Archeomagnetic results on three First Iron Age salt-kilns from Moyenvic (France (original) (raw)
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Archaeomagnetic results on three Early Iron Age salt-kilns from Moyenvic (France
Geophysical Journal International, 2011
Variations of the Earth's magnetic field during the first millennium BC in western Europe remain poorly constrained, especially archaeointensity changes. Three salt-kilns (MOA, MOB and MOC) sampled in Moyenvic (Lorraine, eastern France) have been studied to provide new reference data. Each kiln has been dated by radiocarbon to originate from the Early Iron Age or Hallstatt period (between VIII and Vth Century BC). Rock magnetic experiments and hysteresis results suggest the predominance of pseudo-single domain (PSD) Ti-poor magnetite. Archaeomagnetic directions obtained by thermal and alternating field demagnetizations have high mean inclination (close to 70°) and declination (between 19 and 31°). A first set of classical Thellier-Thellier experiments was conducted on 46 samples with a laboratory field almost parallel to the direction of the characteristic remanent magnetization (ChRM). Only 24 of these specimens present a linear NRM-TRM plot. For other specimens, NRM-TRM plots are concave-up with positive pTRM checks. The very large dispersion observed between the determined palaeointensity values suggests some artefacts have not been fully recognized. A second set of Thellier experiments was conducted on 34 sister specimens with the laboratory field applied quasi-perpendicular to the ChRM. In these cases, mineralogical evolutions during heating and chemical remanent magnetization acquisitions have been clearly recognized, despite positive pTRM checks. The concave-up shapes of NRM-TRM plots appear mainly due to mineralogical alteration rather than to the presence of PSD-MD grains. For the entire set of samples the success rate of the palaeointensity determinations is very low with 80 per cent of the samples rejected. Nevertheless, reliable mean archaeointensities have been obtained for two of the three kilns (MOA, 80.1 ± 14.5 μT and MOB, 86.6 ± 6.9 μT at the latitude of Paris). The high field strength and the archaeomagnetic directions determined, combined with previous published data, provide further evidence for important changes of the Earth magnetic field in Europe during the first half of the first millennium BC. These large variations of the geomagnetic field during the Iron Ages indicate that archaeomagnetism is highly suitable for dating of structures from this period.
Archaeomagnetic dating of a High Middle Age likely iron working site in Corroy-le-Grand (Belgium)
Physics and Chemistry of The Earth, 2008
Archaeological burnt materials and structures provide unique records of direction and intensity of the Earth’s magnetic field in the past, elements that can be absolutely determined applying the archaeomagnetic method. At present, such records within Europe are irregular in both space and time. Presented here is the archaeomagnetic investigation of three kilns that were discovered during a preventive excavation of an archaeological site considered of High Middle Age in Corroy-le-Grand (Belgium) and that are assumed to be related to iron working activities. Archaeological context dating points to kiln operation between the second half of the 10th century until the 12th century AD. As the site is not far from Paris, declination and inclination of the characteristic remanent magnetisation of the kilns were compared with the standard directional secular variation curve for France in order to propose archaeomagnetic dates for the cessation of kiln operation by using probability densities [Lanos, Ph., 2004. Bayesian inference of calibration curves, application to archaeomagnetism. In: Buck, C.E., Millard, A.R. (Eds.), Tools for Constructing Chronologies: Crossing Disciplinary Boundaries. Lecture Notes in Statistics. Springer Verlag, London, pp. 43–82; Lanos, Ph., Le Goff, M., Kovacheva, M., Schnepp, E., 2005. Hierarchical modelling of archaeomagnetic data and curve estimation by moving average technique. Geophysical Journal International 160 (2), 440–476]. This confirms the presumed archaeological age and resulted in more precise time constraints for the last kiln operation. Rock magnetic techniques, proposed by Spassov and Hus [Spassov, S., Hus, J., 2006. Estimating baking temperatures in a Roman pottery kiln by rock magnetic properties: implications of thermochemical alteration for archaeointensity determinations. Geophysical Journal International 167, 592–604], were applied to examine the suitability of the burnt materials from the kilns for archaeointensity determinations and to increase the success rate of the Thellier–Thellier double heating technique. An average value for the field intensity of 69.4 ± 2.5 μT was estimated from 10 specimens from a single kiln, which corresponds reasonably well with published data for Western Europe.
