Influence of the Phase Transformation Behaviour on the Microstructure and Mechanical Properties of a 4.5 wt.-% Mn Q Steel* (original) (raw)

Influence of Austenite Phase Transformation on Existing Microstructure of Low C-Mn Steel

Engineering, Technology & Applied Science Research, 2018

Cold heading quality CHQ steel is widely used for making small components due to its excellent cold heading response. Austenite nucleation and growth morphology of a commercial CHQ steel has been studied by continuous heating experiments using lead-bath up-quenching at different heating temperatures. Modern optical microscope Olympus GX51, scanning electron microscopy techniques have been deployed to reveal and interpret the microstructure. It was found that at 740°C the microstructure shows lack of homogeneity, hence the cold-head-ability of CHQ steel is anisotropic. At high temperatures, in austenite domain, at 60sec, the resultant austenite is highly homogenous. Then the cold-head-ability properties of CHQ steel turned to be isotropic.

The Microstructure and Phase Composition of 35CrSiMN5-5-4 Steel After Quenching and Partitioning Heat Treatment

Archives of Metallurgy and Materials

The aim of the study was to characterise the microstructure of 35CrSiMn5-5-4 steel which was subjected to a new heat treatment technology of quenching and partitioning (Q&P). The parameters of the treatment were chosen on the basis of computer simulations and dilatometric studies of phase transformations occurring in steel. The transmission electron microscopy (TEM) observations of steel microstructure after the Q&P treatment revealed the presence of martensite as well as significant amount of retained austenite in form of layers between the martensite laths. The rod-like carbides in the ferritic areas were also observed, which indicates the presence of lower bainite in steel. It was found that the retained austenite content measured by means of TEM was about 28% for partitioning at 400°C and 25% for partitioning at 260°C. These results are in good agreement with the phase composition calculated theoretically as well as those determined experimentally by use of dilatometric tests.

Dilatometric Study of Phase Transformations in 5 Mn Steel Subjected to Different Heat Treatments

Materials

The work presents results of phase transformation kinetics of hot-rolled 5% Mn steel subjected to different heat treatments. Three different schedules were introduced: isothermal holding in a bainite region, coiling simulation and intercritical annealing. The evolution of microstructure components was investigated using dilatometric and metallographic analyses. According to obtained results, the medium-Mn steel exhibits high resistance for γ/α transformation during the bainite transformation and coiling simulation (upon cooling from the austenite region). During 5 h isothermal holding, no bainite and/or ferrite formation was detected. This results in the formation of martensite upon cooling to room temperature. Differently, when the steel was subjected to the intercritical annealing at 720 and 700 °C (upon heating from room temperature), a final microstructure consisted of ferrite, martensite and retained austenite. At 700 °C, no fresh martensite formation was detected upon cooling ...

Application of Quenching and Partitioning Processing to Medium Mn Steel

Metallurgical and Materials Transactions A, 2014

The present work analyzes the application of quenching and partitioning processing to medium Mn steel to obtain a new type of ultra-high-strength multiphase medium Mn steel. The selection of the quench temperature makes it possible to vary the ultimate tensile strength within a range of 500 MPa. The processing leads to lowcarbon lath martensite matrix with a controlled volume fraction of retained austenite.

Heat treatment effects on the microstructure and mechanical properties of a medium manganese steel (0.2C-5Mn

Materials Science and Engineering A-structural Materials Properties Microstructure and Processing

Microstructures and mechanical properties of 0.2C–5Mn steel processed under different heat treatment conditions were examined by scanning electron microscopy (SEM), Transmission electron microscopy (TEM) and X-ray diffraction (XRD). It was found that high temperature austenization (above Ac3) resulted in a full martensite structure after quenching, which gradually transformed into the ferrite/austenite duplex structure during the following annealing process. However, austenization in the intercritical region (between Ac1 and Ac3) gave a duplex structure after quenching, which was nearly not affected by followed annealing process. The ultrahigh strength ∼1000 MPa and total elongation ∼40% were only obtained in the specimens with 6 h annealing at 650 °C under both heat treatment conditions. However, the excellent mechanical properties could be obtained in the intercritically austenitized samples with only 10 min annealing at 650 °C. Based on the analysis on the relationship between microstructure and mechanical properties, it was found that the total elongation was strongly dependent on the austenite fraction, which was ascribed to the phase transformation induced plasticity of the large volume fraction of austenite. Otherwise, the dependence of the yield stress on the austenite grain size accords with Hall-Petch equation, which implies that the austenite is soft phase. It was concluded that 10 min annealing at 650 °C was enough to obtain a large volume fraction of austenite (∼30%) in 0.2C–5Mn steel when the specimens were austenitized at 675 °C.► Substantially improved mechanical properties of 0.2C–5Mn steels. ► Intercritical austenization followed by short time annealing. ► Phase transformation induced plasticity of the large volume fractioned austenite. ► Dependence of yield stress on austenite grain size accords with Hall–Petch equation.

