Influence of Lead Nitrate on Sulfurizing Flotation of a Copper-Cobalt Oxide Ore (original) (raw)

2021, Walailak Journal of Science and Technology

Copper-cobalt oxide ores contain several minerals that are economically treatable by concentration techniques. The most used technique is froth flotation in which selective reagents are used to recover more valuables. It is, therefore, important to examine the optimal doses of those reagents while investigating the behaviors of minerals at the same time. This study explored the influence of lead nitrate Pb(NO 3) 2 on the froth flotation of oxide ore to increase valuable metals recoveries. Four factors were investigated including Pb(NO 3) 2 dosage, its conditioning, its addition dose in the 2 nd fraction, and sulfidiser dosage. Other parameters were kept constant. The optimum was found at 25 g/t of Pb(NO 3) 2 , conditioning together with sodium silicate (Na 2 SiO 3) for 5 min, the addition of 5 g/t of Pb(NO 3) 2 in the 2 nd fraction, and 3,000 g/t of sulfidiser. Recoveries in concentrates were 79.51 % Copper (Cu) and 60.27 % Cobalt (Co), with grades of 9.49 and 0.67 %, respectively. The conclusion was that the use of Pb(NO 3) 2 can considerably improve copper and cobalt recoveries.

Optimization of Flotation of the Qaleh Zari Mine Oxidized Copper Ore Sample by the Sequential Sulfidation Approach Using the Response Surface Method Technique

Rudarsko-geološko-naftni zbornik

One of the main challenges in the copper oxide processing industry is the application of flotation to reduce operating costs. Sulfidation-flotation is a commonly employed approach for floating oxide minerals using sulfidizers in order to sulfide the mineral’s surface. In this research work, an oxidized sample from the Qaleh Zari copper mine was used which was a high grade with 5.4% of copper (malachite and azurite). The prepared sample was subjected to mineralogical studies, and the obtained results indicated that the sample was oxidized. Malachite and azurite were the predominant minerals of copper oxide, and the predominant waste minerals were quartz and iron oxides (hematite and magnetite). The addition of sodium sulfide and flotation in four consecutive steps was a successful approach to meet the proper recovery and grade. Sodium sulfide, amyl potassium xanthate, sodium sulfide preparation time, and pH were selected as operating parameters using a central composite design (CCD)....

Flotation of Aladagˇoxide lead–zinc ores

Oxide lead–zinc ore sample containing 10.17% Pb, 10.98% Zn, 57 g/t Ag and 164 g/t Cd was subjected to this experimental study and taken from Kayseri located in the foothills of the Aladag ˘ Mountains, Turkey. Preliminary flotation tests with the ore sample indicated that there was no selectivity in terms of zinc recovery; therefore studies were concentrated on producing lead concentrates. In the experiments, the effects of different parameters such as number of stages, amount of Na 2 S, amount of ZnSO 4 and application of gravity concentration prior to flotation were investigated in relation to the metal contents of concentrates and flotation efficien-cies. A lead concentrate with 65.42% Pb was produced with 77% recovery as a result of six stage flotation experiment carried out with 350 g/t KAX, 250 g/t Aero 407 and 4500 g/t Na 2 S and 98.7% of zinc remained in the tailings with 12.23% Zn content. As a result of gravity concentration followed by flotation, a lead concentrate with an average Pb content of 65.80% was produced with 86.5% total Pb recovery. In both cases almost all zinc remained in the tailings and could not be recovered by the addition of different reagents due to its complicated mineralogical structure. Therefore, application of metallurgical processes is proposed for zinc recovery from the tailings.

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