C Dating of Balearic Lime Burials (original) (raw)
Related papers
AMS 14C dating of Balearic Lime-Burials
2011
The Balearic quicklime burials of the Iron Age have been radiocarbon dated. Because the bones found are unsuitable for dating, lime was dated using the titration method, with results indicating that in some samples there is still fossil limestone carbonate present, while other samples suffered from recarbonation. Nevertheless, 14 C dates on lime and organic matter agree when both are present. The titration method allows calculating a consensus value.
Radiocarbon, 2015
Lime burials are a characteristic phenomenon of the protohistoric funerary tradition on the Balearic Islands. At Cova de Na Dent, six samples, representing the entire stratigraphy of the lime burial, were taken for analysis. The radiocarbon dates suggested that the lowest levels of the burial were Late Bronze Age. This is in contradiction with the general belief that the lime burials are a late Iron Age phenomenon. Therefore, a new analysis strategy is put forward, focusing on the so-called 1st fraction, the first CO2 released during the acid lime reaction, which is supposed to be free of fossil carbon. The analysis demonstrates the impossibility to eliminate the fossil carbon fraction completely. This is probably due to the different geological formation of the local limestone deposits (ancient reef barriers) compared to the previous lime burials of Mallorca all coming from mountain areas. 14C analysis from a cremation layer without lime at the onset of the lime burial reveals an I...
Lime burials are a characteristic phenomenon of the protohistoric funerary tradition on the Balearic Islands. At Cova de Na Dent, six samples, representing the entire stratigraphy of the lime burial, were taken for analysis. The radio-carbon dates suggested that the lowest levels of the burial were Late Bronze Age. This is in contradiction with the general belief that the lime burials are a late Iron Age phenomenon. Therefore, a new analysis strategy is put forward, focusing on the so-called 1st fraction, the first CO 2 released during the acid lime reaction, which is supposed to be free of fossil carbon. The analysis demonstrates the impossibility to eliminate the fossil carbon fraction completely. This is probably due to the different geological formation of the local limestone deposits (ancient reef barriers) compared to the previous lime burials of Mallorca all coming from mountain areas. 14 C analysis from a cremation layer without lime at the onset of the lime burial reveals an Iron Age origin of the Cova de Na Dent lime burial.
Radiocarbon dating of the Son Pellisser lime burial (Calvià, Mallorca
The chronology of the Balearic lime burials has been under debate for many years. It has been unclear for a long time when the interments in lime burials came in use during the Iron Age also called the Talayotic period on the Balearic Islands. Different opinions exist, some archaeologists define the entire Iron Age as the Talayotic period, some include also the late Bronze Age in this cultural period. Still others call the middle and Late Iron Age the Post-Talayotic period. In spite of the Hallstatt plateau in the calibration curve the radiocarbon dates of the Son Pellisser lime burial have demonstrated very clearly that the lime burial started most probably around 780 BCE and at least before 550 BCE, rejecting the hypothesis of a Late Iron Age phenomenon. Furthermore, the analysis of the bones confirmed the earlier observations that the Balearic lime burials were the result of a special type of cremation involving the use of fine crushed limestone during the Iron Age.
14C Dating and Material Analysis of the Lime Burial of Cova de Na Dent (Mallorca, Spain)
Lime burials are a characteristic phenomenon of the protohistoric funerary tradition on the Balearic Islands. At Cova de Na Dent, a lime burial has been sampled for analysis. The lime burial was made up of lime and fragmented bones. Six layers were sampled and described in the laboratory according to their color, the consistency of the deposition, and the aspect and quantity of the bone fragments. Bone samples and lime were dated. The lime was analyzed by using petrographic analysis, X-ray diffraction, FTIR spectroscopy, and simultaneous thermal analysis. The results show that the bones were cremated in the presence of crushed rock carbonate. The 14 C dates on the lime suggest an earlier chronology for this ritual, starting in the Bronze Age, as generally is accepted.
2012
This paper describes a method for effective separation of the pure binder fraction of lime mortars for reliable radiocarbon dating. The methodology allows removal of the detrital carbonate fraction and the unburnt limestone particles, obtaining particles of under 1 µm. The extracted fraction ensured that all carbonate has been generated by slaked lime carbonation. Consequently, the measured carbon corresponds to atmospheric carbon. The proposed method allows to obtain pure datable binder, simplifying considerably the performance of radiometric measurements because dating other grain-size fraction is unnecessary. In order to prove the effectiveness of binder refining, the extraction method has been applied to 5 lime mortars of different archaeological periods from the perimeter walls of Santa María la Real parish church (Zarautz, northern Spain).
Radiocarbon, 2012
"This paper describes a method for effective separation of the pure binder fraction of lime mortars for reliable radiocarbon dating. The methodology allows removal of the detrital carbonate fraction and the unburnt limestone particles, obtaining particles of under 1 μm. The extracted fraction ensured that all carbonate has been generated by slaked lime carbonation. Consequently, the measured carbon corresponds to atmospheric carbon. The proposed method allows to obtain pure datable binder, simplifying considerably the performance of radiometric measurements because dating other grain-size fraction is unnecessary. In order to prove the effectiveness of binder refining, the extraction method has been applied to 5 lime mortars of different archaeological periods from the perimeter walls of Santa María la Real parish church (Zarautz, northern Spain"
Centre for Isotopic Research on Cultural and Environmental heritage (CIRCE) has, recently, obtained some promising results in testing the feasibility of mortar radiocarbon dating by means of an ad hoc developed purification procedure (CryoSoniC: Cryobraking, Sonication, Centrifugation) applied to a series of laboratory mortars. Observed results encouraged CryoSoniC accuracy evaluation on genuine mortars sampled from archeological sites of known or independently constrained age (i.e., other 14C dates on different materials). In this study, some 14C measurements performed on genuine mortars will be discussed and compared with independently estimated (i.e., radiocarbon/archaeometrical dating) absolute chronologies of two Spanish sites. Observed results confirm the agreement of the CryoSoniC mortar dates with the archaeological expectations for both examined cases. Several authors reported the possibility of obtaining accurate radiocarbon dates of mortar matrices by analyzing lime lumps: binder-related particles of different sizes exclusively composed of calcium carbonate. In this paper, preliminary data for the absolute chronology reconstruction of the Basilica of the cemetery complex of Ponte della Lama (Canosa di Puglia, Italy) based on lime lumps will also be discussed. Dating accuracy will be quantified by comparing 14C data on mortar lime lumps from a funerary inscription of known age found near the Basilica, in the same study site. For this site, a comparison between absolute chronologies performed by bulk and CryoSoniC purified lime lumps, and charcoal incased in mortars (when found) will also be discussed. Observed results for this site provide evidence of how bulk lime lump dating may introduce systematic overestimations of the analyzed sample while CryoSoniC purification allows accurate dating.