Influence of the Quenching and Partitioning Process on the Transformation Kinetics and Hardness in a Lean Medium Manganese TRIP Steel

Metals

The quenching and partitioning (Q&P) process of lean medium Mn steels is a novel approach for producing ultra-high strength and good formable steels. First, the steel is fully austenitized, followed by quenching to a specific quenching temperature (TQ) in order to adjust an appropriate amount of initial martensite (α’initial). Subsequently, the steel is reheated to a partitioning temperature (TP) in order to ensure C-partitioning from α’initial to remaining austenite (γremain) and thus retained austenite (RA) stabilization. After isothermal holding, the steel is quenched to room temperature (RT), in order to achieve a martensitic-austenitic microstructure, where the meta-stable RA undergoes the strain-induced martensitic transformation by the so-called transformation induced plasticity (TRIP) effect. This paper systematically investigates the influence of the Q&P process on the isothermal bainitic transformation (IBT) kinetics in a 0.2C-4.5Mn-1.3Al lean medium Mn steel by means of d...

Microstructure evolution and phase composition of high-manganese austenitic steels

ABSTRACT Purpose: The aim of the paper is to determine the influence of hot-working conditions on microstructure evolution and phase composition of new-developed high-manganese austenitic steels. Design/methodology/approach: Determination of processes controlling strain hardening was carried out in continuous compression test using Gleeble 3800 thermo-mechanical simulator. Evaluation of processes controlling work hardening and occurring after deformation at 900°C were identified by microstructure observations of the specimens solution heat-treated after plastic deformation to a true strain equal 0.23, 0.50 and 0.91. Phase composition of steels was confirmed by X-ray diffraction analysis. Findings: The steels have a fine-grained austenite microstructure with many annealing twins to a temperature of about 1000°C. The initiation of dynamic recrystallization occurs already after true deformation equal 0.29. Participation of fine grains arranged in a matrix of dynamically recovered grains essentially increases after increasing true strain to 0.5. Fully dynamically recrystallized microstructure of steel can be obtained after the true strain equal 0.9. The conditions of hot-working influence phase state of investigated steels. Steel no. 1 keeps stable austenite microstructure independently from conditions of plastic deformation. Steel with initial bi-phase microstructure keeps a certain portion of ε martensite, yet dependant on conditions of hot-working.

Dilatometric study of phase transformations in advanced high-strength bainitic steel

Journal of Thermal Analysis and Calorimetry, 2014

The work deals with dilatometric studies of a new-developed advanced high-strength bainitic 3Mn-1.5Al steel. Ferritic, bainitic and martensitic phase transformations are investigated in detail in respect of their temperature range forming and microstructures produced under various conditions of both continuous and isothermal cooling. The equilibrium temperatures of A e1 and A e3 and phase composition of the investigated steel were initially calculated whereas critical temperatures of A c1 and A c3 as well as the decomposition of retained austenite were determined upon heating. The major tests consisted of controlled cooling of undeformed or plastically deformed austenite using the dilatometer within the cooling rate range of 2-0.5°C s-1. The effects of the cooling rate and deformation at temperatures of 900 and 1,050°C on the phase transformation behaviour and microstructure were explained. The final experiment was carried out using a thermo-mechanical simulator under conditions of multistep deformation and isothermal holding of the steel at 400°C. Microstructural features were revealed using light microscopy and scanning electron microscopy techniques.

Influence of phase transformations on the mechanical properties of high-strength austenitic Fe-Mn-Cr steel

Metallurgical and Materials Transactions A, 2006

The influence of Cr and N additions on the mechanical properties of a Fe-Mn-C steel was investigated. The chemical composition was found to have a pronounced effect on the strain-hardening behavior, due to the strain-induced sequence of the ␥ : : ␣Ј martensitic transformations. It was found that Cr and N suppress this transformation sequence. At Cr levels higher than 7.5 mass pct, no ␣Ј martensite was formed, which led to a pronounced improvement of the ductility. The differences in transformation behavior can be attributed to the change in the intrinsic stacking-fault energy (ISFE): in the compositional range studied, Cr and N additions cause an increase of the ISFE.

Austenitizing Temperature and Cooling Rate Effects on the Martensitic Transformation in a Microalloyed-Steel

Materials Research, 2020

The effects of the austenitizing temperature and the cooling rate upon the kinetic of athermal martensitic transformation in a microalloyed steel were evaluated. Considering the studied steel, the knowledge about these effects on the martensitic transformation has a great relevance for naval manufacturers and steel researchers. In this study, computational simulation was performed aiming to evaluate the phase's stability. Specimens were submitted to quenching simulations in a dilatometer, considering four different austenitizing temperatures and four cooling rates. The results shown that the austenite chemical composition was not significantly affected by the austenitizing temperatures. Both the austenitic grain size and the cooling rate affected the martensitic transformation kinetics. The larger the austenitic grain size, the higher the Ms. The austenitic grain growth promoted a decrease in the required chemical energy to compensate the free energy increase associated with the lattice strain and the creation of new interfaces, leading to a lower austenite undercooling. An extrinsic effect of the cooling rate on the Ms was observed. For lower cooling rates, the carbide precipitation modified que austenite chemical composition, changing its stability and increasing Ms. A predictability equation, correlating the M S with the austenite grain size and the steel cooling rate, was proposed.