N -(2-Nitrophenylcarbamothioyl)acetamide (original) (raw)

The compound N-(2-Nitrophenylcarbamothioyl)acetamide has been synthesized and characterized. Structural analysis reveals a dihedral angle of 54.82° between the benzene ring and the N-carbamothioylacetamide unit. Intramolecular and intermolecular hydrogen bonding contributes to the stability of the crystal structure, with the formation of dimeric units linked via N-H•••S interactions. Data collection was performed using APEX2 and refinement through SHELXL97, supporting the compound's formation and interaction motifs.