Archeomagnetic study of seven contemporaneous kilns from Murcia (Spain)
Physics of the Earth and Planetary Interiors, 2006
New archeointensity values have been determined from seven Spanish kilns sampled at the same archeological site and dated by archeological constraints as between 1100 and 1200 a.d. The directions of the characteristic remanent magnetization and paleointensities have been obtained from classical Thellier experiments conducted on 69 samples collected from the walls of the kilns. Thermoremanent magnetization (TRM) anisotropy and the cooling rate effect upon TRM intensity acquisition have been investigated in all the samples. Differences between mean archeointensities per site, before and after corrections for cooling rate are between 3 and 17%. The study of these seven "contemporaneous" kilns coming from the same archeological site and treated in the same way in the laboratory allows us to discuss the different factors that can cause the dispersion between sites generally observed in archeointensity studies. The results confirm, on one hand, the need for cooling rate corrections in this kind of study and, on the other hand, the need to obtain several archeointensity determinations per century in order to construct a reliable archeointensity curve. Finally, the new data provide a robust mean intensity (60.3 ± 3.3 T at the latitude of Paris) for the middle of the XII century in Western Europe and constrain better the evolution of the geomagnetic field intensity during medieval times in this area.
Validity of archaeomagnetic field recording: an experimental pottery kiln at Coppengrave, Germany
Geophysical Journal International, 2016
Palaeomagnetic data obtained from archaeological materials are used for reconstructions of the Earth's magnetic field of the past millennia. While many studies tested the reliability of this recorder for palaeointensity only a few studies did this for direction. The study presents an archaeomagnetic and rock magnetic investigation applied to an experimental pottery kiln, which was operated in 2003 to produce stone ware. This kind of high-quality pottery needs a temperature of at least 1160 • C. Shortly before heating of the kiln direct absolute measurements of the absolute geomagnetic field vector have been carried out close to it. After cooling of the kiln 24 oriented palaeomagnetic samples have been taken. Although Curie temperatures are about 580 • C, that is the typical temperature for magnetite, thermal as well as alternating field demagnetisations reveal also a considerable amount of hematite as magnetic carrier. This mixture of magnetite and hematite is dominated by pseudo-single domain grains. Demagnetisation removed in some cases weak secondary components, but in most cases the specimens carried a single component thermoremanent magnetisation. The mean characteristic remanent magnetisation direction agrees on 95 per cent confidence level with the directly measured field direction. Archaeointensity was obtained from five specimens with the Thellier-Coe method and with the multiple-specimen palaeointensity domain-state corrected method. Six of these specimens also provided a result of the Dekkers-Böhnel method, which overestimated the archaeointensity by about 9 per cent compared to the direct value, while after correction for fraction the value agrees very well. For the multiple-specimen palaeointensity domain-state corrected method only fractions between 25 and 75 per cent have been used and specimens showing alteration have been excluded. Above 450 • C many specimens showed alteration of the magnetic grains. Because median destructive temperatures were often above this value in most cases the fraction was less than 50 per cent. Nevertheless the obtained intensity (48.48 ± 0.24 µ) is on 95 per cent confidence level in agreement with the direct observation. Behaviour of the specimens during the Thellier-experiments was not ideal because of narrow unblocking temperature spectra and alteration. Nevertheless, the obtained mean archaeointensity is also in agreement with the direct field observation. Here the relative palaeointensity error is about 6 per cent and very high compared the multiple-specimen palaeointensity domain-state corrected method. The investigation demonstrates that a pottery kiln can provide a very precise estimate of the ancient geomagnetic field vector.
New archeomagnetic secular variation data from Central Europe, II: Intensities
Physics of the Earth and Planetary Interiors, 2020
Variations of the geomagnetic field during the past millennia can be obtained by investigating archeological material. The spatial distribution of the available data across Europe is rather uneven and only about 15% of the sites provide a full vector record of the geomagnetic field. Here we report 39 new reliable paleointensity data for sites from Austria, Germany and Switzerland, with ages ranging between 1500 BCE and 1900 CE. For 31 of them, directional information is available, too. Paleointensities were determined with Thellier type techniques, with the multiple-specimen domain-state corrected paleointensity protocol or with both techniques. Corrections for anisotropy of thermoremanent magnetization were carried out for the structures, showing small variations of only a few per cent in most cases. Cooling rate dependence was tested for 16 structures. Often strong alteration during the experiments was observed. Seven successful cooling rate corrections were applied, which lowered the paleointensity values by about 10%. Values obtained from the multiple-specimen technique are generally somewhat lower than those from the Thellier experiments. Rock magnetic measurements revealed magnetitetype minerals mostly in pseudo single domain range as main magnetic carrier, but also high coercive mineral components like hematite or epsilon iron oxide are present. The new data are mostly in good agreement with published paleointensities. They support the presence of strong intensity variations around 800 CE and in the millennium BCE. The new full vector data reveal that the deep paleointensity minimum observed from German data around 850 BCE is accompanied by large variations in direction with declinations up to 50 • .
