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Research paper thumbnail of ChemInform Abstract: CuAAC: An Efficient Click Chemistry Reaction on Solid Phase

Research paper thumbnail of CuAAC: an efficient Click Chemistry reaction on Solid Phase

ACS combinatorial science, Jan 11, 2015

Click Chemistry is an approach that uses efficient and reliable reactions, such as Cu(I)-catalyze... more Click Chemistry is an approach that uses efficient and reliable reactions, such as Cu(I)-catalyzed azide-alkyne cycloaddition (CuAAC), mainly to bind two molecular building blocks. In addition, CuAAC has showed broad applications in medicinal chemistry and other fields of chemistry. The present review describes the general features and applications of CuAAC in solid-phase (CuAAC-SP), highlighting the suitability of this kind of reaction for peptides, nucleotides, small molecules, supramolecular structures, and polymers, among others. This versatile reaction is expected to become pivotal for meeting future challenges in solid-phase chemistry.

Research paper thumbnail of Resin via click chemistry to apply in SPPS

Research paper thumbnail of Imidazole-1-sulfonyl Azide-Based Diazo-Transfer Reaction for the Preparation of Azido Solid Supports for Solid-Phase Synthesis

ACS Combinatorial Science, 2013

An efficient, standard, mild, and copper-free imidazole-1-sulfonyl azide hydrochloride-based diaz... more An efficient, standard, mild, and copper-free imidazole-1-sulfonyl azide hydrochloride-based diazo-transfer method was implemented in a set of four resins that cover a broad range of hydrophobicity. The imidazole-1-sulfonyl azide hydrochloride is easily prepared/commercially available, stable upon storage at 4°C

Research paper thumbnail of Recent Tricks in Solid-Phase Peptide Synthesis

Peptides as drugs show unique characteristics (high biological activity, high specificity and low... more Peptides as drugs show unique characteristics (high biological activity, high specificity and low toxicity), thereby making them particularly attractive therapeutic agents. During the last years, the pharmaceutical industry, which was traditionally focused on small molecules, has been attracted by the benefits that peptides confer. This is due in part, for the great number of developments carried out in their synthetic strategies, mostly in the Solid-Phase mode.

Research paper thumbnail of Wang Linker Free of Side Reactions

Organic Letters, 2013

A new resin for the solid-phase synthesis of peptide acids was developed. It was based on a linke... more A new resin for the solid-phase synthesis of peptide acids was developed. It was based on a linker with two unique features: methoxy groups as the only activating groups of the phenyl ring and a copper(I)-catalyzed Click chemistry reaction to anchor it to the solid support. The efficiency of this new resin in solid phase peptide synthesis was compared with that of Wang resin.

Research paper thumbnail of ChemInform Abstract: CuAAC: An Efficient Click Chemistry Reaction on Solid Phase

Research paper thumbnail of CuAAC: an efficient Click Chemistry reaction on Solid Phase

ACS combinatorial science, Jan 11, 2015

Click Chemistry is an approach that uses efficient and reliable reactions, such as Cu(I)-catalyze... more Click Chemistry is an approach that uses efficient and reliable reactions, such as Cu(I)-catalyzed azide-alkyne cycloaddition (CuAAC), mainly to bind two molecular building blocks. In addition, CuAAC has showed broad applications in medicinal chemistry and other fields of chemistry. The present review describes the general features and applications of CuAAC in solid-phase (CuAAC-SP), highlighting the suitability of this kind of reaction for peptides, nucleotides, small molecules, supramolecular structures, and polymers, among others. This versatile reaction is expected to become pivotal for meeting future challenges in solid-phase chemistry.

Research paper thumbnail of Resin via click chemistry to apply in SPPS

Research paper thumbnail of Imidazole-1-sulfonyl Azide-Based Diazo-Transfer Reaction for the Preparation of Azido Solid Supports for Solid-Phase Synthesis

ACS Combinatorial Science, 2013

An efficient, standard, mild, and copper-free imidazole-1-sulfonyl azide hydrochloride-based diaz... more An efficient, standard, mild, and copper-free imidazole-1-sulfonyl azide hydrochloride-based diazo-transfer method was implemented in a set of four resins that cover a broad range of hydrophobicity. The imidazole-1-sulfonyl azide hydrochloride is easily prepared/commercially available, stable upon storage at 4°C

Research paper thumbnail of Recent Tricks in Solid-Phase Peptide Synthesis

Peptides as drugs show unique characteristics (high biological activity, high specificity and low... more Peptides as drugs show unique characteristics (high biological activity, high specificity and low toxicity), thereby making them particularly attractive therapeutic agents. During the last years, the pharmaceutical industry, which was traditionally focused on small molecules, has been attracted by the benefits that peptides confer. This is due in part, for the great number of developments carried out in their synthetic strategies, mostly in the Solid-Phase mode.

Research paper thumbnail of Wang Linker Free of Side Reactions

Organic Letters, 2013

A new resin for the solid-phase synthesis of peptide acids was developed. It was based on a linke... more A new resin for the solid-phase synthesis of peptide acids was developed. It was based on a linker with two unique features: methoxy groups as the only activating groups of the phenyl ring and a copper(I)-catalyzed Click chemistry reaction to anchor it to the solid support. The efficiency of this new resin in solid phase peptide synthesis was compared with that of Wang resin.

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