Facile asymmetric construction of a functionalized dodecahydrobenz[a]indolo[3,2-h]quinolizine template (original) (raw)

Facile asymmetric construction of a functionalized dodecahydrobenz[a]indolo[3,2-h]quinolizine template

Tetrahedron, 2009

Abstract

... Ethyl acetate was distilled over calcium sulfate or chloride. Dichloromethane was distilled over calcium hydride. 4.1. Methyl 2-(8-oxo-1,4-dioxaspiro[4.5]decan-7-yl)acetate (4). ... Found: 228.1074). 4.2. Methyl 2-(8-methylene-1,4-dioxaspiro[4.5]decan-7-yl)acetate (5). ...

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