Geophysical Journal International, 2006
The archaeological site near Eisenerz in Upper Styria (Austria) called the Copper Smelting Site S1, was used for copper smelting in the Middle Bronze Age (15th-13th century BC). The dating of the site is based on pottery finds and has been confirmed by radiocarbon dating. Samples of several roasting hearths and furnaces have been collected and consolidated in order to investigate the spatial distribution and the stability of the magnetization of these materials. Around 500 specimens have been obtained for which the natural remanent magnetization (NRM) and the magnetic susceptibility have been measured with a 2G Squid cryogenic magnetometer and a GEOFYZIKA KLY-2 susceptibility meter, respectively.
Physics of the Earth and Planetary Interiors, 2021
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Journal of Geophysical Research, 2008
Archeomagnetic studies on 14 kilns, a group of jar fragments, and a collection of baked bricks dated between 1000 and 1959 AD plus one Roman pottery kiln have been conducted in order to obtain high-quality archeointensity data to enhance the western European database. The Thellier method with corrections for anisotropy of thermoremanent magnetization (TRM) and for cooling rate dependence upon TRM acquisition was used. The effect of TRM anisotropy is only important for the bricks where the corrected and uncorrected mean intensities differ by more than 5%. Cooling rate correction factors determined per sample are up to 15% and per site up to 7.7%. Our 17 new data together with 62 previously published results were used to obtain, by Bayesian modeling, the geomagnetic field intensity over the past two millennia for western Europe. Our results indicate that geomagnetic intensity remained more or less constant between the 1st and 4th centuries and between the 14th and 16th centuries (mean values, at Paris, around 65 and 57 mT, respectively), whereas an important decrease occurs between 1600 and 1800 AD. The detailed evolution of geomagnetic field intensity during the High Middle Ages is not yet well established. Despite their differences, geomagnetic global models predict our results reasonably well. This work indicates the need to obtain a number of archeointensity data for each time interval in order to reliably record variations of the geomagnetic field and to test whether any relationship exists between field intensity and climate.
New high precision full-vector archaeomagnetic data from a roman kiln in Mérida (Spain)
Physics of the Earth and Planetary Interiors 309
This study presents new high precision age and full-vector archaeomagnetic data from a kiln excavated in the Roman archaeological site of Mitreo's house (Mérida, Badajoz, Spain). The age of the kiln was obtained by the stratigraphic method and by the ceramological study of the italic and sigillata pottery found with a very precise age date of 55 ± 15 years AD. Rock-magnetic experiments pointed towards magnetite as the main carrier of remanence and highly reversible thermomagnetic curves suggested that the studied samples were suitable for archaeoeointensity determinations.Paleomagnetic experiments including thermal and stepwise alternating field demagnetization yielded the following mean direction for the kiln: declination D = 0.6°; inclination I = 54.0°; (k = 481; α95 = 2.5°). Archaeointensityexperiments with the Thellier-Coe protocol on 28 samples yielded successful determinations in 27 cases. Anisotropy factors between 0.90 and 1.04 were obtained from anisotropy of thermoremanent magnetization (ATRM) experiments. A mean anisotropy-corrected archaeointensity value F = 56.3 ± 5.5 μT was obtained. The geomagnetic model SHA.DIF.14 k was used for an archaeomagnetic dating yielding a chronological interval between 40 BCE and 150 CE. This low age resolution when compared with the pottery-based age data is related to the behavior of the geomagnetic field in the Iberian Peninsula during the Roman period, which does not allow to differentiate well between results corresponding to those centuries. However, it is also related to the fact that the Iberian archaeomagnetic dataset in the analysed time range is highly scattered. A high quality full-vector data with a very precise age have been obtained which contribute to improve the Iberian secular variation curve and geomagnetic databases.