Oblique Incidence Ultrasonic Reflectometry Device Based on c-axis Tilted ScAlN Films for Evaluating Viscoelastic Properties of Liquids Above 100 MHz (original) (raw)
Related papers
Ultrasonics, 2010
In this work, we propose a study dedicated to the influence of the delay line nature in transverse ultrasonic sensors, dedicated to dynamic high frequency elastic moduli of viscoelastic materials estimation. In literature, these shear ultrasonic rheometers are using delay lines in glass or quartz and normal or oblique incidence of ultrasonic rays. The oblique incidence is used in order to improve the sensitivity of the measurements. We theoretically demonstrate in this work that the use of delay lines in polymers is recommended to improve the sensitivity. Due to modifications, performed on a 10 MHz commercial ultrasonic sensor, we experimentally show on glycerin (which is a Newtonian material) that it is possible to multiply by a factor 10 the sensitivity; compared to delay lines in quartz using a normal incidence of rays. Hence, we overpass the accuracy of the oblique incidence approach with a simpler experimental setup.
Ultrasonics, 2019
In-situ measurement of viscosity advances the field of rheology, and aides the development of sensing systems for condition and performance monitoring of lubricated mechanisms. Many lubricated mechanisms, such as journal bearings or seals, are characterised by three-layer interfaces; an oil separating two solid (usually metallic) bodies. The viscoelastic study of the lubricating oil in layered systems is possible in-situ by means of ultrasonic reflection (Schirru et al. (2015)). General solutions exist for the reflection of longitudinal plane waves from multi-layered solid-fluid systems. Similar solutions can be applied to plane shear waves. The use of a quarter-wavelength intermediate matching layer improves the sensitivity of the ultrasonic measurement and overcomes problems of acoustic mismatch. This opens the possibility of using reflectance methods to measure engineering (metal-oil) bearing applications that are acoustically mismatched. In this paper, a rigorous mathematical model for wave propagation in a three-layer system is solved for the reflection coefficient modulus and validated using a quarter wavelength ultrasonic viscometer. The model was tested against experimental data for two Newtonian reference fluids, water and hexadecane, and for one non-Newtonian reference fluid, squalene plus polyisoprene (SQL + PIP), measured ultrasonically at frequencies between 5 and 15 MHz. The results are in agreement with the expected viscosity values for the reference fluids. Further, the viscosity measurement is not limited to the resonance frequency, but it is performed over a broad band frequency range. This is important to improve measurement confidence and accurate spectroscopy measurement for the determination of viscoelastic properties.
Viscosity measurement in thin lubricant films using shear ultrasonic reflection
Proceedings of the Institution of Mechanical Engineers, Part J: Journal of Engineering Tribology, 2008
When a shear ultrasonic wave is incident on a solid and liquid boundary, the proportion that is reflected depends on the liquid viscosity. This is the basis for some instruments for on-line measurement of bulk liquid viscosity. In machine elements, the lubricant is usually present in a thin layer between two rubbing solid surfaces. The thin film has a different response to an ultrasonic shear wave than liquid in bulk. In this work, this response is investigated with the aim of measuring viscosity in situ in a lubricating film. The proportion of the wave reflected at a thin layer depends on the layer stiffness. A shear wave is reflected by the shear stiffness of the thin layer. For a thin viscous liquid layer, the stiffness is a complex quantity dependent on the viscosity, wave frequency, and film thickness. This stiffness is incorporated into a quasi-static spring model of ultrasonic reflection. In this way, the viscosity can be determined from shear-wave reflection if the oil-film ...
Proceedings of the Institution of Mechanical Engineers, Part J: Journal of Engineering Tribology, 2015
The apparent viscosity of oils in the thin layers that exist in machine elements such as gears and bearings is very different to that in the bulk. In addition, oils in lubricating layers are characterized by non-Newtonian behaviour due to the severe thermodynamic conditions that arise. It is this viscosity that determines the film thickness in lubricated mechanical components. This paper describes a novel methodology based on an ultrasonic approach to determine viscosity in situ in a lubricated contact. The methodology considers the lubricant at the solid boundary as a Maxwell viscoelastic fluid and determines its response to an ultrasonic wave. This approach is then compared with existing methodologies in both a static contact and in a rotating journal bearing. The obtained results have shown that the algorithm proposed in this study is most suitable to study lubricants in the range of 0.3–3 Pas and the measurement error has been found to be less than 10%. This viscosity range is c...
