile one-pot self-assembling route at a two-phase interface. The ingenious P123 was introduced to serve a dual function of carbon precursor and structure-directing agent, which first assembled at the water/oil interfaces and subsequently was in situ carbonized to GLCSs. Then the sisal-like TiO 2 grew gradually on the GLCSs along the preferred direction. This process shows several advantages such as simple processes, mild condition, low cost and good combination of SL-TiO 2 and GLCSs. The combination of SL-TiO 2 with GLCSs significantly helps the adsorption of substrates as well as promotes electron-hole pair separation, exhibiting good photocatalytic activity towards degradation of methylene blue (MB) compared to the pristine SL-TiO 2 and commercial P25. This strategy opens up new perspectives for fabricating novel composites of nanooxides/GLCSs.

Reduced graphene oxide-TiO2 nanocomposite as a promising visible-light-active photocatalyst for the conversion of carbon dioxide

Nanoscale Research Letters, 2013

Photocatalytic reduction of carbon dioxide (CO2) into hydrocarbon fuels such as methane is an attractive strategy for simultaneously harvesting solar energy and capturing this major greenhouse gas. Incessant research interest has been devoted to preparing graphene-based semiconductor nanocomposites as photocatalysts for a variety of applications. In this work, reduced graphene oxide (rGO)-TiO2 hybrid nanocrystals were fabricated through a novel and simple solvothermal synthetic route. Anatase TiO2 particles with an average diameter of 12 nm were uniformly dispersed on the rGO sheet. Slow hydrolysis reaction was successfully attained through the use of ethylene glycol and acetic acid mixed solvents coupled with an additional cooling step. The prepared rGO-TiO2 nanocomposites exhibited superior photocatalytic activity (0.135 μmol gcat −1 h−1) in the reduction of CO2 over graphite oxide and pure anatase. The intimate contact between TiO2 and rGO was proposed to accelerate the transfer ...

One pot environmental friendly nanocomposite synthesis of novel TiO 2 -nanotubes on graphene sheets as effective photocatalyst

A nanocomposite synthesis of TiO 2 NT-graphene was prepared from titanium dioxide nanotubes and graphene oxide (GO) by a simple environmental friendly method (green method). The structure, surface morphology and chemical composition were characterized by Fourier-transform infrared spectroscopy (FT-IR), X-ray diffract meter (XRD), Raman, energy dispersive X-ray spectrometer (EDS), transmission electron microscopy (TEM), and selected area electron diffraction(SAED). XRD results confirm the interaction of TiO 2-NT with graphene. A fast decomposition of the phenol was observed with a degradation efficiency of 70.6% within 180 min.

Structure and photocatalytic properties of TiO2-Graphene Oxide intercalated composite

Chinese Science Bulletin, 2011

TiO2-Graphene Oxide intercalated composite (TiO2-Graphene Oxide) has been successfully prepared at low temperature (80°C) with graphite oxide (GO) and titanium sulfate (Ti(SO4)2) as initial reactants. GO was firstly exfoliated by NaOH and formed single and multi-layered graphite oxide mixture which can be defined as graphene oxide, [TiO]2+ induced by the hydrolysis of Ti(SO4)2 diffused into graphene oxide interlayer by electrostatic

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