Liquid dynamic viscosity measurement by ultrasonic wave mode conversion
2005
This work presents a cell to measure the liquid dynamic viscosity using an ultrasonic wave mode conversion from longitudinal to shear wave and vice-versa. A prototype-measuring cell was constructed to test the proposed method. Measurements of the viscosity of automotive oils (SAE 90 and SAE140) were obtained in the frequency range from 1 to 10 MHz. These results are also compared with the Maxwell model with two relaxation times, showing the dependency of dynamic viscosity with the frequency of the shear wave. The experimental data are in good agreement with those provided by the Maxwell model.
The Journal of the Acoustical Society of America, 2004
Shear wave elasticity imaging ͑SWEI͒, an emerging acoustic technology for medical diagnostics, is based on remote generation of shear waves in tissue by radiation force in the focal region of an ultrasonic beam. In this study, the feasibility of Doppler ultrasonic technique to visualize the remotely induced shear waves was demonstrated. The generation of shear displacement in the focal region of a pulsed 1-MHz ultrasound beam with pulse duration of approximately about 2 ms and intensity levels on the order of 145 W/cm 2 , and consequent propagation of shear wave in tissue-mimicking and muscle tissue in vitro, were measured. The analysis of temporal behavior of shear displacement within the focal plane allowed estimation of shear wave velocities. The velocities were 4 and 7 m/s in hard phantom and tissue containing phantom, respectively. The measured shear displacements on the order of micrometers in gel-based phantoms are in reasonable agreement with theoretical estimates derived from an earlier developed model of shear wave generation by radiation force of focused ultrasound. The study revealed significant dependence of shear strain on the medium viscosity. The complex oscillatory character of shear strain relaxation in viscoelastic phantom and muscle tissue in vitro was observed.
Effect of viscosity on ultrasound wave reflection from a solid/liquid interface
Ultrasonics, 1996
Ultrasonics is the world's leading journal dedicated to the whole science and technology of ultrasound. Contributed material is welcomed in the following fields: elasticity, anelasticity and magnetoelasticity; ultrasonic sensors for process monitoring; nondestructive materials characterization; generation and detection of ultrasound; ultrasonic NDE and NDT; SAW devices; signal processing; acoustooptics; physics of ultrasound; ultrasonic wave propagation; ultrasonic visualization; ultrasonic microscopy; physics and technology of ultrasound in medicine and biology; high-power ultrasonics; actuators and motors; industrial ultrasonics; underwater ultrasonics.
Viscoelastic shear modulus measurement of thin materials by interferometry at ultrasonic frequencies
The Journal of the Acoustical Society of America, 2019
This paper presents a technique for measuring the complex shear modulus of thin slabs of viscoelastic solids based on the measurement of the reflection and transmission of plane shear waves through a sample inserted between two delays lines. Reproducible shear wave transmission through the sample is achieved by inserting bond layers with controlled thickness between the delay lines and the sample and by characterizing beforehand the bond rheology. The frequency dependent complex shear modulus is quantitatively evaluated from the transmission and reflection coefficients using an exact model of interferences within the delay line-bond-sample-bond-delay line sandwich and by selecting the solution among the muliple solutions of the inverse problem from considerations on time of flight and sample thickness. Thanks to its reproducibility and accuracy, this method appears as an original and efficient technique for quantitatively characterizing the high frequency shear modulus of attenuating materials. V
Japanese Journal of Applied Physics
It is important to evaluate the viscoelasticity of muscle for assessment of its condition. However, quantitative and noninvasive diagnostic methods have not yet been established. In our previous study, we developed a method, which used ultrasonic acoustic radiation forces irradiated from two opposite horizontal directions, for measurement of the viscoelasticity. Using two continuous wave ultrasounds, an object can be actuated with an ultrasonic intensity, which is far lower (0.9 W/cm 2) than that in the case of the conventional acoustic radiation force impulse (ARFI) method. In the present study, in vitro experiments using phantoms made of polyurethane rubber and porcine muscle tissue embedded in a gelatin block were conducted. We actuated phantoms by ultrasonic radiation force and measured the propagation velocity of the generated shear wave inside the phantoms using a diagnostic ultrasound system. The viscoelasticities of phantoms were estimated by fitting a viscoelastic model, i.e., the Voigt model, to the frequency characteristic of the measured shear wave propagation speed. In the mechanical tensile test, a softer polyurethane phantom exhibited a lower elasticity and a higher viscosity than a polyurethane phantom with a higher elasticity and a lower viscosity. The viscoelasticity measured by ultrasound showed the same tendency as that in the tensile test. Furthermore, the viscoelasticity of the phantom with porcine muscular tissue was measured in vitro, and the estimated viscoelasticity agreed well with that reported in the literature. These results show the possibility of the proposed method for noninvasive and quantitative assessment of the viscoelasticity of biological soft tissue.